Differential non-destructive image current detection in a fourier transform quadrupole ion trap

Dual-detector differential non-destructive Fourier transform detection in a quadrupole ion trap is shown to improve signal intensity and reduce noise compared with spectra recorded using a single detector. A larger area detector in each end-cap electrode is machined to fit its hyperbolic shape and so minimize field imperfections on the z-axis. Argon, acetophenone and bromobenzene spectra were recorded to allow a comparison between single- and dual-detector (differential) modes of detection and to demonstrate the improvement achieved with differential detection. Copyright 1999 John Wiley & Sons, Ltd.     

Pseudo-steady-state solutions for solidification in a wedge

Polubarinova-Kochina's analytical differential equation methodis used to determine the pseudo-steady-state solution to problemsinvolving the freezing (solidification) of wedges of liquidwhich are initially at their fusion temperature. In particular,we consider four distinct problems for wedges which are: freezingwith the same constant boundary temperature, freezing with thesame constant boundary heat fluxes, freezing with distinct constantboundary temperatures and freezing with distinct constant fluxesat the boundaries. For the last two problems, a Heun's differentialequation with an unknown singularity is derived, which in bothcases admits a particularly elegant simple solution for thespecial case when the wedge angle is . The moving boundariesobtained are shown pictorially.     

In-beam gamma-ray spectroscopy of 190, 197Po

γ -ray transitions in the neutron-deficient nuclei ^{190, 197}Po have been identified using the JUROGAM Ge detector array coupled to the RITU gas-filled separator and the GREAT spectrometer. The yrast band of ¹⁹⁰Po has been firmly established through γ -γ coincidences and extended up to a spin and parity of 14⁺. It displays similar behaviour to its isotones ¹⁸⁶Hg and ¹⁸⁸Pb above the 4⁺ level, thus confirming its prolate nature. In ¹⁹⁷Po the band built upon the 13/2⁺ isomer has been extended up to a spin and parity of 33/2⁺, while the non-yrast band has been observed for the first time. The behaviour of ¹⁹⁷Po is found to be similar to that of the nearby even-mass isotopes, which is consistent with the model in which the i _13/2 neutron is weakly coupled to the states in the even-even core.     

An application of the pixe method: Analysis of trace elements after wet digestion of uterine tissue

The authors present an application of the PIXE (Particle Induced X-ray Emission) method: determination of trace element concentrations in uterine tissue after wet digestion by HNO₃. A method for calibration of the system is described. Results of the analysis of a NBS reference material (National Bureau of Standards), SRM 1577 bovine liver, are given and possible sources of error are discussed. In the authors’ experience, the combination of wet digestion and PIXE provides a tool for reliable analysis of trace element concentrations in tissues.