ICP—AES法测定人体胎盘血清中15种微量元素

用ICP-AES法测定了人体胎盘血清中15种微量元素。本法具有灵敏度较高,校正曲线的线性范围宽,基体效应小,尤其是进样量少等优点。本法可同时测定多种元素。     

利用X射线衍射研究冲击波合成纤锌矿型氮化硼

 用X射线衍射法，对不同结晶度的石墨型氮化硼（gBN）在冲击波作用下转变成的纤锌矿型氮化硼（wBN）产物进行了研究，对wBN中的杂质含量等进行了分析。结果表明：gBN的石墨化指数G.I值对wBN的产率有明显的影响。     

翘嘴鳜铜锌超氧化物歧化酶基因的分子克隆与原核表达

运用RT-PCR和RACE-PCR技术克隆了翘嘴鳜(Siniperca chuatsi)铜锌超氧化物歧化酶(命名为ScCu/Zn-SOD)基因,该基因的cDNA序列全长为804bp,开放阅读框为465bp,编码154个氨基酸。氨基酸序列中含2个Cu/Zn-SOD标签序列、7个铜锌金属结合位点、2个半胱氨酸位点和1个N-糖基化位点;其与胞内Cu/Zn-SOD(icCu/Zn-SOD)和胞外Cu/Zn-SOD(ecCu/Zn-SOD)氨基酸序列的同源性分别为60.13%~92.21%和33.77%~42.21%。在系统进化树中,ScCu/Zn-SOD与其它物种的icCu/Zn-SOD聚成一支。ScCu/Zn-SOD的蛋白晶体结构主要由2个α螺旋和8个β折叠组成,呈β折叠构象,通过结合1个Cu2+和1个Zn2+构成其酶活性中心。ScCu/Zn-SOD的mRNA在翘嘴鳜肌肉、鳃、肝脏和肾脏等组织中均有表达,且鳃中的相对表达量最高。将该基因编码蛋白序列与pET-30a表达载体重组,热激转入大肠杆菌BL21(DE3)感受态细胞中诱导表达,SDS-PAGE检测发现诱导后菌液的超声上清中有可溶性重组蛋白表达。     

Si含量对高锰硅化合物相组成及热电性能的影响研究

采用高频感应熔融、退火结合放电等离子烧结方法制备高锰硅(HMS)化合物MnSi1.70+x(x=0,0.05,0.1,0.15),系统研究了Si含量变化对材料相组成、微结构和热电性能的影响规律.结果表明,当x0.1时,样品由HMS和贫Si的MnSi金属相两相组成,随着Si含量x的增加,MnSi相相对含量减小;当x=0.1时,所得样品为单相HMS化合物;当x0.1时,样品由HMS和过量Si两相组成.随着x的增加,由于样品中高电导的金属相MnSi含量逐渐减少,样品的电导率逐渐下降,而Seebeck系数随之增加.室温下样品载流子浓度和有效质量随x增大逐渐减小,而迁移率逐渐增加.MnSi和Si杂相与HMS相比均为高热导相,因此当x=0.1时,由于样品为单相HMS,从而表现出最低热导率和最高ZT值.MnSi1.80样品在800K时热导率最小值达到2.25W·m-1K-1,并在850K处获得最大ZT值(0.45).     

Regulation of glutamatergic signalling by PACAP in the mammalian suprachiasmatic nucleus

Background  

Previous studies indicate that light information reaches the suprachiasmatic nucleus (SCN) through a subpopulation of retinal ganglion cells that contain both glutamate and pituitary adenylyl cyclase activating peptide (PACAP). While the role of glutamate in this pathway has been well studied, the involvement of PACAP and its receptors are only beginning to be understood. Speculating that PACAP may function to modulate how neurons in the suprachiasmatic nucleus respond to glutamate, we used electrophysiological and calcium imaging tools to examine possible cellular interactions between these co-transmitters.     

Spin-dependent Andreev reflection in a three-terminal Aharonov-Bohm interferometer with coherent indirect coupling

Within the framework of non-equilibrium Green’s functions, we investigate the spin-dependent Andreev reflection (AR) in a three-terminal Aharonov-Bohm interferometer with double quantum dot, taking account of the coherent indirect coupling via the superconducting reservoir. It is found that the time-reversal symmetry is broken by the crossed Andreev reflection (CAR) process, and moreover that the spin-value effect of the linear conductance, the spin-polarised AR current, and a pure spin current can be generated by means of the normal AR and the CAR. Expressions for the AR conductances (the transport coefficients) governing the AR properties of this system are derived analytically. The effect of the coherent indirect coupling on the conductance, the Andreev reflected tunneling magnetoresistance (ARTMR), and the spin-related current in the presence of the AR are amply analyzed. Our results indicate that the optimal properties of this system can be realised by tuning the external parameters.     

激光陀螺锁区特性的研究

从理论和试验两个方面,研究了四边形腔环行激光陀螺的锁区特性.利用环行腔中背向散射光束具有相干性,导出了环行谐振腔综合背向散射与反射镜、反射镜之间的相对位置的关系.在有两个位移反射镜的四边形谐振腔中,理论上得到了综合背向散射系数与谐振腔腔长具有双波长周期.利用综合背向光强实验及锁区与陀螺工作模数实验分别验证了理论的正确性.试验证实散射光的强度与谐振腔的工作模数存在双模周期性,综合背向散射系数大,陀螺锁区大,反之亦然.     

激光陀螺磁灵敏度特性研究

分析、计算了激光陀螺的磁灵敏度特性,并进行了磁灵敏度试验.试验结果及分析表明：在腔体加工准确度不变的情况下,采用合理的设计可以大大降低激光陀螺在某些方向上的磁灵敏度,同时磁试验结果对于设计激光陀螺的磁屏蔽结构具有一定的实用价值.     

Local chemical distribution and electronic structure of Ge1−xTx DMS single crystals (T=Cr,Mn, Fe)

The spatial concentration distribution and local electronic structure of ferromagnetic Ge_1−xT_x (T=Cr, Mn, Fe) DMS single crystals have been investigated by using scanning photoelectron microscopy (SPEM), X-ray absorption spectroscopy (XAS), and photoemission spectroscopy (PES). It is found that doped T ions in Ge_1−xT_x crystals are chemically phase-separated, suggesting that the observed ferromagnetism arises from the phase-separated T-rich phases in Ge_1−xT_x.