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81.
A Study of the Probe Effect on the Apparent Image of Biological Atomic Force Microscopy 总被引:1,自引:0,他引:1
Xue Mei WANG * Lei QIN Long BA Zu Hong LU The State Key Lab of Coordination Chemistry Nanjing University Nanjing National Lab of Molecular Biomolecular Electronics Southeast University Nanjing 《中国化学快报》2001,(12)
The atomic force microscopy (AFM) possesses high spatial resolution and it is compatible with liquid environments. AFM can provide possibility to study a wide range of biological problems at the molecular level and acquire topological information at nanometre resolution under physiological conditions1,2. However, a major problem for image reconstruction of biological specimens is that structures of most biological molecules are very soft and delicate, which could be easily deformed and dama… 相似文献
82.
丙烯腈 (AN)聚合通常采用自由基和阴离子聚合两种 .它们存在催化剂活性低 ,用量大等缺点 .关于丙烯腈的配位聚合研究报道则较少 .最近 ,有报道发现二价稀土化合物可以催化丙烯腈聚合 ,但催化活性较低[1 ,2 ] .本文以二茚基钇 -铝双金属配合物 (C9H7) 2 Y(μ- Et) 2 Al Et2(以下以 Y- Al代表 )为 AN聚合催化剂 ,发现它单独可以催化 AN聚合 .当外加酚钠(Ph ONa)时 ,可以大大提高聚丙烯腈 (PAN)的产率及分子量 .研究了单体浓度、催化剂浓度、温度、时间等对 AN聚合的影响 ,并对其引发机理进行了研究 .Y- Al的合成及聚合方法见文献 [3… 相似文献
83.
非线性Af—Bg型自由基交替共聚反应的固化理论 总被引:1,自引:1,他引:0
利用高分子反应统计理论,给出了非线性Af-Bg型自由基交替共聚反应的溶胶-凝胶分配方程和反应体系的凝凝胶化条件,这些结果是进一步研究与凝胶网络性能相关的网络结构参数的基础。 相似文献
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Internal bremsstrahlung (IB) and double internal bremsstrahlung (DIB) have been studied for initial p-state electron capture. In the case of IB the relative contributions of discrete and continuum intermediate states have been calculated and, in contrast to IB in initial Is state capture, it has been found that the contributions from the discrete intermediate states are dominant. Calculations for DIB have been extended and some approximations used in earlier calculations are shown to be reasonable. Predictions are made for DIB in the EC decay of SU55 Fe and 131Cs, nuclei which may be suitable for experimental investigations. 相似文献
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M. Kildir D. Logan D. Ø. Eriksen D. J. Moses Morton Kaplan E. Duek Louis C. Vaz N. N. Ajitanand John M. Alexander M. S. Zisman 《Zeitschrift für Physik A Hadrons and Nuclei》1984,317(3):291-303
The emission of4He and1H has been measured in coincidence with fission for reactions of 469-MeV56Fe+238U. By using a gas-ionization telescope in kinematic coincidence with a position-sensitive avalanche detector, the folding angle between two fission fragments was determined in order to distinguish fusion reactions from fission following smaller-momentum-transfer collisions. In both fusion fission and sequential fission reactions, the4He/1H energy spectra are relatively narrow with relatively flat angular distributions at backward angles and become broader in energy with enhanced cross-sections at forward angles. The extent of forward peaking is significantly greater for peripheral collisions than for central collisions. The light-charged-particle multiplicities are quite similar for4He and1H, being much larger for fusion fission than for sequential fission. Detailed comparisons of the spectral shapes with Monte Carlo simulations of reaction kinematics impose strong constraints on the participation of different emission sources. We find important contributions to the observed4He/1H emission both from accelerated fragments (FE) and from the composite system prior to fission (CE). For4He emission, the multiplicity of CE is much larger for fusion fission than for sequential fission, possibly as a consequence of the higher spins and shorter reaction times associated with deeply inelastic and quasi-elastic processes. For1H emission, a corresponding but somewhat smaller difference is observed for the CE multiplicities. An excess of4He/1H particles, found at forward angles in both fusion and sequential fission processes, cannot be attributed to evaporative emission from any fragments and therefore must originate in pre-thermalization emission. 相似文献
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结合Aa-Bb,Cc型缩聚反应,给出了溶胶中含内环化的溶胶-凝胶分配公式及凝胶化条件。 相似文献
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