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31.
Heloiza Ferreira Alves-Prado Fabiana Carina Pavezzi Rodrigo Simões Ribeiro Leite Valéria Maia de Oliveira Lara Durães Sette Roberto DaSilva 《Applied biochemistry and biotechnology》2010,161(1-8):333-346
Hemicelluloses are polysaccharides of low molecular weight containing 100 to 200 glycosidic residues. In plants, the xylans or the hemicelluloses are situated between the lignin and the collection of cellulose fibers underneath. The xylan is the most common hemicellulosic polysaccharide in cell walls of land plants, comprising a backbone of xylose residues linked by β-1,4-glycosidic bonds. So, xylanolytic enzymes from microorganism have attracted a great deal of attention in the last decade, particularly because of their biotechnological characteristics in various industrial processes, related to food, feed, ethanol, pulp, and paper industries. A microbial screening of xylanase producer was carried out in Brazilian Cerrado area in Selviria city, Mato Grosso do Sul State, Brazil. About 50 bacterial strains and 15 fungal strains were isolated from soil sample at 35 °C. Between these isolated microorganisms, a bacterium Lysinibacillus sp. and a fungus Neosartorya spinosa as good xylanase producers were identified. Based on identification processes, Lysinibacillus sp. is a new species and the xylanase production by this bacterial genus was not reported yet. Similarly, it has not reported about xylanase production from N. spinosa. The bacterial strain P5B1 identified as Lysinibacillus sp. was cultivated on submerged fermentation using as substrate xylan, wheat bran, corn straw, corncob, and sugar cane bagasse. Corn straw and wheat bran show a good xylanase activity after 72 h of fermentation. A fungus identified as N. spinosa (strain P2D16) was cultivated on solid-state fermentation using as substrate source wheat bran, wheat bran plus sawdust, corn straw, corncob, cassava bran, and sugar cane bagasse. Wheat bran and corncobs show the better xylanase production after 72 h of fermentation. Both crude xylanases were characterized and a bacterial xylanase shows optimum pH for enzyme activity at 6.0, whereas a fungal xylanase has optimum pH at 5.0–5.5. They were stable in the pH range 5.0–10.0 and 5.5–8.5 for bacterial and fungal xylanase, respectively. The optimum temperatures were 55C and 60 °C for bacterial and fungal xylanase, respectively, and they were thermally stable up to 50 °C. 相似文献
32.
Ana Paula A. Marques Marcos Takashi S. Tanaka Elson Longo Edson R. Leite Ieda Lucia Viana Rosa 《Journal of fluorescence》2011,21(3):893-899
SrMoO4 doped with rare earth are still scarce nowadays and have attracted great attention due to their applications as scintillating
materials in electro-optical like solid-state lasers and optical fibers, for instance. In this work Sr1−xEuxMoO4 powders, where x = 0.01; 0.03 and 0.05, were synthesized by Complex Polymerization (CP) Method. The structural and optical
properties of the SrMoO4:Eu3+ were analyzed by powder X-ray diffraction patterns, Fourier Transform Infra-Red (FTIR), Raman Spectroscopy, and through Photoluminescent
Measurements (PL). Only a crystalline scheelite-type phase was obtained when the powders were heat-treated at 800 °C for 2 h,
2θ = 27.8° (100% peak). The excitation spectra of the SrMoO4:Eu3+ (λEm. = 614 nm) presented the characteristic band of the Eu3 + 5L6 transition at 394 nm and a broad band at around 288 nm ascribed to the charge-transfer from the O (2p) state to the Mo (4d)
one in the SrMoO4 matrix. The emission spectra of the SrMoO4:Eu3+ powders (λExc. = 394 and 288 nm) show the group of sharp emission bands among 523–554 nm and 578–699 nm, assigned to the 5D1→7F0,1and 2 and 5D0→7F0,1,2,3 and 4, respectively. The band related to the 5D0→7F0 transition indicates the presence of Eu3+ site without inversion center. This hypothesis is strengthened by the fact that the band referent to the 5D0→7F2 transition is the most intense in the emission spectra. 相似文献
33.
34.
Eduardo de Almeida Paulo Rogério Massoni Amauri Antonio Menegário Laudi Cunha Leite Dante Pazzanese Duarte Lanna Virgílio Franco do Nascimento Filho 《X射线光谱测定》2011,40(6):424-426
This article describes a comparison of conventional energy‐dispersive X‐ray fluorescence (EDXRF) and synchrotron radiation total‐reflection X‐ray fluorescence (SRTXRF) for Co determination in ruminal fluid from Holstein cow. This element is used as marker for animal nutrition studies. For EDXRF, 200 µl of the sample were dried on 6.35 µm Mylar film at 60 °C. The excitation was carried out using an X‐ray tube with Mo target and Zr filter operated at 30 kV/20 mA. For SRTXRF, 10 µl of the sample were pipetted on a Lucite carrier and dried at 60 °C. In both the techniques, Ga was used as internal standard and the acquisition time was 200 s. The trueness of both techniques was evaluated through the standard addition method, the recoveries obtained by SRTXRF and EDXRF were 76 and 99%, and the limits of detection, 13 and 240 µg l?1, respectively. Copyright © 2011 John Wiley & Sons, Ltd. 相似文献
35.
Maria Hermínia de Paula Leite Mello Mário Olivero Marques da Silva 《manuscripta mathematica》2000,101(2):191-198
In this paper we consider the question of the existence of a nonstable vector bundle monomorphism u:α→β over a closed, connected and smooth manifold M, when dimension of α= 3, dimension of β= dimension of M=n≡ 0(4). The singularity method provides the full obstruction to this problem and under some homological hypothesis we can compute it in terms of well known invariants. Received: 31 May 1999 相似文献
36.
Igor Leite Freire 《Journal of Mathematical Analysis and Applications》2010,367(2):716-9473
Using the scalar curvature of the product manifold S2×R and the complete group classification of nonlinear Poisson equation on (pseudo) Riemannian manifolds, we extend the previous results on symmetry analysis of homogeneous wave equation obtained by H. Azad and M.T. Mustafa [H. Azad, M.T. Mustafa, Symmetry analysis of wave equation on sphere, J. Math. Anal. Appl. 333 (2007) 1180-1188] to nonlinear Klein-Gordon equations on the two-dimensional sphere. 相似文献
37.
João R. Cardoso F. Silva Leite 《Journal of Computational and Applied Mathematics》2010,233(11):2867-2875
Two widely used methods for computing matrix exponentials and matrix logarithms are, respectively, the scaling and squaring and the inverse scaling and squaring. Both methods become effective when combined with Padé approximation. This paper deals with the computation of exponentials of skew-symmetric matrices and logarithms of orthogonal matrices. Our main goal is to improve these two methods by exploiting the special structure of skew-symmetric and orthogonal matrices. Geometric features of the matrix exponential and logarithm and extensions to the special Euclidean group of rigid motions are also addressed. 相似文献
38.
Leite Irena Andrianov Victor Zelencova-Gopejenko Diana Loza Einars Kazhoka-Lapsa Iveta Domracheva Ilona Stojak Marta Chlopicki Stefan Kalvins Ivars 《Chemistry of Heterocyclic Compounds》2021,57(12):1235-1235
Chemistry of Heterocyclic Compounds - 相似文献
39.
P.S. Pizani M.R. Joya F.M. Pontes L.P.S. Santos M. Godinho E.R. Leite E. Longo 《Journal of Non》2008,354(2-9):476-479
Intense photoluminescence in the visible region was observed at room temperature in standard soda-lime-silica glass powder, mechanically milled in a high-energy attrition mill. The emission band maximum shows an interesting dependence on the exciting wavelength, suggesting the possibility to tune the PL emission. These findings indicate that the photoluminescence may be directly related to unsatisfied chemical bonds correlated with the high surface area. The Raman scattering and ultraviolet–visible optical reflectance measurements corroborate this assertion. Transmission electron microscopy measurements indicate that samples milled more than 10 h present the formation of nanocrystallites with about 10–20 nm. 相似文献
40.
Sara Pacelli de Sousa Marcial Guilherme Carneiro Elaine A. Leite 《Journal of nanoparticle research》2017,19(10):340
Paclitaxel (PTX) is a well-known antitumor drug, widely utilized in the treatment of breast, ovarian, head, and neck tumors, among others. The low aqueous solubility (< 1.0 μg/mL; log P = 3.96) limits its use by intravenous route, and alternatives found for the marketed products are associated with high toxicity. Incorporation of PTX into lipid nanocarriers has been considered an interesting nontoxic alternative for this route, but drug loading is usually low. This study aimed to analyze the influence of the lipid composition and three different lipid nanosystems—solid lipid nanoparticles, nanostructured lipid carriers (NLCs), and nanoemulsion—in PTX encapsulation and its biological response. The three proposed systems were prepared by hot melt homogenization followed by ultrasonication. Among the blank formulations first prepared, NLC had the smallest size (74 ± 1 nm), with negative zeta potential (? 11.4 ± 0.1 mV). The incorporation of 0.10 mg/mL PTX into this NLC formulation yielded high and stable encapsulation (0.089 ± 0.003 mg/mL), also supported by polarized light microscopy and differential scanning calorimetry curves. NLC-PTX was very effective against MCF-7 (IC50 25.33 ± 3.17 nM) and MDA-MB-231 breast cancer cell lines (IC50 2.13 ± 0.21 nM), compared to free PTX (IC50 > 500 nM). In addition, no significant cytotoxicity was found against fibroblast cells. Taken together, these results demonstrated that PTX was successfully incorporated into NLC with appropriate physicochemical characteristics for intravenous administration, suggesting that the use of NLC as vehicle to incorporate PTX may be a promising strategy in the treatment of breast cancer. 相似文献