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1.
W. D. Hutchison A. V. J. Edge N. Yazidjoglou D. H. Chaplin 《Hyperfine Interactions》1992,75(1-4):291-298
The high resolution hyperfine spectroscopy, modulated adiabatic passage of oriented nuclei (MAPON), has been applied for the
first time to high purity, elemental systems. Detailed comparisons between the electric quadrupole hyperfine interactions
(EQI’s) and, in particular, their distributions, are obtained for60CoCo where the hosts are a single crystal of hcp cobalt and a polycrystalline cobalt foil of predominantly fcc character. For
hcp Co, with the electronic magnetization, M, parallel to the c-axis, the mode value P/h=3e2qQ/4I(2I−1)h=−48.5(5) kHz. This fractional distribution implies the sharpest electric field gradient (efg) measured in a metal
to date, using MAPON spectroscopy, in excess of two times sharper than that of the most dilute impurity efg in a crystallographically
cubic ferromagnetic host. The mode efg is Vzz=−27.3(32)×1019 Vm−2. For the polycrystalline, predominantly fcc foil, prepared by quenching, the EQI mode value is P/h=−6.2(4) kHz with a FWHM
of 12.0(7) kHz yielding a mode efg of Vzz=−3.5(5)×1019 Vm−2. 相似文献
2.
W. D. Hutchison N. Yazidjoglou D. J. Isbister D. H. Chaplin L. N. Shakhmuratova 《Hyperfine Interactions》1993,80(1-4):1173-1178
Results for an inhomogeneously broadened60CoFe NMRON sample have been obtained for gamma detected single pulse (nutation) and two pulse (free induction decay) experiments in the region of intermediate-to-lowR(=1/). Here 1 is the angular frequency measure of the strength of the ferromagnetically enhanced RF field at the nucleus and is the HWHM of the inhomogeneously broadened line. Comparisons of the oscillatory FID signals obtained are made with the theoretical predictions of the following paper [6]. 相似文献
3.
Santosh K. Shrestha Heiko Timmers Aidan P. Byrne Wayne D. Hutchison Don H. Chaplin Rakesh Dogra 《Hyperfine Interactions》2004,158(1-4):407-411
A radioisotope ion implanter has been developed using a cesium-sputtering, negative ion source, which offers versatility and
sustained operation. Employing the molecular 111In16O− ion, μCi activities of the radioisotope probe 111In/Cd have been implanted into different material hosts. The implanted tracer activity has been shown to be sufficient for
LTNO, NMRON and PAC. A new NMRON resonance for 111InAg was observed at 75.08 MHz. In2O3 powder performed well as the radioisotope carrier in the ion source, with the ratio of radioisotope and parasitic ion current
being typically 4 × 10−4. 相似文献
4.
S. G. Hutchison C. M. Wai J. Dong R. J. Kearney 《Plasma Chemistry and Plasma Processing》1995,15(2):353-367
The feasibility of producing titanium metal from titanium tetrachloride in a thermal plasma under equilibrium and adiabatic expansion conditions has been theoretically investigated. Free energy minimization and adiabatic expansion calculations to simulate a nozzle expansion were used to study the practicality of production. The crucial requirements for the production of titanium powder from TiCl4 and H2 appear to be rapid quenching of the plasma gas at high temperature (e.g., 3700 K) and appropriate reactant concentrations. Quenching of tire plasma gas and production of titanium powder can be achieved by adiabatic expansion through a nozzle. Preliminary experimental data indicate that titanium powder of approximately 5 nm in size can be produced in an argon plasma rising a nozzle expansion approach. 相似文献
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8.
Maxwell Sherrod L. Culligan Brian Hutchison Jay B. Utsey Robin C. Sudowe Ralf McAlister Daniel R. 《Journal of Radioanalytical and Nuclear Chemistry》2017,311(1):439-446
The sorption and diffusion behavior of cesium was studied to support the interpretation of the ongoing in-situ experiments in the Olkiluoto test site. The distribution coefficients of cesium in the Olkiluoto pegmatitic granite, veined gneiss and their main minerals were obtained by batch sorption experiments and the diffusion of cesium was studied in rock cubes. The results were modelled with PHREEQC and Comsol Multiphysics. The distribution coefficients of cesium were largest in biotite and veined gneiss. The effective diffusion coefficients of cesium from the diffusion model were 3 × 10−13 m2 s−1 for veined gneiss and 4 × 10−13 m2 s−1 for pegmatitic granite.
相似文献9.
D. H. Chaplin W. D. Hutchison M. P. Kopp N. Yazidjoglou 《Hyperfine Interactions》1988,43(1-4):241-247
Electric quadrupole interactions of impurity nuclei in single crystals of54MnNi,125SbNi and125SbFe have been studied as a function of crystal field direction and applied magnetic field using MAPON. Distributions are in all
cases broad compared with the mode values of the EQI's. For54MnNi the mode efg is isotropic to better than 5% between the easy <111> axis and a hard <100> axis. The efg is +0.88 (15)x 1019 Vm−2. The mode efg for125SbFe along its easy <100> axis is one half of that along a hard <112> axis, and one third of that measured along the easy <111>
axis of125SbNi. The much larger efg mode and distribution seen in125SbNi, for four to eight times greater dilution than for125SbFe, suggests intrinsic contributions due to valence screening effects in the more itinerant nickel host. 相似文献
10.
Lattice images of 4H, 5H, and 6H perovskite polytypes have been obtained. With the electron beam parallel to 10
, the images are correlated directly with the projected structures of the polytypes. Stacking faults were found only in the 6H compound, and consisted of additional cubic close-packed AO3 layers. Ordering of cation vacancies in the 5H material was evident in the lattice image as an array of white dots. 相似文献