工作点测量系统在合肥光源的应用研究

 介绍了利用合肥光源(HLS)的工作点测量系统进行一些束流参数的测量及其应用研究，这些参数包括工作点、β函数；自然色品以及中心频率。同时还进行了清洗电极对工作点的影响的测量。给出了一些测量结果，测量结果与理论计算值相当吻合。     

Band gap tunable and improved microstructure characteristics of Cu2ZnSn(S1−x,Sex)4 thin films by annealing under atmosphere containing S and Se

Cu₂ZnSn(S_xS_1?x)₄ (CZTSSe) thin films were prepared by annealing a stacked precursor prepared on Mo coated glass substrates by the sputtering technique. The stacked precursor thin films were prepared from Cu, SnS₂, and ZnS targets at room temperature with stacking orders of Cu/SnS₂/ZnS. The stacked precursor thin films were annealed using a tubular two zone furnace system under a mixed N₂ (95%) + H₂S (5%) + Se vaporization atmosphere at 580 °C for 2 h. The effects of different Se vaporization temperature from 250 °C to 500 °C on the structural, morphological, chemical, and optical properties of the CZTSSe thin films were investigated. X-ray diffraction patterns, Raman spectroscopy, and X-ray photoelectron spectroscopy results showed that the annealed thin films had a single kesterite crystal structure without a secondary phase. The 2θ angle position for the peaks from the (112) plane in the annealed thin films decreased with increasing Se vaporization temperature. Energy dispersive X-ray results showed that the presence of Se in annealed thin films increased from 0 at% to 42.7 at% with increasing Se vaporization temperatures. UV–VIS spectroscopy results showed that the absorption coefficient of all the annealed thin films was over 10⁴ cm^?1 and that the optical band gap energy decreased from 1.5 eV to 1.05 eV with increasing Se vaporization temperature.     

通讯波段单光子探测器的研制

将InGaAs/InP雪崩光电二极管应用于盖革模式下,采用门脉冲模式淬灭雪崩,并使用魔T混合网络抑制尖峰噪声,实现了通信波段1550 nm的单光子探测.在APD工作温度为223 K时,测得暗计数率与探测效率的比值为0.035.     

准同心广义经纬相机的成像模型及高精度标定

对于大尺度运动目标的参数测量,固定相机存在着视场与空间分辨率之间的矛盾,并且当测量空中或海上目标时相机的标定也十分困难。跟踪式相机(如光电经纬仪)能解决此问题,但存在体积大、成本高和操作复杂等缺点。结合两者特点取长补短,将相机固定在二维旋转平台上,尽可能实现同心放置,组成准同心广义经纬相机进行中远场高精度测量,测量过程中转台实时跟踪目标并为相机提供外参数。此方法并没有光电经纬仪非常严格的同心同轴的安装要求。在合理假设基础上建立了经纬相机成像模型,提出了线性求解及平差优化相机参数的方法。大量仿真与实际测量验证了模型和标定方法的正确性和高精度。广义经纬相机测量系统组合巧妙、装拆和操作简单、体积小、成本低、可全视场测量且测量精度高,有广泛且重要的应用前景。     

光学系统受迫振动的激光测量方法

将激光信号与高帧频CCD结合,解决了光学系统中振动信号和激光信号之间的转换问题,不仅能够测量振动对系统光束指向稳定性的影响,而且能够得到振动信号本身的频率特性。利用该方法对振源为150 Hz和200 Hz两种条件下的光学系统受迫振动进行测量,得到了与输入信号相吻合的振动信号属性。通过实验与分析得知:时域振幅测量精度为6.25 m,频域分辨力为2 Hz,方法简便高效,测量结果准确,已应用于角多路准分子激光主振荡功率放大器系统打靶试验平台光束指向稳定性的研究中。     

三七中Cu、Pb和Cd含量的不确定度评定

采用电感耦合等离子体-原子发射光谱法测定三七中Cu、Pb和Cd,对影响测定结果的不确定度来源进行了分析,在此基础上评定了分析结果的不确定度。研究表明,样品的重复性和校准曲线的拟合是影响不确定度的主要原因。     

The ac conductivity and complex impedance of CuO-doped (Ba0.5Sr0.5)TiO3 ceramic

The AC conductivity and complex impedance spectroscopy of CuO-doped (Ba_0.5Sr_0.5)TiO₃ ceramic were investigated. X-ray diffraction analysis showed that CuO-doped (Ba_0.5Sr_0.5)TiO₃ has a perovskite structure without any pyrochlore phase. Frequency dependent dielectric permittivity was discussed at a different temperature range. The activation energy was calculated and discussed through the Arrehnius equation from the ac conductivity with different frequency plots. CuO-doped (Ba_0.5Sr_0.5)TiO₃ ceramics have a negative temperature coefficient of resistivity. Dependence of impedance spectroscopy on frequency and temperature showed that the conduction process in the CuO-doped (Ba_0.5Sr_0.5)TiO₃ ceramic follows the thermally activated conduction mechanism.     

Design of multiplexed fiber optic chemical sensing system using clad-removable optical fibers

To prevent possible threats to public safety and economic loss from chemical leakage accidents, novel chemical sensing techniques for regular monitoring and leakage detection have been developed for various fields. We propose a fiber optic liquid chemical sensor (FOCS) system using specialty optical fibers and an optical time domain reflectometer (OTDR), and is based on the leaky wave mode sensing principle. OTDR enables simple multiplexing where individual sensor nodes along the fiber length could be interrogated by a common OTDR. The sensor node in the optical fiber is prepared by removing the desired length of a protective layer using mechanical stripping and chemical etching techniques. A novel laser stripping technique with superior capability to fabricate quasi-distributed dense sensor nodes is devised as well. The FOCS system is further analyzed to characterize the sensor response behavior in relation to the sensor node length and possible environmental and chemical temperature effect. Under the condition satisfying the leaky wave mode principle and within the minimum acceptable refractive index (RI) range by the system, this FOCS system could monitor numerous liquid chemicals with variable refractive indices and has been tested with positive results. In addition, the system shows the possibility for multi-point detection and is further expanded into a hybrid technique capable of estimating the refractive index range of the detected chemical.     

Experimental observation of tangent-azimuthal non-spiral optical vortex

Optical vortices have attracted much attention recently due to their novel properties and widening applications. And lots of optical vortices can be obtained though most of them turn on spiral pattern on increasing azimuthal angle. In this paper, one kind of non-spiral optical vortex was proposed whose front phase distribution is tangent function of azimuthal angle. And this kind of optical vortices were also observed experimentally by computer-generated hologram method. It was found that when topological charge is smaller than unit one, vortex beam shape changes considerably on increasing topological charge, from hollow pattern to curve shape. When topological charge is bigger than unit and is times of 0.5, vortex beam turns symmetrical polygonal pattern though there is crack between adjacent sides, and the side number is twice of topological charge.     

电感耦合等离子体-质谱法测定工业硅中的痕量硼和磷

建立电感耦合等离子体-质谱法(ICP-MS)测定工业硅中痕量B和P的分析方法.采用HF-HNO3混合酸处理样品,对仪器工作参数进行优化,以Rh为校正内标,有效克服了基体效应及多元素分子离子干扰.分析结果表明,方法的检出限为:B为2.0μg·L-1、P为8.5μg · L-1,B和P的加标回收率分别为:97.2％-103.6％、95.2 ％-102.8％,精密度分别为2.6％、3.5％.方法可准确、快速测定工业硅中痕量元素B和P.