Field—ion microscopy observation of single—walled carbon nanotubes

Field-ion microscopy(FIM),a tool for surface analysis with atomic resolution,has been employed to observe the end structure of single-walled carbon nanotubes(SWCNTs).FIM images revealed the existence of open SWCNT ends,Amorphous carbon atoms were also observed to occur around SWCNTs and traditional field evaporation failed to remove them.Heat treatment was found to be efficacious in altering the end structures of SWCNT bundles.Carbon and oxygen atoms released from heated tungsten filament are believed to be responsible for the decoration imposed on the SWCNT ends.     

基于Goose LDW-PSO的管壳式换热器优化设计

管壳式换热器在工业中的应用越来越广泛,对于设计者和使用者来说使其费用最小化是一个很重要的目标。本文以最小化管壳式换热器的总费用为优化目标,提出了运用基于雁群启示的惯性权重线性下降粒子群优化算法(Goose LDW-PSO)对其进行优化设计。为了验证这种方法的有效性,用Goose LDW-PSO对管壳式换热器进行了优化设计,并与原始设计结果进行了比较。比较结果表明,虽然管子数目增加,但是换热器的总费用比传统方法少了很多。     

超声波法提取迎春花总黄酮含量的工艺研究

研究了超声波法对迎春花中总黄酮的提取条件。其最优提取条件为:料液比1∶40,超声波温度20℃,作用时间20min。在此条件下,用NaNO2-Al(NO3)3-NaOH显色法测定的总黄酮为18.22%,RSD=1.48%(n=5)。     

The MAEAM Model and Anharmonic Theory for the Bulk Modulus of A1 Metal

The modified analytic embedded atom method （MAEAM） model and the anharmonic theory are used to study the bulk modulus of fcc A1 metal. The result shows that the bulk modulus can be described by a quadratic function of temperature. The result is in good agreement with the experimental data and theoretical results calculated by the first principle calculation etc. This outcome indicates that the temperature dependence of the bulk modulus for f cc A1 metal can be academically studied with the MAEAM model combining with the anharmonic theory.     

Crossover from a continuum study of chiral susceptibility

We derive a model-independent integral formula for chiral susceptibility and attempt to present a continuum model study of it within the framework of Dyson–Schwinger equations. An appropriate regularization is implemented to remove the temperature-independent quadratic divergence inherent in this quantity. While it demonstrates a second-order phase transition characteristic in the chiral limit, the result obtained supports a crossover at physical current quark masses, which is in good agreement with recent lattice studies.     

小型轻便式流速仪检定系统设计

为满足FP系列流速仪的计量检定需求,提出了一种小型便携式流速仪检定系统的设计方案。根据匀速运动时间等约束条件确定了环形水槽的几何参数。采用FPGA和上位机作为数据处理和控制核心,实现了对伺服电机转速的精确控制。设计了光电编码器和无线摄像机与上位机之间的通信方式,实现了检定装置标准流速值和被检仪器示值的数据读取。对测试数据的处理方法和测控软件的结构框架进行了分析。同时,对实验装置的测量误差进行了分析。结果表明,标准流速值的扩展不确定度为1.28×10-3m/s,检定装置符合量值传递要求,可作为FP系列流速仪计量检定的标准装置。     

溶剂浮选-紫外分光光度法分析/富集废水中草甘膦铵盐的研究

基于在酸性条件下,草甘膦铵盐与Fe^3＋可生成稳定配合物,同时以孔雀石绿（MG）作为捕捉剂可提高该配合物在异辛醇等有机溶剂中的溶解度,据此建立了溶剂浮选-紫外分光光度法分析/富集草甘膦生产废水中的草甘膦铵盐的方法。同时考察了捕捉剂和螯合剂及其用量、pH、浮选时间、有机溶剂等因素对浮选效果的影响,并将溶剂浮选法与泡沫浮选法以及溶剂萃取法进行了比较,结果表明溶剂浮选法分离/富集效果最好,草甘膦铵盐回收率达91.2%。     

Nanoscale formation mechanism of conducting filaments in NiO thin films

We have studied the nanoscale electrical properties of NiO thin films by using conducting atomic force microscopy (CAFM) to understand the mechanism of resistance change of the NiO thin films as we changed the applied voltage. We observed that inhomogeneous conducting filaments were generated by external voltage bias; in addition, some of the inhomogeneous conducting filaments were durable while some of them were not, and they disappeared. We deduced that the resistance change of the NiO thin films was related to inhomogeneous filamentary conducting paths generated by both Ni ions in thermodynamically unstable NiO and the existence of conducting filament segments generated by high voltage bias.     

利用近红外光谱检测多层组织血氧饱和度的研究

利用近红外光谱无创检测生物组织血氧饱和状态,是一种极富研究和应用前景的检测技术,在临床检测中被广泛应用.但常规临床检测应用于指端仅反映局部血氧饱和度信息,在使用中具有局限性,信号的可信度也存在质疑.该文提出了一种采用反射式脉搏血氧饱和度检测技术检测生物多层组织氧合状况的新方法,该方法通过调节入射光强以适应解剖学中生物组织多层结构的检测.应用该方法针对手指结构的实验结果表明,随着入射光强的改变,反映血氧饱和状态的光电脉搏波信号有显著变化.结合手指解剖学分析表明,光电脉搏波信号的变化与手指的多层面组织结构相对应,反映不同层面血氧饱和状态.这一特点表明,通过此法可以针对生物组织的多层结构进行测量.     

Spectroscopic Properties and Electronic Structure of Bis(L—Histidine)Copper(II) Dinitrate Dihydrate

Electronic absorption spectrum, photoacoustic absorption spectrum and ESR spectrum of bis(L-histidine)copper(II) dinitrate dihydrate crystal were recorded. The experimental results are discussed quantitatively with ligand field theory (LFT) and the radial wave function of non-free copper(II). Our calculations coincides well with the experimental results, and in particular, provides significant correlations between the spectra and coordination structures. The ESR spectrum gives some information about the restudy of classification for the ESR spectra of bis(amino acidato)copper(II) complexs. Additionally, the differences between crystal and frozen solution spectra due to the variance of PH are also reported for the title compound.