基于Shibboleth的校际跨域认证研究与实现

分析比较跨域认证相关技术,基于Shibboleth的跨域认证系统最适合用于校际间的身份认证,实现资源和服务的单点登录和共享,因此通过对Shibboleth认证机制的改进,实现校际间的LDAP认证方式、关系型数据库认证方式和SAML2认证方式的认证集成.最后,在跨校认证基础上构建资源共享应用和全局服务应用.     

大变倍比光学被动半无热化变焦系统设计

针对传统变焦光学系统在环境温度变化的情况下,变焦全程无法一致清晰成像以及需频繁调焦的问题,提出了一种光学被动半无热化变焦系统设计方法,并设计了一种光学被动半无热化变焦系统.变焦系统的焦距为30～1000mm,工作波段为486～656 nm,光圈为F4.4～F8,短焦采用光学被动无热化设计.变焦系统的成像质量良好,结构非...     

聚变堆熔盐冷却偏滤器靶板结构设计与分析

为提高偏滤器的抗中子辐照能力,兼顾高热承载能力和聚变堆经济性的需要,提出了基于熔盐冷却(MSC)的偏滤器靶板结构设计。它采用FLiNaK作为冷却剂,钨镧合金为热沉材料,钨为第一壁材料。通过数值计算评估了靶板的热负荷承载能力,并完成了偏滤器冷却剂回路设计,优化了偏滤器各模块之间的流量分配。此MSC偏滤器靶板设计可以有效去除10~15MW•m^-2热负荷,为适应未来聚变堆偏滤器靶板发展的需要提供了一种设计解决方案。     

Synthesis of a Novel Flame Retardant and Its Synergistic Effect With a Phosphapheanthrene Flame Retardant in Polypropylene/Polyethylene Vinyl Acetate Blends

A novel flame retardant (NSiB) containing nitrogen, silicon and boron was synthesized through reacting of N-(β-aminoethyl)-γ-aminopropyl trimethoxy-silane (KH-792) and boric acid. The structure of NSiB was characterized by Fourier transform infrared (FTIR) spectroscopy and scanning electron microscopy with energy dispersive spectrometry (SEM-EDS). The effects of NSiB on the flame retardancy and thermal behaviors of polypropylene (PP)/polyethylene vinyl acetate (EVA) blends were investigated by limiting oxygen index value (LOI), vertical burning tests (UL-94) and thermal gravimetric analysis tests (TGA). The results showed that the flame retardancy and thermal stability of PP/EVA blends were improved with the addition of NSiB. When 7.5 wt% DOPO (phosphaphenanthrene) and 0.5 wt% NSiB were incorporated, the LOI value of the PP/EVA blends was 26.9%, and the class V-0 of UL-94 test was passed, as compared to the LOI value of 22.4% and class V-2 of UL-94 test for 8.0 wt% DOPO only and 16.7% and fail, respectively, for the PP/EVA blends alone. The char structure observed by SEM indicated that the surface of the char for the PP/EVA/7.5 wt% DOPO/0.5 wt% NSiB blends had a denser and continuous char structure when compared with that of the PP/EVA blends and PP/EVA/8.0 wt% DOPO blends. These results indicated that there was a good synergistic effect for NSiB and DOPO.     

HIAF高能辐照终端感生放射性

本工作是基于蒙特卡罗模拟软件FLUKA对高能强流重离子加速器（HIAF）高能辐照终端感生放射性进行初步研究。该终端可运行质子最高能量为9.3 GeV,最大流强是1.45×1012 pps（particle per second）。研究内容包括:（1）预测高能辐照终端内活化物质的放射性活度特性;（2）预测不同冷却时间高能辐照终端内残余剂量率分布。研究结果表明,HIAF正常运行时高能辐照终端内的感生放射性主要受束流垃圾桶活化产生的放射性核素影响。当加速器连续运行100天冷却4小时,垃圾桶表面残余剂量率为2.375 mSv·h-1。终端内空气中13N和15O动态饱和比浓度大于其对应的导出空气浓度。冷却水中13N和15O的活度大于对应的ALI_min。该研究是HIAF辐射防护基础研究以及加速器环境影响评价的一项重要内容。The Monte Carlo code FLUKA was used to predict the induced radioactivity of high-energy irradiation terminal of HIAF. The maximum energy of proton is 9.3 GeV, and the maximum current is 1.45×1012 pps (particle per second). In this study we were to predict:(1) the activity properties of activated substances in the experimental terminal; (2) the residual dose rate distribution in the experimental terminal at different cooling time. The results indicate that the induced radioactivity in the high energy irradiation terminal of the HIAF is mainly affected by the radionuclide induced in the beam dump. The residual dose rate on the surface of the beam dump is 2.375 mSv·h-1, after 100 d irradiation and 4 h cooling. The dynamic saturation ratio of 13N and 15O induced in the air inside the terminal is higher than its corresponding derived air concentration. The activity of 13 N and15O induced in cooling water is higher than its ALI_min. This study is a part of radiation protection basic research and environmental impact assessment for HIAF.     

重离子冷却储存环CSRm双电子复合实验研究类锂36,40Ar15+离子同位素移动

配备电子冷却装置的重离子储存环为开展高电荷态离子的双电子复合（dielectronic recombination,DR）精密谱学研究提供了绝佳的实验平台。本工作在兰州重离子加速器冷却储存环主环（HIRFL-CSRm）上开展了类锂36,40Ar15+离子的双电子复合实验,实验观测了电子-离子质心系能量范围为0~35 eV的双电子复合速率系数谱。通过外推法获得了36,40Ar15+离子2s_1/2→2p_1/2和2s_1/2→2p_3/2的跃迁能量。同时利用GRASP2K程序理论计算了36,40Ar15+离子2s_1/2→2p_1/2和2s_1/2→2p_3/2跃迁的质量移动因子和场移动因子,进而得到双电子复合谱的同位素移动值。36,40Ar15+离子2s_1/2→2p_1/2和2s_1/2→2p_3/2同位素移动分别为0.861 meV和0.868 meV。它们均小于目前CSRm上双电子复合实验的实验分辨为~10 meV,进而解释了实验测量的DR谱上未能观察到同位素移动的原因。然而,高电荷态离子的同位素移动场效应与原子序数Z5成正比,因此,在重离子加速器冷却储存环实验环（HIRFL-CSRe）以及未来大型加速器--强流重离子加速器装置（HIAF）上有望通过DR精密谱学方法研究高电荷态重离子甚至放射性离子的同位素移动,进而获得相关原子核的核电荷半径等信息。The cooler storage ring is equipped with an electron-cooler. It is an excellent experimental platform for dielectronic recombination (DR) experiment of highly-charged ions. In this paper, the dielectronic recombination experiments of lithium-like Ar15+ ions with mass number 36 and 40 are conducted at the HIRFL-CSRm(main ring of the Cooling Storage Ring of Heavy Ion Research Facility in Lanzhou). The experimental electron-ion collision energy scale is from 0 eV to 35 eV. Extrapolation method is exploited to obtain the excitation energies of transitions 2s_1/2→2p_1/2 and 2s_1/2→2p_3/2 of the 36,40Ar15+ ions from experimental data. Meanwhile, GRASP2K program is utilized to calculate the mass shift factors and field shift factors of 36,40Ar15+ ions for 2s_1/2→2p_1/2 and 2s_1/2→2p_3/2 transitions to obtain isotope shifts in DR spectra. In theoretical calculation, isotope shifts of 36,40Ar15+ ions corresponding to 2s_1/2→2p_1/2 and 2s_1/2→2p_3/2 are 0.861 meV and 0.868 meV, respectively. They are both less than the experimental precision (~10 meV) of these dielectronic recombination experiments at the CSRm, which explains that isotope shifts cannot be distinguished from the experimental dielectronic recombination spectra. However, the field shift of highly-charged ions is proportional to Z5. In the future, the dielectronic recombination experiments of highly-charged heavy ions even radioactive ions will be conducted at the HIRFL-CSRe (experimental ring of the Cooling Storage Ring of Heavy Ion Research Facility in Lanzhou) and the future large accelerator facility--HIAF(High intensity Heavy-ion Accelerator Facility) to measure isotope shifts to obtain the nuclear charge radius information.     

HIAF BRing及高能外靶实验终端的辐射屏蔽设计

强流重离子加速器（HIAF）是中国科学院近代物理研究所自主研制的一台高能强流重离子加速器,它可以实现p到U的全离子加速。为了保证HIAF运行时的辐射安全,针对该装置的增强器（BRing）及高能外靶实验终端,利用蒙特卡洛程序FLUKA及外推法计算得到了加速p,C及U三种离子时所需的辐射屏蔽。结果表明,加速质子时所需屏蔽厚度最大,并以此为依据给出了全地下结构的屏蔽设计。在此基础上,提出了一种估算高能质子/重离子加速器束流均匀损失时横向屏蔽厚度的方法。结果显示,估算结果与FLUKA计算结果符合较好,验证了该方法的有效性和准确性。High Intensity heavy-ion Accelerator Facility (HIAF) is designed by the Institute of Modern Physics, Chinese Academy of Sciences, which can accelerate particles from proton up to uranium. To guarantee the radiation safety of HIAF during operation, the FLUKA code and extrapolation method were adopted to calculate the shielding thickness. The calculations were based on proton, carbon and uranium particles when losing on the Booster Ring (BRing) and the high-energy experimental terminal. The results indicate that the shielding thickness required for accelerating protons was the largest. Basing on the results, a method for estimating the lateral shielding of a high-energy proton/heavy-ion accelerator was proposed. A good agreement shows between the estimated results and the FLUKA calculated results, the validity and accuracy of the method were verified.     

鞍山式铁矿SiO2含量的热红外光谱分析方法

SiO₂含量是铁矿石质量控制的主要技术指标,亦是衡量铁矿石品质好坏的关键指标之一,对选矿方法、配矿流程的确定具有重要意义。传统的SiO₂含量测定法虽然准确度高,但工作量大,操作繁琐,花费时间长,难以快速、高效确定铁矿石中SiO₂含量。采用红外光谱辐射计Turbo FT对辽宁省鞍钢集团鞍千矿业有限责任公司的“鞍山式”铁矿样品进行热红外光谱测试,分析了光谱特征,构建了比值指数(RI)、差值指数(DI)和归一化指数(NDI),并确定光谱指数与样品SiO₂含量相关性最显著的敏感波段及对应的相关系数值;优选出与样品SiO₂含量相关性最显著的归一化指数(NDI),构建样品SiO₂含量的定量反演模型,并进行了验证。结果表明,三种光谱指数与样品SiO₂含量的敏感波段均位于余辉带特征(RF)的左边界8.06与8.2 μm处,相关系数均达到0.9以上,其中NDI与样品SiO₂含量的相关性最高;基于NDI构建了实验样品SiO₂含量的二次函数反演模型,预测误差为3.57%。该方法相对于传统的研磨化验法,具有工作强度小、便捷、快速、高效、无污染的优点,对遥感找矿也具有一定指导意义。     

Small‐angle scattering of polychromatic X‐rays: effects of bandwidth,spectral shape and high harmonics

Polychromatic X‐ray sources can be useful for photon‐starved small‐angle X‐ray scattering given their high spectral fluxes. Their bandwidths, however, are 10–100 times larger than those using monochromators. To explore the feasibility, ideal scattering curves of homogeneous spherical particles for polychromatic X‐rays are calculated and analyzed using the Guinier approach, maximum entropy and regularization methods. Monodisperse and polydisperse systems are explored. The influence of bandwidth and asymmetric spectra shape are explored via Gaussian and half‐Gaussian spectra. Synchrotron undulator spectra represented by two undulator sources of the Advanced Photon Source are examined as an example, as regards the influence of asymmetric harmonic shape, fundamental harmonic bandwidth and high harmonics. The effects of bandwidth, spectral shape and high harmonics on particle size determination are evaluated quantitatively.     

基于可见光-近红外光谱的BIF磁性率确定方法研究

铁矿中磁性率是评价铁矿床工业价值和划分矿石工业类型的重要指标。传统的磁性率测定法存在工作量大、效率低、周期长的缺陷,成为经济、合理、高效开采铁矿资源的瓶颈问题。采用便携式地物光谱测试仪对辽宁省鞍钢集团鞍千矿业有限责任公司的BIF实验样品进行可见光-近红外光谱测试,分析了光谱特征,构建了比值指数(RI)、差值指数(DI)和归一化指数(NDI),并确定光谱指数与样品磁性率相关性最显著的敏感波段及对应的相关系数值;优选出与样品磁性率相关性最显著的比值指数(RI),构建实验样品磁性率的定量反演模型,并进行了验证。结果表明,三种光谱指数与样品磁性率敏感波段均位于935与1 050 nm,且该波段处的相关系数均达到0.9以上,其中比值指数与样品磁性率的相关性最高;基于比值指数构建的实验样品磁性率定量反演模型的预测误差为0.038,反演磁性率与实测磁性率的判定系数(R2)为0.964 5,预测结果比较理想。为确定BIF的磁性率提供了一种新方法,该方法具有工作强度小、经济、高效、便捷的优点,且对遥感找矿具有一定指导意义。