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491.
Journal of Thermal Analysis and Calorimetry - Knitwear fabrics are now becoming an ultimate choice of clothing consumers because of their easiness in wearing, simplicity, lasting appearance and...  相似文献   
492.
In this paper, we report a strong enhanced emission from laser produced plasma in air from iron oxide nano-material in comparison with the corresponding bulk samples. The enhancement strength differs with different Nd:YAG laser harmonics wavelengths. The analysis showed that such enhancement increased exponentially with the plasma evolution time, while it declines as the laser fluence increased. Experimental data analysis clearly showed that the observed enhancement is mainly associated with the change in the plasma electron density. We claim that this strong enhanced optical emission from laser produced plasma is due to the surface plasmon resonant excitation preferably on nano-oxide materials. Such experimental findings could improve the laser-induced breakdown spectroscopy sensitivity down to extremely low concentrations.  相似文献   
493.
A five-component crystal of lanthanum–gallium silicate group La3Ga5.3Ta0.5Al0.2O14 (LGTA) was grown by the Czochralski method. The LGTA crystal possesses unique thermal properties and substitution of Al for Ga in the unit cell leads to a substantial increase of electrical resistance at high temperatures. The unit cell parameters of LGTA were determined by powder diffraction. X-ray topography was used to study the crystal structure perfection: the growth banding normal to the growth axis were visualized. The independent piezoelectric constants d 11 and d 14 were measured by X-ray diffraction in the Bragg and Laue geometries. Excitation and propagation of surface acoustic waves were studied by the double-crystal X-ray diffraction at the BESSY II synchrotron radiation source. The analysis of the diffraction spectra of acoustically modulated crystals permitted the determination of the velocity of acoustic wave propagation and the power flow angles in different acoustic cuts of the LGTA crystal.  相似文献   
494.
This paper presents a new enhanced design of fibre Bragg grating for flattening the gain profile of an erbium-doped fibre amplifier in transmission configuration. This grating has modulation of refractive index change and constant chirp rate, wherein both profiles of the parameters are properly apodized. The design utilizes an alternative approach to the renowned inverse scattering method, yet produces a similar spectral response quality and conceptually simpler. Moreover, it offers precise control over all parameters of the grating structure. It is shown that the design approach could produce gain-flattening filters of satisfactory quality through simulations using the accurate transfer matrix method.  相似文献   
495.
A group G is said to be capable if it is isomorphic to the central factor group H/Z(H) for some group H. Let G be a nonabelian group of order p 2 q for distinct primes p and q. In this paper, we compute the nonabelian tensor square of the group G. It is also shown that G is capable if and only if either Z(G) = 1 or p < q and Gab=\mathbbZp×\mathbbZp{G^{\rm ab}=\mathbb{Z}_{p}\times\mathbb{Z}_{p}} .  相似文献   
496.
We have developed a microfabricated biochip that enumerates CD4+ T lymphocytes from leukocyte populations obtained from human blood samples using electrical impedance sensing and immunoaffinity chromatography. T cell counts are found by obtaining the difference between the number of leukocytes before and after depleting CD4+ T cells with immobilized antibodies in a capture chamber. This differential counting technique has been validated to analyze physiological concentrations of leukocytes with an accuracy of ~9 cells per μL by passivating the capture chamber with bovine serum albumin. In addition, the counter provided T cell counts which correlated closely with an optical control (R(2) = 0.997) for CD4 cell concentrations ranging from approximately 100 to 700 cells per μL. We believe that this approach can be a promising method for bringing quantitative HIV/AIDS diagnostics to resource-poor regions in the world.  相似文献   
497.
We designed an artificial one-dimensional DNA nanotrack that contains two T-motifs. It can be fabricated in a free solution and with a mica-assisted growth process. Also, we introduced a dry and wet method for the restoration of DNA nanostructures in order for them to be used in multiple applications.  相似文献   
498.
Composites of ZrO2 and CdO nanocrystals with conducting polyaniline/p-nitroaniline blended in different ratios have been prepared and investigated by UV-vis spectrophotometer, luminescence spectrophotometer and structural characterization of copolymer was studied by FTIR method. A decrease in nanocrystals photoluminescence (PL) has been observed with the increase in the concentration of PANI/PNA in the composites. A phenomenon of quenching is observed in the nanocrystals by luminescence.  相似文献   
499.
The reaction of substituted benzyl-, aroylmethyl-, or 1-phenetylisatins with hexaethyltriaminophosphine has been shown to lead to the formation of a library of 3,3′-biindolinylidene-2,2′-diones with functionalized benzyl-, aroylmethyl-, and 1-phenetyl fragments at the nitrogen atom.  相似文献   
500.
Asymmetric flow field flow fractionation (AsFlFFF) was combined with pyrolysis-gas chromatography mass spectrometry for a sized based fractionation and a detailed compositional study of the triglycerides and cholesterol associated with the various lipoprotein subclasses present in human serum. Serum samples were injected in the AsFlFFF instrument and fractionated with a time-delayed exponential decay cross flow program. The fractions collected after AsFlFFF elution were injected into a programmable temperature vaporizer (PTV) GC-injector, containing a fritted liner. A temperature and split-flow program for the PTV injector was optimized for the thermally assisted hydrolysis and methylation of the compounds of interest. The resulting fatty acid and cholesterol methyl esters were separated by GC and characteristic fragment ions were detected by MS. The system was optimized and calibrated with triglyceride and cholesterol standards for quantitative analysis. The possible interference by phospholipids with the quantitative results was investigated and found to be of minor importance.The concentrations and lipoprotein profiles of triglycerides and cholesterol were determined in a pooled serum sample of healthy volunteers and a serum sample of a sepsis patient. The results obtained with the GC–MS approach were compared with those of a previously developed method based on AsFlFFF with a dual enzymatic reaction detection system. A good agreement of the profiles was found, for cholesterol as well as for the triglycerides, even when the GC–MS method quantifies the fatty acids while with the enzymatic reaction method the glycerol concentrations are determined. Total cholesterol and triglyceride concentration values for the serum samples showed good agreement with the results of the standard enzymatic method as used in practice in the university hospital.  相似文献   
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