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Tetsushi Kijima Masakazu Nishida Haruhiko Fukaya Masato Yoshida Hideo Sawada 《Journal of polymer science. Part A, Polymer chemistry》2013,51(12):2555-2564
A reddish‐brown fluoroalkyl end‐capped 2‐acrylamido‐2‐methylpropanesulfonic acid (AMPS) oligomer/acetone composite was prepared by heating the white oligomer powder with acetone at 80 °C for 3 h. The color was not observed in the corresponding non‐fluorinated AMPS oligomer/acetone composite, which was prepared under similar conditions. The coloring was probably caused by the formation of acetone polyaldol condensation products in the fluorinated oligomeric gel network cores. The colored RF‐(AMPS)n‐RF/acetone composite powders were stable and did not exhibit any color change after 2 years in natural light at room temperature. The colored composite powders dissolved in methanol to give a reddish‐brown solution at room temperature. However, the retro‐polyaldol condensation decolored the solution after 1 day at room temperature. This is the first example of the retro‐aldol polycondensation of acetone under mild conditions. The decoloration increased by between 38‐ and 70‐fold under UV irradiation, compared with that in dark conditions. The coloring–decoloring behavior was consistent and repeatable; therefore our fluorinated oligomer/acetone composites are promising candidates for new fluorinated coloring materials. © 2013 Wiley Periodicals, Inc. J. Polym. Sci., Part A: Polym. Chem. 2013, 51, 2555–2564 相似文献
154.
Naoto Nishio Kentaro Yamana Yasutaka Yamaguchi Takehiko Inaba Koji Kuroda Tadashi Nakajima Kouhei Ohno Hideo Fujimura 《国际流体数值方法杂志》2010,63(12):1435-1447
In this study, the whole process of liquid droplet impact onto a liquid surface up to the consequent formation of the central column was simulated using the smoothed particle hydrodynamics method (SPH), and compared with an experiment using a high‐speed video camera. The surface tension tensor for the particle‐based expression was adequately included as the gradient of the surface tension and that enabled the simulation leading to the formations of crater and crown as well as the consequent central column. The simulated time series of the crater depth and diameter and crown height corresponded quantitatively well with the experimental result up to the rebound motion while discrepancies remained as a lower central column height in the simulation, and this seemed to be ascribed to the difficulty in realizing the complex surface structure that inevitably appeared in the fast rebound motion. Copyright © 2009 John Wiley & Sons, Ltd. 相似文献
155.
Hideo Soga 《Communications in Mathematical Physics》1990,133(1):37-52
In the first half of this paper, we construct asymptotic solutions of linear anisotropic elastic equations. In the latter half, we investigate waves reflected by boundaries for plane incident waves in terms of these solutions. Especially, it is examined whether or not the mode-conversion occurs near points where the incident waves hit the boundaries perpendicularly. 相似文献
156.
Simultaneous two-dimensional imaging of an unburnt area and a reacting area was performed using laser-induced fluorescence. Acetone was added to fuel as a tracer, and OH radical was used as a marker of the reacting area. A narrow band tunable KrF excimer laser (248 nm) was employed to excite acetone and OH simultaneously. Two intensified CCD cameras with different wavelength filters were used to detect these two kinds of species respectively. Detecting 294-314 nm (A-X (3, 2), etc.) for OH and 335-410 nm for acetone, we obtained images of each species without interference of a signal from the other. The method was also successfully applied to flames in a pressurized combustion chamber under the pressure of 0.5 MPa. 相似文献
157.
We have observed a non-periodic diameter modulation in SiC nanowire growth. The modulation was tentatively attributed to a stick-slip motion in a self-organized vapor-liquid-solid (VLS) growth, and was characterized by methods of time-series analysis. From the power-law decay behavior of a fat tail of the probability distribution of increments with the exponent 2.1±0.2, the modulation was interpreted as a Lévy flight. The degree of determinism is also discussed. 相似文献
158.
Adsorption of N2 and N2O at various sites on Ni(7 5 5) has been investigated by density functional theory (DFT) method (periodic DMol3). Several possible adsorption structures (attaching the nitrogen atom to the surface, or lying parallel) are found for both molecules. There is a clear binding energy preference of N2 and N2O for step sites in contrast to the case of CO. It is revealed that the decomposition of N2O occurs exclusively near the step, but not on the terrace. Two decomposition channels can be considered; dissociative adsorption and spontaneous decomposition during TPD ramp. Three possible candidates for the precursor of the spontaneous decomposition of N2O during TPD ramp are discussed. 相似文献
159.
The estimation problems for the conventional step-up method (the observed breakdown voltages are not given at all) and the new step-up method (some of the observed breakdown voltages are given) are analyzed when the underlying probability distribution (of breakdown voltage level) is assumed to be gumbel distributions for minima and maxima. The new step-up test method has advantages compared to the conventional method: (1) the confidence intervals of the estimates become smaller and (2) the estimates can be obtained with higher probability. In some case of real step-up breakdown voltage test, a fit of the gumbel distribution to the data case is found to be superior to that of the normal distribution, which suggests the usefulness of the gumbel distribution for the underlying distribution in the step-up breakdown voltage test. 相似文献
160.