基于Labwindows/CVI的无人机畸变测试系统设计

针对现代无人机电网电压畸变参数检测的需求,设计了一种基于Labwindows/CVI的无人机专用畸变测试系统;根据实际装备的需求,设计过程中注重便携的特点和模块化设计思想,完成了系统的硬件和软件设计;为了提高设计的准确性,该系统还采用硬件滤波和数字滤波两种滤波方式进行滤波;实际应用表明,该系统能够准确测出无人机电网的畸变参数与畸变频谱,且各项测试指标均达到了设计要求,能够满足无人机电网交直流畸变测试的需要。     

ANALYTICAL SOLUTION FOR ROTATIONAL RUBBING PLATE UNDER THERMAL SHOCK

提出了热冲击和碰摩故障共同作用下的旋转悬臂板系统动力特性解析解法. 基于变分原理,推导出考虑碰摩力沿宽度方向差异性的薄板系统运动微分方程,将该方程的解分解为热冲击悬臂板准静态解和碰摩薄板热冲击动力解. 通过计算旋转悬臂板的模态特性和温度分布函数,获得了碰摩叶片旋转悬臂板模型的热冲击振动解析解,讨论分析得出热冲击和碰摩故障对薄板振动的影响规律. 研究表明:碰摩振动表现为复杂的多频率耦合振动,高频振动较为显著;热冲击振动表现为简单的低频振动形式,强烈的热冲击导致碰摩薄板趋于低频振动. 碰摩引起的振动形式较热冲击故障更加复杂,更容易引起叶片的破坏. 增大的摩擦系数加剧了碰摩引起的振动,利用减小表面粗糙程度等方法降低摩擦系数,可以达到减小碰摩破坏程度的目的.     

A remarkable anion effect on palladium nanoparticle formation and stabilization in hydroxyl-functionalized ionic liquids

Pd nanoparticles (NPs) with a small size and narrow size distribution were prepared from the decomposition of Pd(OAc)(2) in a series of hydroxyl-functionalized ionic liquids (ILs) comprising the 1-(2'-hydroxylethyl)-3-methylimidazolium cation and various anions, viz. [C(2)OHmim][OTf] (2.4 ± 0.5 nm), [C(2)OHmim][TFA] (2.3 ± 0.4 nm), [C(2)OHmim][BF(4)] (3.3 ± 0.6 nm), [C(2)OHmim][PF(6)] (3.1 ± 0.7 nm) and [C(2)OHmim][Tf(2)N] (4.0 ± 0.6 nm). Compared with Pd NPs isolated from the non-functionalized IL, [C(4)mim][Tf(2)N] (6.2 ± 1.1 nm), it would appear that the hydroxyl group accelerates the formation of the NPs, and also helps to protect the NPs from oxidation once formed. Based on the amount of Pd(OAc)(2) that remains after NP synthesis (under the given conditions) the ease of formation of the Pd NPs in the [C(2)OHmim](+)-based ILs follows the trend [Tf(2)N](-), [PF(6)](-) > [BF(4)](-) > [OTf](-) > [TFA](-). Also, the ability of the [C(2)OHmim](+)-based ILs to prevent the Pd NPs from undergoing oxidation follows the trend [Tf(2)N](-) > [PF(6)](-) > [TFA](-) > [OTf](-) > [BF(4)](-). DFT calculations were employed to rationalize the interactions between Pd NPs and the [C(2)OHmim](+) cation and the various anions.     

In situ time-resolved DXAFS study of Rh nanoparticle formation mechanism in ethylene glycol at elevated temperature

A combination of in situ time-resolved DXAFS and ICP-MS techniques reveals that the formation process of Rh nanoparticles (NPs) from rhodium trichloride trihydrate (RhCl(3)·3H(2)O) in ethylene glycol with polyvinylpyrrolidone (PVP) at elevated temperature is a first-order reaction, which indicates that uniform size Rh NPs appear consecutively and these Rh NPs do not aggregate with each other.     

Czerny-Turner正交型光栅单色仪的波长校准

研究了Czerny-Turner正交型光栅单色仪的波长校准技术。结合单色仪的结构参数和特点,提出以符合光栅方程的正弦曲线作为仪器出射波长的校准方程,基于最小二乘法原理给出校准方程的拟合残差表达式,由于校准方程的非线性,应用二维Nelder-Mead单纯形法求解拟合残差的待定系数,建立了波长与光栅转角的精确表达式,并通过实验验证了该算法的准确性。结果表明,经过校准的单色仪波长定位精度小于0.1nm,比设计要求提高一个数量级。该方法在Czerny-Turner正交型光栅单色仪的波长校准过程中,应用简单,容易实现,只需稍加修改步进电机的控制程序,即可完成对仪器出射波长的快速实时校准,实用性强。     

Multiple factor hierarchical clustering algorithm for?large scale web page and search engine clickstream data

The developments in World Wide Web and the advances in digital data collection and storage technologies during the last two decades allow companies and organizations to store and share huge amounts of electronic documents. It is hard and inefficient to manually organize, analyze and present these documents. Search engine helps users to find relevant information by present a list of web pages in response to queries. How to assist users to find the most relevant web pages from vast text collections efficiently is a big challenge. The purpose of this study is to propose a hierarchical clustering method that combines multiple factors to identify clusters of web pages that can satisfy users?? information needs. The clusters are primarily envisioned to be used for search and navigation and potentially for some form of visualization as well. An experiment on Clickstream data from a processional search engine was conducted to examine the results shown that the clustering method is effective and efficient, in terms of both objective and subjective measures.     

Semilocal Convergence of a Class of Modified Super-Halley Methods in Banach Spaces

In this paper, we consider the semilocal convergence of a class of modified super-Halley methods for solving nonlinear equations in Banach spaces. The semilocal convergence of this class of methods is established by using recurrence relations. We construct a system of recurrence relations for the methods, and based on it, we prove an existence–uniqueness theorem that shows the R-order of the methods.     

Controllable transport of water through nanochannel by rachet-like mechanism

By using molecular dynamics simulation, we have investigated systematically the feasibility of continuous unidirectional water flux across a deformed single-walled carbon nanotube (SWNT) driven by an oscillating charge outside without osmotic pressure or hydrostatic drop. Simulation results indicate that the flux is dependent sensitively on the oscillating frequency of the charge, the distance of the charge from the SWNT, and the asymmetry of the water-SWNT system. A resonance-like phenomenon is found that the water flux is enhanced significantly when the period of the oscillation is close to twice the average hopping time of water molecules inside the SWNT. These findings are helpful in developing a novel design of efficient functional nanofluidic devices.     

Synthesis,Characterization, DNA‐binding Properties,and ­Antioxidant Activity of a Copper(II) Complex with 1, 3‐Bis­(1‐allaylbenzimidazol‐2‐yl)‐2‐oxopropane

A new complex of copper(II) picrate (pic) with 1, 3‐bis(1‐allaylbenzimidazol‐2‐yl)‐2‐oxopropane (aobb), with the composition [Cu(aobb)₂](pic)₂, was synthesized and characterized. The crystal structure of the copper(II) complex revealed that the coordination environment around the central copper(II) atom is a distorted octahedral arrangement. Electronic absorption spectroscopy, ethidium bromide displacement experiments and viscosity measurements indicate that the ligand and the Cu^II complex can strongly bind to calf thymus DNA, presumably by an intercalation mechanism. Furthermore, the antioxidant activity of the Cu^II complex was determined by superoxide and hydroxyl radical scavenging method in vitro, which indicate that the Cu^II complex has the activity to suppress OH ^· and O₂ ^{· –}.     

Hybrid theoretical,experimental and numerical study of vibration and buckling of composite shells with scatter in elastic moduli

Hybrid theoretical, experimental and numerical method is proposed for free vibration and buckling of composite shell with unavoidable scatter in elastic moduli. Based on the Goggin’s measurement techniques, the elastic moduli for material T300-QY8911 are measured, and a set of experimental points are obtained. The measurements of elastic moduli are quantified by either (1) the smallest ellipsoid and (2) the smallest four-dimensional uncertainty hyper-rectangle. Then uncertainty propagation in vibration and buckling problems of composite shell by ellipsoidal analysis and interval analysis are, respectively, studied from the theoretical standpoint. Comparison between these analyses is performed numerically.