Dual-parameter Correlation Analysis of the Fluorescence Data of 1-Methyl-2-formyl-5-substituted Pyrrole(4-nitrophenyl)hydrazones

effect、pohrencct．l－methyl－2－formvl－5－Y－substitutedpyrrole（4－nltrophenyl）Ndrazones．Correlationresultsmrthefluorescencespectraldataofsubstitutedstyrenesanda－Onthebasisof＊themagnitudesofevaluatedlpm。／p、。”］valuesofEq．l，Inwhichp”a“（orPn。。／an，。）andPa（orP。』／a。。）rePresentthePolarandsPin－delocallzatloneffect，wehaverecentlyproposedthattherearefourcategoriesofpossiblecircumstancesforcorrelationanalysisofradlcalreactlvltlesandspectralpropeTtlesl．IBothpolarandsp…     

单功能基叔胺型弱碱树脂的合成及其滴定曲线研究

合成了以苯乙烯－二乙烯苯为骨架的若干叔胺型弱碱性树脂，研究了胺化反应条件，胺化试剂及交联度等对叔胺产碱树脂功能单一性的影响，测定了强碱交换量低的叔胺树脂的滴定曲线特征，找到了适合作为热再生树脂弱碱组分的单功能基叔胺树脂的合成条件。     

EFFECT OF INTERNAL VISCOSITY OF POLYMERIC FLUIDS UNDER STRONG EXTENSIONAL FLOWS

The dumbbell model with internal viscosity for a dilute polymer solution is investigated based on a balance of viscous drag and restoring Brownian forces.An approximate method is used to obtain the solution of extensional stress in closed form in the case of steady flow.For different internal viscosities,this parametric study shows different asymptotic regimes of the extensional viscosity as a function of strain rate.This analysis may explain the attenuation of pressure drop in strong flows from a phenom...     

PURIFICATION OF GINKGO LEAVES EXTRACT WITH MACROPOROUS ADSORBENT BASED ON UREA-FORMALDEHYDE CONDENSED POLYMERS

I INTRODUCTIONGinkgo biloba L. is one of the important economic trees, which is widely distributed inChina. In recent years, medicinal and healthful preparations based on the extractS from ginkgoleaves have been rapidly developed for the treatment of peripheral circulatory and cerebralinsufficiencyl']. Such eXtracts contain flavonol glycosides and terpene lactones as thepharmacologically active compounds. Organic-solvent extraction is one of the earliest methodsto prepare the extracts o…     

Precise absolute positioning for a single-frequency user

A new strategy to realize precise absolute positioning for a single-frequency user is presented. In the presented strategy, the receiver clock and ambiguities are removed using the satelliteand epoch-differenced (SDED) algorithm. As a further development of the SDED algorithm, a regional augmentation network is used to generate the SDED atmospheric delays at the user. The weakened mathematic property due to the epoch-differenced operation is improved by adding the generated atmospheric delays and applying the robust estimation. To test the new approach, the 24-h data at 5 Continuous Operation Reference Station (CORS) stations in Shanghai is processed. The results show a more than 96% success rate, defined as the case where three directions achieve the desired positioning accuracy of 10 cm, when the observation is longer than 20 min. The 20-min static results show that the new method can reach an accuracy of 3.42, 4.76 and 9.26 cm in the North, East and Up directions, respectively. An experiment was carried out to assess the kinematic positioning. The results show that the kinematic positioning accuracy is 4.11, 5.31 and 4.05 cm in the north-south, east-west and height directions,respectively.     

Additional symmetries of constrained CKP and BKP hierarchies

The additional symmetries of the constrained CKP (cCKP) and BKP (cBKP) hierarchies are given by their actions on the Lax operators, and their actions on the eigenfunction and adjoint eigenfunction {Φ i , Ψ i } are presented explicitly. Furthermore, we show that acting on the space of the wave operator, *k forms new centerless W cC 1+∞ and W cB 1+∞ -subalgebra of centerless W 1+∞ respectively. In order to define above symmetry flows *k of the cCKP and cBKP hierarchies, two vital operators Y k are introduce...     

尼卡巴嗪原料药及制剂中4,4′-二硝基均苯二脲与2-羟基-4,6-二甲基嘧啶的HPLC法同时测定

建立了同时测定尼卡巴嗪原料药及其制剂中4,4′-二硝基均苯二脲(DNC)和2-羟基-4,6-二甲基嘧啶(HDP)的高效液相色谱法。试样用二甲基亚砜溶解,以Hypersil BDS C18为色谱柱,乙酸/乙酸铵溶液-乙腈(体积比1∶1)为流动相,HDP和DNC的检测波长分别为290、350 nm。DNC和HDP的质量浓度分别在0.354~70.9 mg/L和0.146~29.2 mg/L范围内与色谱峰面积呈良好线性关系,标准曲线方程分别为ρ=7.307×10-5S-0.043 58和ρ=1.648×10-5S-0.084 83,相关系数(r)分别为1.000和0.999 9。用建立的方法测定尼卡巴嗪原料药中的DNC和HDP含量,测定结果与分光光度法无显著差异,DNC和HDP的相对标准偏差均小于0.5%。     

余代数上余倾斜余模的结构

研究了余代数上余倾斜余模的结构特征,证明了每个余倾斜余模都可以写成不可分解的两两非同构的余模的直和形式,每个余倾斜余模包含所有的内射不可分解模作为直和项.最后构造了余倾斜余模的两个例子.     

基于AFS拓扑和FCM的模糊聚类分析

聚类分析是数据挖掘的一个重要研究课题，模糊聚类是聚类分析的一个有效手段。本文在分析AFS方法和FCM算法的基础上，设计了一个基于AFS拓扑和FCM的模糊聚类算法，进行iris数据的聚类实验证明它聚类结果优于传统的FCM聚类算法，具有很好的推广性和实际应用价值。