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31.
32.
Weisshoff H Preiss A Nehls I Win T Mügge C 《Analytical and bioanalytical chemistry》2002,373(8):810-819
A hyphenated HPLC-(1)H NMR method for the identification and quantification of PAHs in soil samples has been developed and applied to a PAH reference sample provided by the Federal Institute for Materials Research and Testing (BAM, Berlin, Germany). The results were compared with those obtained by HPLC-DAD, HPLC-F, and GC-MS analyses of the same sample. 相似文献
33.
Miller RI Kiefl RF Brewer JH Sonier JE Chakhalian J Dunsiger S Morris GD Price AN Bonn DA Hardy WH Liang R 《Physical review letters》2002,88(13):137002
Evidence for static alternating magnetic fields in the vortex cores of underdoped YBa2Cu3O6+x is reported. Muon spin rotation measurements of the internal magnetic field distribution of the vortex state of YBa2Cu3O6.50 in applied fields of H = 1 T and H = 4 T reveal a feature in the high-field tail of the field distribution which is not present in optimally doped YBa2Cu3O6.95 and which fits well to a model with static magnetic fields in the vortex cores. The magnitude of the fields is estimated to be 18(2) G and decreases above T = 10 K. We discuss possible origins of the additional vortex core magnetism within the context of existing theories. 相似文献
34.
Benzocyclobutene 10 and 3-oxabicyclo [3.2.0]hepta-1, 4-diene 11 are formed by gas-phase pyrolysis of the title compound 9 . The results are discussed with reference to the estimated reaction parameters. It is found that the activation due to oxygen in 9 is relatively weak in comparison to its effect on the reactivity of oxaquadricyclanes 1 . 相似文献
35.
Sutherland M Li SY Hawthorn DG Hill RW Ronning F Tanatar MA Paglione J Zhang H Taillefer L DeBenedictis J Liang R Bonn DA Hardy WN 《Physical review letters》2005,94(14):147004
Low-temperature heat transport was used to investigate the ground state of high-purity single crystals of the lightly doped cuprate YBa2Cu3O6.33. Samples were measured with doping concentrations on either side of the superconducting phase boundary. We report the observation of delocalized fermionic excitations at zero energy in the nonsuperconducting state, which shows that the ground state of underdoped cuprates is a thermal metal. Its low-energy spectrum appears to be similar to that of the d-wave superconductor, i.e., nodal. The insulating ground state observed in underdoped La2-xSrxCuO4 is attributed to the competing spin-density-wave order. 相似文献
36.
A new survey of all world data on superallowed beta decays provides demanding tests of, and tight constraints on, the weak interaction. In confirmation of the conserved vector current hypothesis, the vector coupling constant G(V) is demonstrated to be constant to better than three parts in 10(4), and any induced scalar current is limited to f(S)=0.0013 in electron rest-mass units. Any possible fundamental scalar current is similarly limited to /C(S)/C(V)/=0.0013. The superallowed data also determine the up-down element of the Cabibbo-Kobayashi-Maskawa (CKM) matrix to be V(ud)=0.9738(4). With Particle Data Group values for V(us) and V(ub), the top-row test of CKM unitarity yields /V(ud)/(2)+/V(us)/(2)+/V(ub)/(2)=0.9966(14); if V(us) comes instead from two recent results on K(e3) decay, this sum becomes 0.9996(11). Either unitarity result can be used to constrain the possible existence of right-hand currents. 相似文献
37.
Savard G Buchinger F Clark JA Crawford JE Gulick S Hardy JC Hecht AA Lee JK Levand AF Scielzo ND Sharma H Sharma KS Tanihata I Villari AC Wang Y 《Physical review letters》2005,95(10):102501
The masses of the radioactive nuclei (46)V and its decay daughter (46)Ti have been measured with the Canadian Penning Trap on-line Penning trap mass spectrometer to a precision of 1 x 10(-8). A Q(EC) value of 7052.90(40) keV for the superallowed beta decay of (46)V is obtained from the difference of these two masses. With this precise Q value, the Ft value for this decay is determined with improved precision. An investigation of an earlier Q-value measurement for (46)V uncovers a set of 7 measurements that cannot be reconciled with modern data and affects previous evaluations of V(ud) from superallowed Fermi decays. A new evaluation, adding our new data and removing the discredited subset, yields new values for G(V) and V(ud). When combined with recent results for V(us), this yields modified constraints for the unitarity of the Cabibbo-Kobayashi-Maskawa matrix and other extensions of the standard model. 相似文献
38.
We define cheat sensitive cryptographic protocols between mistrustful parties as protocols which guarantee that, if either cheats, the other has some nonzero probability of detecting the cheating. We describe an unconditionally secure cheat sensitive nonrelativistic bit commitment protocol which uses quantum information to implement a task which is classically impossible; we also describe a simple relativistic protocol. 相似文献
39.
Oganesyan VS Barclay JE Hardy SM Evans DJ Pickett CJ Jayasooriya UA 《Chemical communications (Cambridge, England)》2004,(2):214-215
The potential of NIS spectroscopy to study the iron-sulfur clusters in metalloproteins is illustrated using model compounds. The origin of the intense low energy transfer bands is discussed. 相似文献
40.
Hardy JC Iacob VE Sanchez-Vega M Neilson RG Azhari A Gagliardi CA Mayes VE Tang X Trache L Tribble RE 《Physical review letters》2003,91(8):082501
The half-life, 3.8755(12) s, and superallowed branching ratio, 0.5315(12), for 22Mg beta decay have been measured with high precision. The latter depended on gamma-ray intensities being measured with an HPGe detector calibrated for relative efficiencies to an unprecedented 0.15%. Previous precise measurements of 0+ --> 0+ transitions have been restricted to the nine that populate stable daughter nuclei. No more such cases exist, and any improvement in a critical Cabibbo-Kobayashi-Maskawa unitarity test must depend on precise measurements of more exotic nuclei. With this branching-ratio measurement, we show those to be possible for T(z)=-1 parents. We obtain a corrected Ft value of 3071(9) s, in good agreement with expectations. 相似文献