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11.
Noriko SUTO Makoto HARADA Jun IZUTSU Toshiyasu NAGAO 《Proceedings of the Japan Academy. Series B, Physical and biological sciences》2006,82(5):175-180
In order to accurately estimate the geomagnetic transfer functions in the area of the volcano Mt. Iwate (IWT), we applied the interstation transfer function (ISTF) method to the three-component geomagnetic field data observed at Mt. Iwate station (IWT), using the Kakioka Magnetic Observatory, JMA (KAK) as remote reference station. Instead of the conventional Fourier transform, in which temporary transient noises badly degrade the accuracy of long term properties, continuous wavelet transform has been used. The accuracy of the results was as high as that of robust estimations of transfer functions obtained by the Fourier transform method. This would provide us with possibilities for routinely monitoring the transfer functions, without sophisticated statistical procedures, to detect changes in the underground electrical conductivity structure. 相似文献
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Makoto Kume Atsunori Hirano Bungo Ochiai Takeshi Endo 《Journal of polymer science. Part A, Polymer chemistry》2006,44(11):3666-3673
A spiro orthoester with an exomethylene group (exoSOE) was radically copolymerized with acrylonitrile or vinyl acetate at several feed ratios to obtain the corresponding copolymers having spiro orthoester moieties in the side chain. The obtained copolymers could be crosslinked via the double ring‐opening polymerization of the spiro orthoester moieties in their side chain by a treatment with BF3OEt2. The volume changes upon the crosslinking of the copolymers were evaluated by density measurements with a micromeritics gas pycnometer. The copolymers experienced less than 1% volume expansion instead of volume shrinkage during typical cationic crosslinking, regardless of the copolymer compositions. Negligible shrinkage was observed during the thermal cationic crosslinking of a film cast from a nitrobenzene solution of the copolymers containing a benzylthiophenium salt as a thermally latent cationic initiator. The constantly low volume changes during the crosslinking of the copolymers from exoSOE probably depended on the almost zero volume change during the cationic polymerizations of spiro orthoester derivatives. This indicates that exoSOE is an effective monomer for crosslinkable polymers without volume changes. © 2006 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 44: 3666–3673, 2006 相似文献
14.
Makoto Kato Azusa Tsukigase Hiromitsu Tanaka Arimitsu Usuki Isamu Inai 《Journal of polymer science. Part A, Polymer chemistry》2006,44(3):1182-1188
Isobutylene isoprene rubber (IIR)‐clay nanocomposites have been prepared successfully by melt intercalation with maleic anhydride‐grafted IIR (Ma‐g‐IIR) and organophilic clay. In IIR‐clay nanocomposites, the silicate layers of the clay were exfoliated and dispersed into the monolayer. The nanocomposites exhibited greater gas barrier properties compared with those of Ma‐g‐IIR. When 15 phr clay was added, gas barrier properties were 2.5 times greater than those of Ma‐g‐IIR. © 2005 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 44: 1182–1188, 2006 相似文献
15.
Makoto Kume Yuya Maki Bungo Ochiai Takeshi Endo 《Journal of polymer science. Part A, Polymer chemistry》2006,44(24):7040-7053
Spiro orthocarbonate (SOC) monomers having either an exomethylene group {3,3‐dimethyl‐9‐methylene‐1,5,7,11‐tetraoxaspiro[5.5]undecane (ExoSOC)} or an allyl group {9‐allyl‐3,3‐dimethyl‐1,5,7,11‐tetraoxaspiro[5.5]undecane (AllylSOC)} were radically copolymerized with vinyl monomers at several feed ratios to obtain the corresponding copolymers having SOC moieties in the side chain. The obtained copolymers were crosslinked via the double ring‐opening polymerization of the SOC moieties by a treatment with boron trifluoride etherate. The volume changes during the crosslinking of the copolymers were evaluated by density measurements with a gas pycnometer. As the SOC moiety composition increased, the volume shrinkage during the crosslinking was suppressed, and that finally changed into volume expansion. The volume changes during the crosslinking of the copolymers from AllylSOC were slightly larger than those of the copolymers from ExoSOC. The higher volume expansions in the crosslinking of AllylSOC‐based copolymers were ascribable to the lower steric hindrance around the SOC moieties. © 2006 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 44: 7040–7053, 2006 相似文献
16.
Kazuhiko Nakano Toshihiro Nakamura Izumi Nakai Akira Kawase Makoto Imai Mikio Hasegawa Yohichi Ishibashi Isamu Inamoto Kazuhuyu Sudou Masaru Kozaki Akira Tsuruta Akihiro Ono Kazutoshi Kakita Mamoru Sakata 《Analytical sciences》2006,22(9):1265-1268
The Japan Society for Analytical Chemistry has developed some new plastic certified reference materials (CRMs) for the analysis of mercury in polyester disks using XRF analysis. These CRMs (named as JSAC 0621-0625) were prepared by casting polyesters including a toluene solution of organometallic compounds as a standard. Concentrations of the five levels of mercury ranged from 0 to 250 mg/kg. Homogeneity tests of prepared disks had shown excellent results. Interlaboratory comparison study for the certification was performed by 15 laboratory participants. The z-scores in robust statistical method was applied for the evaluation of outliers. The certified values were assigned after discarding outliers. The uncertainties of certified values were determined as the confidence levels of 95%. 相似文献
17.
Weighted Strichartz estimates with homogeneous weights with critical exponents are proved for the wave equation without a support restriction on the forcing term. The method of proof is based on expansion by spherical harmonics and on the Sobolev space over the unit sphere, by which the required estimates are reduced to the radial case. As an application of the weighted Strichartz estimates, the existence and uniqueness of self‐similar solutions to nonlinear wave equations are proved on up to five space dimensions. © 2006 Wiley Periodicals, Inc. 相似文献
18.
LetX be ann-element set and letA and? be families of subsets ofX. We say thatA and? are crosst-intersecting if |A ∩ B| ≥ t holds for all A ∈A and for allB ∈ ?. Suppose thatA and ? are crosst-intersecting. This paper first proves a crosst-intersecting version of Harper's Theorem:
- There are two crosst-intersecting Hamming spheresA 0,? 0 with centerX such that |A| ≤ |A 0| and|?| ≤ |? 0| hold.
- Suppose thatt ≥ 2 and that the pair of integers (|A) is maximal with respect to direct product ordering among pairs of crosst-intersecting families. Then,A and? are Hamming spheres with centerX.
- Ifn + t = 2k ? 1 then |A| |?| ≤ max \(\left\{ {\left( {K_k^n + \left( {_{k - 1}^{n - 1} } \right)} \right)^2 ,K_k^n K_{k - 1}^n } \right\}\) holds, whereK l n is defined as \(\left( {_n^n } \right)\left( {_{n - 1}^n } \right) + \cdots + \left( {_l^n } \right).\)
- Ifn + t = 2k then |A| |? ≤ (K k n )2 holds.
19.
Tetrakis-acridinyl peptide 1 assuming a right-handed helical stacked conformation of the acridinyl units can bind to DNA duplex with a very high affinity of 10(8) (M-bp)(-1) even at a high salt concentration of 0.2 M NaCl, irrespective of the base composition. Peptide 1 gave rise to 1600-times enhancement of its fluorescence upon binding to an AT polymer due to the collapse of this stacked structure, but the fluorescence is not enhanced with a GC polymer, though the binding constants of 1 for both polymers were the same. 相似文献
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