SPME-GC-MS快速分析炼油厂废水中痕量VOCs

采用固相微萃取-气相色谱-质谱联用(SPME-GC-MS)对炼油厂废水中痕量挥发性有机化合物(VOCs)进行了定性分析,简化了预处理过程,总分析时间为1h左右.对比处理前后的废水样品的MS定性结果,为废水处理工艺的评价以及有机物降解机理提供了依据.     

Synthesis,structure, spectroscopic and magnetic properties of a novel two-dimensional copper(II) complex Na2[Cu(pba)] · 6H2O [pba = 1,3-propylenebis(oxamato)]

The copper(II) complex Na₂[Cu(pba)] · 6H₂O has been synthesized and its structure determined. It consists of a novel two-dimensional network of [Cu(pba)]^2– anions connected to each other through the sodium ion as a bridge. Spectroscopic and magnetic properties have been measured and a spin distribution calculation has been carried out with the GAUSSIAN-94. Theoretical calculations indicate the rather larger spin density on nitrogen atoms should be responsible for the satellite lines appearing beside the main hyperfine coupling signs of copper(II). The antiferromagnetic interaction may be due to the intermolecular interaction and/or different copper(II) ions through the Na⁺ bridge in the same layer.     

非等间距序列建模过程中存在的问题及改进

在研究非等间距序列的基础上 ,本文将非等间距累加运用于非等间距序列的建模过程中 ,使原有模型得到改进 .实例表明 ,改进后模型的精度有了很大提高     

Control of LHCD on the HL-2A Tokamak

in order to study non-indutive plasma current production, the lower hybrid current drive（LHCD） experiment on the HL-2A tokamak is carried out. Simultaneously a microcomputer has been used to control the whole LHCD system. During the experiment this year, we can monitor and protect the LHCD system by use of the microcomputer control system, which will imediately switch off the microwave power to be launched into the tokamak if the plasma is disrupted. All this ensure that the microwave is injected into the equipment correctly.     

蓝宝石R面上ZnO薄膜的NH3掺杂研究

以NH₃为掺杂源,利用金属有机化学气相沉积(MOCVD)系统在蓝宝石R面上生长出掺氮ZnO薄膜。通过XRD,SEM测量优化了其生长参数,在610℃和在80sccm的NH₃流量下生长出了〈1120〉单一取向的ZnO薄膜。经Hall电阻率测量,得知该薄膜呈现弱p型或高电阻率,并对其光电子能谱进行了研究。     

高频聚焦换能器声场的激光测量法

本文描述了一种使用激光测振技术测量高频聚焦换能器声场布的方法，并给出了使用该方法对一种高频聚换能器进行测量的结果，通过理论计算对结果的正确性进行了验证。     

铁铝催化体系催化丙烯酸丁酯聚合

研究了Fe(acac)3-Al(i-Bu)3-8-羟基喹啉(acac=乙酰丙酮)催化体系催化丙烯酸丁酯(BA)聚合，考察了聚合规律，用凝胶渗透色谱研究了聚合物分子量和分子量分布．动力学研究表明聚合反应对单体浓度呈一级关系，表观活化能为13．9kJ／mol．     

锥形光纤间耦合特性的分析与检测

将通信光纤的末端拉制成锥形，利用光信号在光纤锥形区特有的传输和耦合特性，实现了光纤的耦合、连接和分束。用耦合模理论分析了锥形光纤间的传输和耦合性质，给出了光信号两锥形光纤间的耦合与两锥形光纤的距离和锥形区重叠长度等实验结果。     

半导体激光自混频干涉式传感器中的干涉与调制

应用F-P模型，阐述了半导体激光自混频干涉式传感器的干涉与调制过程，同时给出了相应的计算．     

修正的Shepard型算子的Lp-逼近

摘要:本文在L_[0.1]~p空间给出了 Durrmeyer型修正的shepard算子D_n(f,x),对 f∈L_[0.1]~p,(p≥1),得到了下列的Jackson型估计:││D)n(f)-f││_p≤ C_(pλω)(f,n~(-1))p,λ≥2, Cω(f,n~(-1)logn)p,λ=2, C_(pλω)(f,n~(-1))p,1<λ<2,