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141.
The thermal decomposition of piperidine hydrothiocyanate, piperazine hydrothiocyanate, and the dihydrothiocyanates of ethylenediamine and 1,3-diaminopropane has been studied using TG. Piperidine hydrothiocyanate decomposes in a single step while the dihydrothiocyanates follow more complicated decomposition patterns yielding H2S and half of the organic moiety first. The second step involves the loss of H2S and the remainder of the organic moiety. In each case, complex polymeric materials result. Piperazine hydrothiocyanate also decomposes in two steps, the first involving the loss of half of the piperazine and the second involving the loss of piperazine and H2S. Kinetic parameters have been determined for all these reactions. 相似文献
142.
143.
Yu. K. Voron'ko A. B. Kudryavtsev V. V. Osiko E. V. Sorokin 《Journal of Applied Spectroscopy》1991,55(4):953-957
Translated from Zhurnal Prikladnoi Spektroskopii, Vol. 55, No. 4, pp. 535–540, October, 1991. 相似文献
144.
R. J. Vanderbei 《Mathematical Programming》1989,43(1-3):31-44
The affine-scaling modification of Karmarkar's algorithm is extended to solve problems with free variables. This extended primal algorithm is used to prove two important results. First the geometrically elegant feasibility algorithm proposed by Chandru and Kochar is the same algorithm as the one obtained by appending a single column of residuals to the constraint matrix. Second the dual algorithm as first described by Adler et al., is the same as the extended primal algorithm applied to the dual. 相似文献
145.
A new geometrical method to determine the surface damage threshold for ultrashort pulses is presented. It consists in the formation of a surface damage profile by a movement of the sample across the laser beam focus. A single measurement of the maximum transversal dimension of this damage profile, which depends solely on the laser beam power, is used to calculate the local damage threshold intensity. It is also theoretically shown that the damage in the transverse dimension can be controlled under the diffraction-limited spot. 相似文献
146.
The consequences of Ge deposition on Br-terminated Si(1 0 0) were studied with scanning tunneling microscopy at ambient temperature after annealing at 650 K. One monolayer of Br was sufficient to prevent the formation of Ge huts beyond the critical thickness of 3 ML. This is possible because Br acts as a surfactant whose presence lowered the diffusivity of Ge adatoms. Hindered mobility was manifest at low coverage through the formation of short Ge chains. Further deposition resulted in the extension and connection of the Ge chains and gave rise to the buildup of incomplete layers. The deposition of 7 ML of Ge resulted in a rough surface characterized by irregularly shaped clusters. A short 800 K anneal desorbed the Br and allowed Ge atoms to reorganize into the more energetically favorable “hut” structures produced by conventional Ge overlayer growth on Si(1 0 0). 相似文献
147.
R. J. Hinde 《Few-Body Systems》2006,38(2-4):187-191
We compute the vibrational coupling between two H2 molecules from ab initio quantum chemical calculations of the H2-H2 potential carried out at the full configuration interaction level of theory using the atom-centered aug-cc-pVTZ basis set
for hydrogen. We compare the full configuration interaction results with those obtained using two variants of coupled cluster
theory and find that a fully iterative treatment of connected triples may be required to estimate the H2-H2 vibrational coupling accurately using coupled cluster theory. 相似文献
148.
In this paper we study root system generalizations of the quantum Bose-gas on the circle with pair-wise delta-function interactions.
The underlying symmetry structures are shown to be governed by the associated graded algebra of Cherednik's (suitably filtered)
degenerate double affine Hecke algebra, acting by Dunkl-type differential-reflection operators. We use Gutkin's generalization
of the equivalence between the impenetrable Bose-gas and the free Fermi-gas to derive the Bethe ansatz equations and the Bethe
ansatz eigenfunctions. 相似文献
149.
We study oscillation in a gyrotron with allowance for reflections from an output horn. Regions with different system behaviors,
such as stationary oscillation, self-modulation, and complex-dynamics regimes are found in the parameter plane. The scenarios
of appearance of chaotic oscillations are considered. It is shown that they can emerge via either a sequence of period-doubling
bifurcations or destruction of quasiperiodic motion. For chaotic attractors, Lyapunov exponents are calculated and their dimensions
are estimated on the basis of the Kaplan-Yorke formula. The dimension values turn out to be anomalously large, which is stipulated
by the presence of a large number of high-Q eigenmodes in the gyrotron cavity due to operation near the cutoff frequency of
an electrodynamic system.
__________
Translated from Izvestiya Vysshikh Uchebnykh Zavedenii, Radiofizika, Vol. 49, No. 10, pp. 887–899, October 2006. 相似文献
150.
In this paper, we explore the interplay of four different conjectures on certain zero-sum problems in Zp Zp. This study of the inter-relations between these conjectures leads to the conclusion that determining the structure of minimal zero sequences (see below for the precise definition) is crucial. Also, we study the analogous situation in Zn. 相似文献