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951.
Crystal Structure of the Zinc Amide Zn[N(SiMe3)2]2 X‐ray quality crystals of Zn[N(SiMe3)2]2 (monoclinic, P21/c) are obtained by sublimation of the zinc amide Zn[N(SiMe3)2]2 at —30 °C in vacuo (300 torr). According to the result of the X‐ray structural analysis, Zn[N(SiMe3)2]2 contains an almost linear N‐Zn‐N unit with two short N‐Zn bonds. 相似文献
952.
C.H Chung S.D KimH.J Kim F.O AdurodijaK.H Yoon J Song 《Solid State Communications》2003,126(4):185-190
The dependence of structural properties and surface morphology of Cu-In alloy layers on the composition and sputtering deposition sequence were investigated by X-ray diffraction, scanning electron microscopy and energy-dispersive X-ray spectroscopy. The properties of the co-sputtered alloy layers changed abruptly around the composition boundary when the Cu/In ratio reached 1/2. This can be explained by the effective heat of formation (EHF) model, which has been used to predict the sequence of phase formation for metal diffusion couples. The use of a co-sputtered alloy layer with a high In concentration was not suitable for fabricating solar cells, because the film had a very rough morphology due to large In islands formed on the CuIn2 phase. However, it was possible to minimize this phase by In sputtering followed by co-sputtering with a Cu/In ratio of 1 (Cu-In/In/Glass). This permitted the fabrication of a homogeneous Cu-In alloy layer, which was not possible through the simple co-sputtering. 相似文献
953.
L. D. Popov 《Central European Journal of Mathematics》2004,2(1):76-86
For a linear complementarity problem with inconsistent system of constraints a notion of quasi-solution of Tschebyshev type
is introduced. It’s shown that this solution can be obtained automatically by Lemke’s method if the constraint matrix of the
original problem is copositive plus or belongs to the intersection of matrix classes P
0 and Q
0. 相似文献
954.
Here we prove a limit theorem in the sense of the weak convergence of probability measures in the space of meromorphic functions
for a general Dirichlet series. The explicit form of the limit measure in this theorem is given.
Partially supported by Lithuanian Foundation of Studies and Science 相似文献
955.
In the paper the asymptotics for Dirichlet polynomials associated to certain cusp forms are obtained.
Partially supported by Lithuanian Foundation of Studies and Science 相似文献
956.
957.
Aji P. Mathew Gabriel Groeninckx G. H. Michler H. J. Radusch Sabu Thomas 《Journal of Polymer Science.Polymer Physics》2003,41(14):1680-1696
The effects of the blend ratio and initiating system on the viscoelastic properties of nanostructured natural rubber/polystyrene‐based interpenetrating polymer networks (IPNs) were investigated in the temperature range of ?80 to 150 °C. The studies were carried out at different frequencies (100, 50, 10, 1, and 0.1 Hz), and their effects on the damping and storage and loss moduli were analyzed. In all cases, tan δ and the storage and loss moduli showed two distinct transitions corresponding to natural rubber and polystyrene phases, which indicated that the system was not miscible on the molecular level. However, a slight inward shift was observed in the IPNs, with respect to the glass‐transition temperatures (Tg's) of the virgin polymers, showing a certain degree of miscibility or intermixing between the two phases. When the frequency increased from 0.1 to 100 Hz, the Tg values showed a positive shift in all cases. In a comparison of the three initiating systems (dicumyl peroxide, benzoyl peroxide, and azobisisobutyronitrile), the dicumyl peroxide system showed the highest modulus. The morphology of the IPNs was analyzed with transmission electron microscopy. The micrographs indicated that the system was nanostructured. An attempt was made to relate the viscoelastic behavior to the morphology of the IPNs. Various models, such as the series, parallel, Halpin–Tsai, Kerner, Coran, Takayanagi, and Davies models, were used to model the viscoelastic data. The area under the linear loss modulus curve was larger than that obtained by group contribution analysis; this showed that the damping was influenced by the phase morphology, dual‐phase continuity, and crosslinking of the phases. Finally, the homogeneity of the system was further evaluated with Cole–Cole analysis. © 2003 Wiley Periodicals, Inc. J Polym Sci Part B: Polym Phys 41: 1680–1696, 2003 相似文献
958.
I. V. Bodnar 《Technical Physics》2003,48(5):587-591
The thermal expansion coefficients and the thermal conductivity of Bridgman-grown crystals of CuGa1−x
InxTe2 solid solutions are investigated. It is found that the thermal expansion coefficient varies with x linearly, while the thermal conductivity is minimal when x=0.5. The Debye temperature and the rms dynamic atomic displacements are calculated from experimental data. It is shown that
the Debye temperature decreases and the rms displacements in the crystal lattice sharply increase as the In content in the
solid solutions grows. 相似文献
959.
Matthew H Ervin 《Microscopy and microanalysis》2003,9(1):18-28
The environmental cell device discussed in this paper provides a modest low-vacuum scanning electron microscopy (SEM) capability to a standard SEM without requiring additional pumping. This environmental cell confines a volume of low vacuum in contact with the sample surface using a container that has an aperture for admitting the primary electron beam. The aperture is large enough to permit a limited field of view of the sample, and small enough to limit the outflow of gas into the SEM chamber to that which can be accommodated by the standard SEM pumping system. This environmental cell also functions as a gaseous detector device. 相似文献
960.
E. Sh. Gutshabash 《JETP Letters》2003,78(11):740-744
The integration procedure based on the generalized Darboux transform is suggested for the Ishimori magnet model. Exact solutions are constructed for the model on the background of spiral structures. The possibility of phase transition in the system is hypothesized. 相似文献