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71.
72.
Results of the benchmark test are presented of comparing numerical schemes solving shock wave of Ms = 2.38 in nitrogen and argon interacting with a 43∘ semi-apex angle cone and corresponding experiments. The benchmark test was announced in Shock Waves Vol. 12, No. 4, in which we tried to clarify the effects of viscosity and heat conductivity on shock reflection in conical flows. This paper summarizes results of ten numerical and two experimental applications. State of the art in studies regarding the shock/cone interaction is clarified. PACS 01.50.Kw, 47.15.Pn Communicated by K. Takayama  相似文献   
73.
This paper develops an efficient particle tracking algorithm to be used in fluid simulations approximated by a high-order multidomain discretization of the Navier–Stokes equations. We discuss how to locate a particle's host subdomain, how to interpolate the flow field to its location, and how to integrate its motion in time. A search algorithm for the nearest subdomain and quadrature point, tuned to a typical quadrilateral isoparametric spectral subdomain, takes advantage of the inverse of the linear blending equation. We show that to compute particle-laden flows, a sixth-order Lagrangian polynomial that uses points solely within a subdomain is sufficiently accurate to interpolate the carrier phase variables to the particle position. Time integration of particles with a lower-order Adams–Bashforth scheme, rather than the fourth-order Runge–Kutta scheme often used for the integration of the carrier phase, increases computational efficiency while maintaining engineering accuracy. We verify the tracking algorithm with numerical tests on a steady channel flow and an unsteady backward-facing step flow.  相似文献   
74.
A high-throughput research platform was developed for the preparation and subsequent catalytic liquid-phase screening of ion-exchanged zeolites, for instance with regard to their use as heterogeneous catalysts. In this system aqueous solutions and other liquid as well as solid reagents are employed as starting materials and 24 samples are prepared on a library plate with a 4 × 6 layout. Volumetric dispensing of metal precursor solutions, weighing of zeolite and subsequent mixing/washing cycles of the starting materials and distributing reaction mixtures to the library plate are automatically performed by liquid and solid handlers controlled by a single common and easy-to-use programming software interface. The thus prepared materials are automatically contacted with reagent solutions, heated, stirred and sampled continuously using a modified liquid handling. The high-throughput platform is highly promising in enhancing synthesis of catalysts and their screening. In this paper the preparation of lanthanum-exchanged NaY zeolites (LaNaY) on the platform is reported, along with their use as catalyst for the conversion of renewables.  相似文献   
75.
Correlations between positive pions are investigated in the target fragmentation region of 200A GeV16O+nucleus collisions. The pions are measured with the Plastic Ball detector in the WA80 experiment at the CERN SPS. The target mass dependence of the radii and the correlation strength extracted by interferometry is studied. A new approach to the fit of the correlation function is introduced. The correlation strength and both invariant and transverse radii increase with decreasing target mass. The transverse radius for16O+C reactions appears to be much larger than the geometrical radius of the nuclei involved. For the Au target only a small fraction of the measured pions contributes to the apparent correlation. Hints for a much larger second component in16O+Au reactions are observed. Rescattering phenomena may provide a clue to understand these phenomena.  相似文献   
76.
Consider the following decision problem which P. Winkler and V. Bulitko (independently) showed was undecidable: Given a finite set Φ of rooted graphs and a positive integer r, is there a graph G such that Φ represents, up to isomorphism, the set of all r-neighborhoods of G? We show the undecidability of the related problem in which G is required to be the covering digraph of a partial ordering. Our construction shows that the problem remains undecidable (for certain fixed r) even when G is also required to be planar and bipartite.  相似文献   
77.
78.
The transverse spin relaxation of positive muons has been measured on an Al single crystal and on polycrystalline In after irradiation with 2 MeV electrons at 9 K or 11 K, sample transfer at 4.2 K, and various subsequent annealing treatments. The Al data are analysed in terms of diffusion-limited trapping by vacancies. This yields a muon diffusivityD μ which within experimental accuracy is proportional toT between 4 K and 50 K, indicating that in this temperature intervalD μ is dominated by one-phonon-assisted incoherent tunnelling. In In only very small effects due to the irradiation could be observed. The muons appear to be localized in octahedral interstices. From the motional averaging taking place above about 20 K the diffusivity ofD μ in In is deduced.  相似文献   
79.
In the present study, we have investigated different strategies for diastereoselective synthesis of thia[n]helicenes. We describe the introduction of different chiral auxiliaries at various positions and investigated their effect in the photocyclization reaction. Different chiral groups were placed at the sterically hindered position of the helical core and their interactions with various solvents and metals like copper were investigated. The use of CuI salts has led to high diastereoselectivity in the photocyclization process and we were successful in obtaining the thia[5]helicene in enantiomerically pure form in good yield. The single diastereomer obtained was characterized by X‐ray crystallography. From the study of the barrier of racemization of these thia[5]helicenes, the stability was found to be comparable to unsubstituted tetrathia[7]helicenes and substituted diazadithia[7]helicenes. This approach provides an easy access to enantiopure helicenes.  相似文献   
80.
Experiments to demonstrate the use of the background-oriented schlieren (BOS) technique in hypersonic impulse facilities are reported. BOS uses a simple optical set-up consisting of a structured background pattern, an electronic camera with a high shutter speed and a high intensity light source. The visualization technique is demonstrated in a small reflected shock tunnel with a Mach 4 conical nozzle, nozzle supply pressure of 2.2 MPa and nozzle supply enthalpy of 1.8 MJ/kg. A 20° sharp circular cone and a model of the MUSES-C re-entry body were tested. Images captured were processed using PIV-style image analysis to visualize variations in the density field. The shock angle on the cone measured from the BOS images agreed with theoretical calculations to within 0.5°. Shock standoff distances could be measured from the BOS image for the re-entry body. Preliminary experiments are also reported in higher enthalpy facilities where flow luminosity can interfere with imaging of the background pattern. A version of this paper was presented at the 25th International Symposium on Shock Waves in Bangalore in July 2005.  相似文献   
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