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861.
Times of longitudinal T
1b
and transverse T
2b
magnetic relaxation of hexane and decane molecules in micropores of ZSM-5 silicalite were measured as functions of the content of these liquid n-alkanes in zeolite and of temperature. The stepwise changes in the T
1b
and T
2b
times were revealed in the region of 8% content of hydrocarbons. The observed changes in the concentration and temperature dependences of T
1b
and T
2b
times are explained by the rearrangement of silicalite crystal lattice under the action of adsorbed molecules. 相似文献
862.
The development of the poly(3‐hydroxybutyrate) (PHB) morphology in the presence of already existent poly(vinylidene fluoride) (PVDF) spherulites was studied by two‐stage solidification with two separate crystallization temperatures. PVDF formed irregular dendrites at lower temperatures and regular, banded spherulites at elevated temperatures. The transition temperature of the spherulitic morphology from dendrites to regular, banded spherulites increased with increasing PVDF content. A remarkable amount of PHB was included in the PVDF dendrites, whereas PHB was rejected into the remaining melt from the banded spherulites. When PVDF crystallized as banded spherulites, PHB could consequently crystallize only around them, if at all. In contrast, PHB crystallized with a common growth front, starting from a defined site in the interfibrillar regions of volume‐filling PVDF dendrites. It formed by itself dendritic spherulites that included a large number of PVDF spherulites. For blends with a PHB content of more than 80 wt %, for which the PVDF dendrites were not volume‐filling, PHB first formed regular spherulites. Their growth started from outside the PVDF dendrites but could later interpenetrate them, and this made their own morphology dendritic. These PHB spherulites melted stepwise because the lamellae inside the PVDF dendrites melted at a lower temperature than those from outside. This reflected the regularity of the two fractions of the lamellae because that of those inside the dendrites of PVDF was controlled by the intraspherulitic order of PVDF, whereas that from outside was only controlled by the temperature and the melt composition. The described morphologies developed without mutual nucleating efficiency of the components. © 2003 Wiley Periodicals, Inc. J Polym Sci Part B: Polym Phys 41: 873–882, 2003 相似文献
863.
P. Krais J. F. H. Custers J. K. Putzeiko und Fujii-Kanekoto 《Fresenius' Journal of Analytical Chemistry》1938,114(5-6):235-237
Ohne Zusammenfassung 相似文献
864.
865.
866.
D. I. Naiduss W. W. Kiesewetter S. L. Dikanskaja J. Schapiro R. Meurice J. Cartiaux E. F. Posorski G. N. Murthy S. Mihaéloff A. D. Rich J. J. Vollertsen Gh. Ghimicescu G. Kotsis C. T. Townsend J. A. Esty F. C. Baselt R. Dubrisay J. Gascon E. R. Scheggia K. M. Renner E. S. Miller C. A. Mitchell A. G. Sossin und S. E. Spektor 《Fresenius' Journal of Analytical Chemistry》1939,118(1-2):48-51
Ohne Zusammenfassung 相似文献
867.
M. Wunder und V. Thüringer 《Fresenius' Journal of Analytical Chemistry》1913,52(12):737-739
Ohne Zusammenfassung 相似文献
868.
Ohne Zusammenfassung 相似文献
869.
Freiherrn M. v. Thielmann 《Mathematische Annalen》1906,62(3):401-408
Ohne Zusammenfassung 相似文献
870.
Thermal behaviour and biochemical activity of potassium-silicate-phosphate glasses modified by addition of Ca, Mg, acting
as ecological fertilisers of controlled release rate of the nutrients for plants were studied. It has been found that the
biochemical activity of silicate-phosphate glasses depends on the nature and the number of components forming the glassy framework
and is related to the thermal stability of glass demonstrated by the formation of new compounds during the process of crystallisation.
It is proved that these seemingly different properties are determined by the same parameters which are the strengths bonds
of glass network-formers and modifiers as well as their chemical affinity.
This revised version was published online in July 2006 with corrections to the Cover Date. 相似文献