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871.
872.
Lucas Hernández Pedro Hernández José Vicente 《Fresenius' Journal of Analytical Chemistry》1993,345(11):712-715
Summary The determination of methyl-parathion (MPT), ortho (ONP), meta (MNP) and para nitrophenol (PNP) has been studied by differential pulse voltammetry with a carbon-paste electrode modified with 50% (w/w) of C18. A study of the influence of the pH in the preconcentration cell and the measurement cell was carried out for an electrode with 50% modifier and an accumulation time of 5 min. The voltammograms were recorded with a sweep rate of 40 mV s–1 and a pulse amplitude of 50 mV. With the optimum conditions of pH for both of the steps, various other variables were studied. The variables for each compound were optimized and the possibility of application to the determination of a mixture of the four compounds was investigated. The determination limits found for all the compounds are: 2 ng ml–1 for ONP, 5 ng ml–1 for MNP, 4.3 ng ml–1 for PNP and 7.9 ng ml–1 for MPT. The method was applied to samples of a small lake which gathers rain water and water filtered from land on which cereals are grown. 相似文献
873.
Consideringsystem:x=φ(y)-F(x),y=-g(x){(E)inwhichF(x)=∫x0f(t)dt,f(x),g(x),φ(y)arecontinuous,andsatisfytheconditionswhichensur... 相似文献
874.
3-Hydroxybutyramides are obtained in high optical yield from ethyl (±)-3-hydroxybutyrate and aliphatic amines when the reaction is catalyzed by Candida antartica lipase. The chemical reduction of these 3-hydroxybutyramides yields the corresponding 1,3 -aminoalcohols. 相似文献
875.
THE SCHWARZIAN DERIVATIVE IN SEVERAL COMPLEX VARIABLES(II) 总被引:1,自引:0,他引:1
THESCHWARZIANDERIVATIVEINSEVERALCOMPLEXVARIABLES(II)GONGSHENGYUQIHUANGZHENGXUEANManuscriptreceivedAugust30,1996.De... 相似文献
876.
877.
在文(1),(2),(3)的基础上,我们首先在德摩根拓扑代数上用有限覆盖性质定义了紧性,并引入ω-元,ω-d-q-聚点等概念,并着重讨论了紧性与q-收敛性之间的关系。 相似文献
878.
ASYMPTOTIC NORMALITY OF PARAMETERSESTIMATION IN EV MODEL WITH REPLICATEDOBSERVATIONS 总被引:2,自引:0,他引:2
1 IntroductionFOrnully the EV (Errors-ill-Vaiables) nrodel is just tlie regressiOli medel with both depen-dent aud iudependeut variables arc subject to error (see, fOr exan1ple, [21~[71 alid tlie literaturecited tl1ere). Collsiderillg tliat iu mauy practical aPplications, taking replicated observationspresellts lio esseutial dimculties. heuce can offer a couveuiellt choice in avoidillg artilicia1 as-sunWtions about tlie nlodel. This case was studied ill essay [11, in which estinators of a … 相似文献
879.
Günter Georg Hoffmann Hans-Jürgen Hochkamp 《Fresenius' Journal of Analytical Chemistry》1992,344(4-5):227-228
Summary The application of a digital signal processor (DSP) to Fourier-transform infrared spectroscopy is described, which allows for near real-time display of the transformed interferograms as spectra. 相似文献
880.
Using a Bostick Gun as a plasma source, we have been investigating the effects of a moving plasma front on the frequency of an incident R.F. signal. We have been able to measure frequency shifts of 10 MHz frequency with a 2.6 GHz signal. The density is such that the plasma frequency is well above the transmitter frequency 1.3 meters from the plasma source. No magnetic field is used. 相似文献