扩散场扇扫重建格林函数实现近表盲区缺陷检测

针对结构近表盲区缺陷检测难题,发展了一种扩散声场扇扫重建格林函数的超声检测方法.在对扩散场扇扫重建格林函数理论分析的基础上,通过5 MHz超声相控阵探头对铝块近表盲区缺陷进行了检测实验并对影响成像结果的延时时间、时间窗宽和扫查方式进行了分析.结果显示,该方法可以有效检测铝块近表1.5?3 mm的盲区缺陷;扇形扫查方式的...     

肝素钠掺杂球状聚吡咯的合成及其电化学电容

以生物制剂肝素钠为掺杂剂,由自组装方法合成出平均粒径为100 nm的球状聚吡咯(PPy),用作超级电容器电极材料.透射电镜(TEM)、循环伏安、恒流充放电和电化学交流阻抗测试表明,肝素钠掺杂聚吡咯呈现较好的形貌和电容性质,在电流密度3 mA/cm2下充放电,单电极比电容达到338 F/g.     

广义模糊粗糙集的不确定性度量

研究广义模糊粗糙集的不确定性问题,利用一种新的信息熵定义模糊粗糙集的模糊性度量,并给出这种度量的性质,证明当且仅当A是经典可定义集合时其模糊粗糙集的模糊性度量FR(A)等于0。     

Size and temperature effects on band gaps in periodic fluid-filled micropipes

A new model is proposed for determining the band gaps of flexural wave propagation in periodic fluid-filled micropipes with circular and square thin-wall cross-sectional shapes, which incorporates temperature, microstructure, and surface energy effects. The band gaps depend on the thin-wall cross-sectional shape, the microstructure and surface elastic material constants, the pipe wall thickness, the unit cell length, the volume fraction, the fluid velocity in the pipe, the temperature change,and the thermal expansion coefficient. A systematic parametric study is conducted to quantitatively illustrate these factors. The numerical results show that the band gap frequencies of the current non-classical model with both circular and square thin-wall cross-sectional shapes are always higher than those of the classical model. In addition,the band gap size and frequency decrease with the increase of the unit cell length according to all the cases. Moreover, the large band gaps can be obtained by tailoring these factors.     

新型手性氨基酸烯砜的合成

以苯亚磺酸钠和3-氯-2-甲基-1丙烯为原料,经偶联、氯化、溴化,之后再与氨基酸胺化反应合成得到了两个新型手性氨基酸烯砜化合物。所获得化合物的结构经HR-MS,1H,13C和/或DEPT NMR验证。