Aggregation Properties of an Amphiphilic Methanofullerene Derivative in THFH_2O Solvent Mixtures

Water-soluble fullerenes not only have a number of important applications in biological chemistry1, but also form ordered aggregate structures that can be utilized in materials science2. There are reports that some water-soluble fullerene derivatives can form ordered structures in water, such as vesicle, nanorod and nanoparticle2-5. However, relatively few reports on the aggregation process have been reported. Knowledge of factors that affect the cluster formation in solution is of consider…     

γ辐射引发淀粉目由基衰减的动力学研究

用ESR方法研究了红薯淀粉在γ射线预辐照下,产生的淀粉自由基特性及其室温下的自由基衰减动力学反应。结果表明在室温条件下,淀粉自由基的相对浓度随辐射剂量的增大而增加。自由基相对浓度的室温衰减用二级反应动力学处理,求得了衰减速率常数和淀粉自由基反应的半衰期。     

In situ Synthesis of Oligonucleotides on Plasma Treated Polypropylene Microporous Membrane

Polypropylene microporous membranes were treated with plasma in a mixture of N2 and H2 (1:2 in volume). Attenuated total reflectance Fourier transform infrared spectroscopy (ATR-FTIR), X-ray photoelectron spectroscopy (XPS) and ultra-violet (UV) spectra demonstrated the success of grafting amino groups. The density of the polar amino groups on the membrane surface is about 0.59 μmol/cm^2. The as-treated membranes were successively applied to the in situ synthesis of oligonucleotides and an average coupling yield was more than 98%. The surface feature of the treated membrane is suggested to be responsible for its advantage over a glass slide.     

三溴偶氮胂褪色光度法测定土壤及化学试剂中铬（VI）

在 0 .4 8mol/L硝酸介质中 ,Cr( )与三溴偶氮胂 (TBA)发生褪色反应 ,该反应的表观摩尔吸光系数ε516nm=1.0 4× 10 5L· mol-1· cm-1,铬 ( )含量在 0— 1.0× 10 -4 g/L范围内呈良好线性关系。该法用于土样及化学试剂中 Cr( )的测定 ,结果令人满意。     

卡尔曼滤波紫外光度法同时测定酱油、食醋中的山梨酸和苯甲酸

在酸性条件下，采用乙酸乙酯萃取、Na2HPO4溶液反萃取分离酱汪、食醋中的山梨酸、苯甲酸，卡尔曼滤波法计算结果，并与比值导数波谱法进行比较。结果表明，卡尔曼滤波法较地数波谱法有较高准确度和精密度，并能监测干扰物质存在与否。用于实际样品分析有更高的可靠性。     

von Neumann代数中套子代数上的Lie同构

本文给出因子von Neumann代数中的幂等算子在广义Lie积下的一个刻画; 得到因子von Neumann代数中套子代数的幂等算子在Lie积下的一个特征．作为应用, 研究了因子von Neumann代数中套子代数上的Lie同构,并证明因子von Neumann 代数中套子代数之间的Lie同构,要么是同构与广义迹之和,要么是负反同构与广义迹之和．     

Optimization of a Cryogenic System at Temperature 2 K for the PKU-FEL Facility

The conceptual design of a cryogenic system at temperature 2 K for the Peking University Free Electron Laser （PKU-FEL） facility is carried out. In order to minimize the scale of the cryogenic system and the running cost, the superconducting accelerator and the superconducting injector will mainly run at a long-pulsed mode. Optimization of the 2-K cryogenic system is carried out based on the heat load estimation and running parameters. Total cooling power of 52.5 W for the long-pulsed mode is necessary for the PKU cryogenic system. The PKU cryogenic system will be the first 2-K system for accelerators in China and will provide experience for similar facilities.     

多级轴流压气机全工况特性计算

本文使用三维粘性流动计算软件Fine／Numeca,对某十五级轴流压气机进行了内流流场和全工况特性的数值计算尝试。分析了该压气机在设计工况和非设计工况的性能,同时把整机计算结果和前七级叶片的计算结果进行了比较。计算结果表明,当计算的级数较少时,目前的软件和硬件平台可以比较合理地预测压气机的全工况特性;而当计算的级数较多时,准确的数值模拟仍需要更为准确的多级模型和数值方法。     

Positive Steady States of a Prey-predator Model with Diffusion and Non-monotone Conversion Rate

In this paper, we study the positive steady states of a prey-predator model with diffusion throughout and a non-monotone conversion rate under the homogeneous Dirichlet boundary condition. We obtain some results of the existence and non-existence of positive steady states. The stability and uniqueness of positive steady states are also discussed.