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891.
892.
The liver, kidney and muscle samples from seven cetaceans were digested by microwave digestion, and trace elements amounts of V, Cd, Cu, Zn, As, Cr, Ni, Mn, Se, Hg and Pb were determined by inductively coupled plasma mass spectrometry (ICP-MS), and the health risk assessment for Zn, Cu, Cd, Hg, Se in the liver was conducted. The results of international lobster hepatopancreas standard (TORT-2) showed acceptable agreement with the certified values, and the relative standard deviation (RSD) of eleven kinds of trace elements were less than 3.54%, showing that the method is suitable for the determination of trace elements in cetaceans. The experimental results indicated that different tissues and organs of the dolphins had different trace elements, presenting the tissue specificity. There is a certain inter-species difference among different dolphins about the bioaccumulation ability of the trace elements. The distribution of trace elements in whales presented a certain regularity: the contents of most elements in liver, kidney were much higher than the contents of muscle tissues, Cu, Mn, Hg, Se, and Zn exhibit the higher concentrations in liver, while Cd was mainly accumulated in kidney. And according to the health risk assessment in liver, the exceeding standardrate of selenium and copper in seven kinds of whales was 100%, suggesting that these whales were suffering the contamination of trace elements. The experimental results is instructive to the study of trace elements in cetaceans, while this is the first report for the concentrations in organs of Striped dolphin, Bottlenose dolphin, Fraser's Dolphin and Risso's dolphin in China, it may provide us valuable data for the conservation of cetaceans. 相似文献
893.
Upgrade of beamline BL08B at Taiwan Light Source from a photon‐BPM to a double‐grating SGM beamline 下载免费PDF全文
Jih‐Young Yuh Shan‐Wei Lin Liang‐Jen Huang Hok‐Sum Fung Long‐Life Lee Yu‐Joung Chen Chiu‐Ping Cheng Yi‐Ying Chin Hong‐Ji Lin 《Journal of synchrotron radiation》2015,22(5):1312-1318
During the last 20 years, beamline BL08B has been upgraded step by step from a photon beam‐position monitor (BPM) to a testing beamline and a single‐grating beamline that enables experiments to record X‐ray photo‐emission spectra (XPS) and X‐ray absorption spectra (XAS) for research in solar physics, organic semiconductor materials and spinel oxides, with soft X‐ray photon energies in the range 300–1000 eV. Demands for photon energy to extend to the extreme ultraviolet region for applications in nano‐fabrication and topological thin films are increasing. The basic spherical‐grating monochromator beamline was again upgraded by adding a second grating that delivers photons of energy from 80 to 420 eV. Four end‐stations were designed for experiments with XPS, XAS, interstellar photoprocess systems (IPS) and extreme‐ultraviolet lithography (EUVL) in the scheduled beam time. The data from these experiments show a large count rate in core levels probed and excellent statistics on background normalization in the L‐edge adsorption spectrum. 相似文献
894.
Development of Two‐Channel Phosphorescent Core–Shell Nanoprobe for Ratiometric and Time‐Resolved Luminescence Imaging of Intracellular Oxygen Levels 下载免费PDF全文
895.
Characteristics of Friedel pairs and diffraction contrast tomography with non‐perpendicular rotation axis 下载免费PDF全文
Qiru Yi Gang Li Jie Zhang Sheng‐Nian Luo Duan Fan Zhenhua Gao Yanping Wang Guanfeng Gao Shiping Jiang Xiaoming Jiang 《Journal of synchrotron radiation》2015,22(4):1062-1071
The characteristics of Friedel pairs in diffraction contrast tomography (DCT) are studied in the condition that the rotation axis of the sample is not exactly perpendicular to the incident X‐ray direction. For the rotation axis approximately aligned along the vertical direction, the Friedel pairs close to the horizontal plane are insensitive to the non‐perpendicularity of the rotation axis, and can be used to refine the sample‐to‐detector distance and X‐ray energy, while the Friedel pairs close to the vertical direction are sensitive to the non‐perpendicularity of the rotation axis, and can be used to determine the rotation axis orientation. The correct matching proportion of Friedel pairs decreases with increasing non‐perpendicularity of the rotation axis. A method of data processing considering rotation axis misalignment is proposed, which significantly increases the correct matching and indexing proportions of the diffraction spots. A pure aluminium polycrystalline sample is investigated using DCT at beamline 4W1A of Beijing Synchrotron Radiation Facility. Based on the analysis of Friedel pairs, the sample‐to‐detector distance and X‐ray energy are refined to be 8.67 mm and 20.04 keV, respectively. The non‐perpendicular angle of the rotation axis is calculated to be 0.10°. With these refined geometric parameters, the matching proportion of the spatial position of diffraction spots is 90.62%. Three‐dimensional reconstruction of the sample with 13 grains is realised using the algebraic reconstruction technique. It is demonstrated that the precise correction of the orientation of the sample rotation axis is effective in DCT suffering from rotation axis misalignment, and the higher accuracy in determining the rotation axis is expected to improve the reconstruction precision of grains. 相似文献
896.
针对某钢厂转炉煤气加压站大风机电机采用工频加变频的恒压闭环运行方式,变频风机极易发生喘振的现象,为了确保大风机稳定、安全的运行,在风机喘振的预防和控制方法上进行改进。采用两台风机同步变频调速与最小极值流量法的模糊PID控制相结合的防喘振控制方法,同步变频调速控制策略有效地预防喘振的发生,最小极值流量法的模糊PID控制策略最大限度的扩大了风机的运行区间,通过MATLAB软件仿真,证明模糊PID的动态响应速度和鲁棒性较常规PID有较大的改良。控制系统通过工业网络完成现场设备和远程的通讯,使控制系统达到高水平的智能自动化。 相似文献
897.
898.
899.
报道了基于半导体激光端面抽运Nd:YAG的4F3/2–4I13/2 跃迁的弱谱线多波长激光输出. 实验对比了透明陶瓷与单晶材料的激光输出特性, 表明透明陶瓷和单晶材料荧光谱强度的略微差异, 导致了多波长输出时相同两个波长之间的激光强度比在两种材料中的差异. 基于两种耦合输出镜片, 激光阈值都在2 W左右. 在13.5 W的抽运功率下, 基于Nd:YAG透明陶瓷获得了输出功率4.05 W、强度比1 :2的1338与1356 nm双波长激光和输出功率3.65 W、强度比13 : 1的1356与1414 nm 双波长激光, 斜率效率分别达33.9% 和31.9%. 相似文献
900.