The asymptotics of solutions to elliptic equations with nonlinear boundary conditions

Asymptotics of solutions to elliptic equations with nonlinear boundary conditions are studied.     

气相色谱法测定海洋沉积物中十氯酮残留

研究了提取溶剂效率、毛细管柱极性、净化条件及共溶出干扰物等因素对十氯酮测定的影响;对比了加速溶剂提取及超声波提取方式,考察了DB-17、DB-1701与DB-5毛细管柱分离度,及不同比例甲醇/正己烷混合溶液作为定容溶液的分析结果。建立了加速溶剂萃取,H2SO4净化分离,DB-5毛细管柱电子捕获检测器(ECD)-气相色谱法(GC)测定海洋沉积物介质中有机氯农药类持久性有机污染物十氯酮残留分析方法。将5 g沉积物干样与3 g活化铜粉及3 g无水Na2SO4混匀后,采用二氯甲烷-丙酮(1∶1,V/V)进行加速溶剂萃取;萃取液浓缩后,用H2SO4净化,以1%甲醇-正己烷混合溶液定容后,采用DB-5非极性毛细管柱,及配备电子捕获检测器气相色谱测定十氯酮含量。本方法采用外标法进行定量分析,在0.005～0.1 mg/L浓度范围内,线性相关系数为0.9989;加标回收率为75%～98%;相对标准偏差为3.7%～9.6%(n=6);检出限为0.12 ng/g。     

氩氧流量比对CeOx-SnOx膜微观结构及光学性能的影响

采用磁控反应共溅射的方法,以金属Ce和Sn为金属源,成功地制备出CeOx-SnOx薄膜.利用扫描电子显微镜(SEM)、X射线衍射(XRD)、透射电子显微镜(TEM)和X射线光电子能谱(XPS)等测试手段对薄膜的结构、表面形貌及成分进行了分析和表征.结果表明薄膜以岛状模式生长,随氩氧比降低,结晶性增强,出现CeO2和SnO相.此外,利用紫外-可见分光光度计对薄膜的光学性能进行了研究,测试结果表明薄膜对紫外光有极强的吸收作用.当氩氧流量比为3∶1时,紫外光平均透过率仅为5.80;,而可见光平均透过率为81.48;.     

Mathematical Analysis of Technological Parameters for Producing Superfine Prepregs by Flattening Carbon Fibers

Mechanics of Composite Materials - A mathematical model and a technique for evaluating the technological process parameters to obtain superthin prepregs by flattening carbon tows impregnated with...     

Microgravimetric study of electrochemical properties of PEDOT/WO3 composite films in diluted sulfuric acid

Journal of Solid State Electrochemistry - Poly-3,4-ethylenedioxythiophene composite films with tungsten oxide (PEDOT/WO3) were obtained by potentiodynamic deposition of tungsten oxide from acidic...     

光学实验教学法的改进

对光学实验教学法做了一些改进：1)将单个光学实验划分为相对独立的单元，每个单元用不同的实验方法研究一个待测的物理量或观察分析一个物理现象；2)加强预习报告要求；3)以调整仪器为主的操作考核。     

In honor of the sixtieth birthday of M. I. Yadrenko,corresponding member of the Academy of Sciences of Ukraine

In honor of the sixtieth birthday of M. I. Yadrenko, corresponding member of the Academy of Sciences of Ukraine     

Absence of Critical Points for a Class of Quantum Hierarchical Models

Hierarchical models of quantum anharmonic oscillators with a polynomial anharmonicity and interaction decaying as (distance)^-1-λ are considered. For a class of such models (including ϕ⁴-type anharmonicity ones), it is shown that the critical fluctuations of the position operator are absent, for all λ > 0 and all temperatures, provided the oscillators mass in less than some threshold value depending on the anharmonicity parameters. This result may be interpreted as a rigorous mathematical justification of physical arguments showing that quantum fluctuations can damp phase transitions. Received: 12 April 1996 / Accepted: 25 October 1996