FAAS法测定硫酸中的铜、铁和锌

采用火焰原子吸收光谱法测定硫酸中铜、铁和锌,确定了最佳仪器工作条件和样品处理方法.在选择好的实验条件下,测定铜的特征浓度为0.005μg/mL/1%;铁的特征浓度为0.014μg/mL/1%吸收;锌的特征浓度为0.002μg/mL/1%吸收.回收率分别为铜97.7%-98.2%,铁98.2%-99.4%,锌96.8%-98.7%.     

Effect of bias condition on heavy ion radiation in bipolar junction transistors

The characteristic degradations in a silicon NPN bipolar junction transistor(BJT) of 3DG142 type are examined under irradiation with 40-MeV chlorine(Cl) ions under forward,grounded,and reverse bias conditions,respectively.Different electrical parameters are in-situ measured during the exposure under each bias condition.From the experimental data,a larger variation of base current(I B) is observed after irradiation at a given value of base-emitter voltage(V BE),while the collector current is slightly affected by irradiation at a given V BE.The gain degradation is affected mostly by the behaviour of the base current.From the experimental data,the variation of current gain in the case of forward bias is much smaller than that in the other conditions.Moreover,for 3DG142 BJT,the current gain degradation in the case of reverse bias is more severe than that in the grounded case at low fluence,while at high fluence,the gain degradation in the reverse bias case becomes smaller than that in the grounded case.     

一种高压光学样品池系统的设计与实验研究

设计和研制了一种用于溶液样品光学特性原位检测的高压光学样品池成套系统,组件包括手动泵、增压器和高压样品池。其中样品池开有3处光学窗口,以水为传压介质,设计的最高使用压力为600MPa。当用JGS1石英作窗口时,密封和保压效果良好;由于受到石英材质强度的限制,使用压力应控制在300MPa以下。为检验该系统在高压原位检测方面应用的可行性,进行了色氨酸高压荧光光谱的采集。     

OPTICAL PROPERTIES OF δ-DOPED GaAs AND GaAs/Al0.1Ga0.9As SUPERLATTICES

Radiative transition in δ-doped GaAs superlattices with and without Al_0.1Ga_0.9As barriers is investigated by using photoluminescence at low temperatures. The experimental results show that the transition mechanism of δ-doped superlattices is very different from that of ordinary superlattices. Emission intensity of the transition from the electron first excited state to hole states is obviously stronger than that from the electron ground state to hole states due to larger overlap integral between wavefunctions of electrons in the first excited state and hole states. Based on the effective mass theory we have calculated the self-consistent potentials, optical transition matrix elements and photoluminescence spectra for two different samples. By using this model we can explain the main optical characteristics measured. Moreover, after taking into account the bandgap renormalization energy, good agreement between experiment and theory is obtained.     

核核碰撞中不稳定轻核的方位角各向异性发射

利用符合的粒子粒子关联测量，研究了２５ＭｅＶ／ｕ^４０Ａｒ＋^１９７Ａｕ反应中不稳定轻核的在平面发射和出平面发射．对于中速的不稳定轻核，观测到在平面发射几率增大，这表明该反应系统中存在旋转效应．该现象随碰撞参数增大更为强烈，而随着不稳定核激发态能量的升高稍有变弱     

压力循环流化床中的传热研究

本文从理论与试验上研究压力循环流化床中床－壁面传热系数的变化规律。对常压循环流化床中的传热模型进行修正，发展了压力循环流化床中的传热模型。试验测试了床内传热系数随床内固体颗粒浓度、颗粒径和运行风速的变化规律。提出计算床－壁面传热系数的无量纲经验公式。     

Investigation of Elliptical Gaussian Beam in Optical Disk System

1.IntroductionLaserdiodehasbeenx`idelyusedinfibrc-opticcommunicat:onandopticaldisk$yctems.LaserbeamIsradiationangle(fullangu1aratha1f-maximumintensitypoint)ismeasuredbothparllelandPerpendiculartothcjunctionp1anclgenera1ly.o//=6,~1o",oJ-=2o"~5O':Inerasableopticaldisksystemsasmagneto-optica1disksystems,thelaserbcamiscollimatedandshapedtobecircularsymInetricbeaminordcrtoaquireahighintensityandhighqualityscanningbeamiPot,butitsoptica1systemiscomplicatedandeasyaddingassocialaberration.usingaellip…     

折反式微光夜视物镜的光学设计

介绍一种长焦距、大相对孔径微光夜视物镜的光学设计。设计参数为焦距100 mm,相对孔径1/1.4,视场10。为增大视距,减小物镜尺寸和质量,并且满足在宽光谱范围消色差的要求,选择均为球面的折反式物镜结构,在相同焦距和相对孔径的条件下折反式系统比折射系统尺寸更小,质量更轻。在设计过程中引入曼金反射镜,增加设计自由度。经优化设计达到较好的成像质量,空间频率在50 lp/mm时,轴上传递函数大于0.4,轴外传递函数大于0.2,与像增强器极限分辨率相匹配,全视场畸变小于2 %,物镜总长达到67 mm。     

复杂背景下红外弱小目标检测算法研究

复杂背景下低信噪比弱小目标的检测是红外预警系统中的重点和难点。为解决红外图像中杂波干扰多、目标信噪比低等问题,提出一种非线性空间滤波的目标检测方法。该算法在传统线性空间滤波算法的基础上,通过对预测点周围4个象限的背景灰度值进行计算,并动态地调节阈值,以达到突出小目标的目的。试验结果表明:当背景包含较多复杂因素时,采用非线性空间滤波的检测方法可有效地抑制杂波,实现弱小目标的提取,与线性滤波算法结果相比较,虚警数降低了3/4,且易于工程实现。     

微波消解-电感耦合等离子体-质谱法测定大米中的铅、镉、汞和砷

应用微波消解-电感耦合等离子体-质谱法(ICP-MS)一次进样同时测定大米中的铅、镉、汞、砷含量.采用8mL硝酸+2mL过氧化氢的微波消解体系,消解后无需赶酸,定容后直接用ICP-MS测定.实验发现,运用该方法干扰少,速度快,多元素同时分析,重现性好,准确度高.该方法的回收率分别为:Pb:100.9％、Cd:90.1％、Hg:86.1％、As:92.8％.Pb、Cd、Hg、As方法检出限均为0.001ng/mL.