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Brian Brookman Ewa Bulska Owen Butler Michael Koch Tracey Noblett Kees van Putten Piotr Robouch 《Accreditation and quality assurance》2012,17(4):445-451
A summary of the working group (WG) discussions on proficiency testing (PT) and external quality assessment (EQA) held at the EURACHEM Workshop, Istanbul, 3?C6 October 2011, is provided. The six WGs covered a range of issues concerned with current practice and future directions; implementing the requirements of ISO/IEC 17043 by PT/EQA providers (WG1); accrediting PT/EQA providers to ISO/IEC 17043 (WG2); pre- and post-analytical aspects in PT/EQA (WG3); evaluating participant performance in qualitative PT/EQA schemes (WG4); establishing PT/EQA schemes in developing countries (WG5); and establishing acceptability criteria in microbiology PT/EQA schemes (WG6). Delegates with different backgrounds were on each WG in order to capture a range of views and experience from a number of different sectors. Working group representatives included PT/EQA providers, participants in PT/EQA schemes and end-users of PT results such as accreditation bodies and regulatory authorities, from countries around the world. 相似文献
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C.E. Kees I. Akkerman M.W. Farthing Y. Bazilevs 《Journal of computational physics》2011,230(12):4536-4558
This paper presents a formulation for free-surface computations capable of handling complex phenomena, such as wave breaking, without excessive mass loss or smearing of the interface. The formulation is suitable for discretizations using finite elements of any topology and order, or other approaches such as isogeometric and finite volume methods. Furthermore, the approach builds on standard level set tools and can therefore be used to augment existing implementations of level set methods with discrete conservation properties. Implementations of the method are tested on several difficult two- and three-dimensional problems, including two incompressible air/water flow problems with available experimental results. Linear and quadratic approximations on unstructured tetrahedral and trilinear approximations on hexahedral meshes were tested. Global conservation and agreement with experiments as well as computations by other researchers are obtained. 相似文献
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Onno de Vegt Herman Vromans Fried Faassen Kees van der Voort Maarschalk 《Particle & Particle Systems Characterization》2005,22(2):133-140
The particle size distribution of pharmaceutically active materials and other fine chemicals determines the performance of the final product to a large extent. Often milling of these particles is necessary. It is not possible to determine the milling conditions solely on the basis of the particle size distribution of the starting material, because the (mechanical) properties of the material also determine the desired milling conditions. It is often not possible to optimize milling conditions experimentally because the amount of material available is frequently highly limited. A theoretical approach towards predicting the best milling conditions is needed. The purpose of this study was to develop a method to predict the desired milling conditions given a specific (organic) solid material. The selection function and the breakage distribution function are usually the starting points in modeling the milling process. The selection function is the parameter that includes the material and mill properties. Dimensional analysis made it possible to correlate the selection function with material properties. A set of theories available in the literature enable prediction of the material properties. For different compounds (lactose, paracetamol, a steroidal compound, and two heterocyclic compounds) the selection functions were calculated. The calculations predict differences: lactose reduces slowly in size, while one of the heterocyclic compounds shows the most intense fracture. 相似文献
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In this paper we characterize a value, called a marginalistic value, for monotonic set games, which can be considered to be the analog of the Shapley value for TU-games. For this characterization we use a modification of the strong monotonicity axiom of Young, but the proof is rather different from his. 相似文献
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Daria A. Chernova Andrey KH. Vorobiev 《Journal of Polymer Science.Polymer Physics》2009,47(1):107-120
ESR spectra of three spin probes with different molecular volumes: 2,2,6,6‐tetramethyl‐4‐oxopiperidine‐1‐oxyl, di‐p‐anisylnitroxide, and nitroxide derivative of fullerene in glassy polystyrene, polyvinyl trimethylsilane, and Teflon AF‐2400 were calculated numerically within the model of quasi‐libration motions. Temperature ranges, where the model is capable to reproduce spectra within experimental errors, were defined. It was found that simulation of X‐band ESR spectra allows to determine quasi‐libration amplitudes around molecular axes X and Y with accuracy ~ 3° and around Z axis with accuracy ~ 15–20°. A shape of distribution of quasi‐libration amplitudes was also determined qualitatively by ESR spectra simulations. It was established that the average amplitude of quasi‐libration motion depends on the free volume of each polymer and geometrical molecular volume of a spin probe. Quasi‐libration amplitudes increase as the temperature increases, and reach the value of 40 degrees. We found that upon further temperature increase, quasi‐libration model becomes inapplicable for quantitative numerical spectra simulation. © 2008 Wiley Periodicals, Inc. J Polym Sci Part B: Polym Phys 47: 107–120, 2009 相似文献