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991.
992.
Jia‐Yuh Sheu Yeh‐Long Chen Cherng‐Chyi Tzeng Shu‐Lin Hsu Kuo‐Chang Fang Tai‐Chi Wang 《Helvetica chimica acta》2003,86(7):2481-2489
Certain 1‐ethyl‐ and 1‐aryl‐6‐fluoro‐1,4‐dihydroquinol‐4‐one derivatives were synthesized and evaluated for antimycobacterial and cytotoxic activities. Preliminary results indicated that, for 1‐aryl‐6‐fluoroquinolones, both 7‐(piperazin‐1‐yl)‐ and 7‐(4‐methylpiperazin‐1‐yl) derivatives, 9b and 11a , are able to completely inhibit the growth of M. tuberculosis at a concentration of 6.25 μg/ml, while the 7‐[4‐(2‐oxo‐2‐phenylethyl)piperazin‐1‐yl] derivative 13 exhibits only 31% growth inhibition at the same concentration. For 1‐ethyl‐6‐fluoroquinolones, both 7‐[4‐(2‐oxopropyl)piperazin‐1‐yl]‐ and 7‐[4‐(2‐oxo‐2‐phenylethyl)piperazin‐1‐yl]‐derivatives, 2a and 2b , respectively, show complete inhibition, while their 2‐iminoethyl and substituted phenyl counterparts 3a and 2c are less active. In addition, the 6,8‐difluoro derivative was a more‐favorable inhibitor than its 6‐fluoro counterpart ( 2b vs. 2d ). These results deserve full attention especially because 2a, 2b, 9b , and 11a are non‐cytotoxic at a concentration of 100 μM . Furthermore, compound 9b proved to be a potent anti‐TB agent with selective index (SI)>40 and an EC90 value of 5.75 μg/ml. 相似文献
993.
F. Tercero J. A. López Fernández E. García L. de Haro M. C. Carter A. Barcia B. Galocha J. L. Besada 《International Journal of Infrared and Millimeter Waves》2003,24(5):669-681
The Beam Mode Expansion (BME) approach for corrugated conical feed horn plus meniscus lens is presented. This approach is useful for providing the radiation pattern as it propagates through an optical system. A developed theoretical model has been verified measuring near and far field of a built horn and lens. These results have been used for designing the optical system of a Cassegrain antenna at 100GHz using the fundamental Gaussian beam mode (GBM) of the new approach. Multimode analysis has been performed with the pre-designed system in order to test the fundamental GBM results. 相似文献
994.
Felipe Cucker Steve Smale Ding-Xuan Zhou 《Foundations of Computational Mathematics》2004,4(3):315-343
We describe a model for the evolution of the languages used by the agents of a
society. Our main result proves convergence of these languages to a common
one under certain conditions. A few special cases are elaborated in more
depth. 相似文献
995.
Haihong Fang Binyuan Hu Lingshen Wang Rongli Lu Cui Yang 《Frontiers of Chemistry in China》2008,3(2):193-197
Nanometer MgO was prepared via a sol-gel auto-combustion technique using magnesium nitrate as raw material and citric acid
as chelating agent. IR spectra of the dried gel were used to investigate the structure of the precursors. By studying the
different TG curves of magnesium citrate gel prepared by different methods, we found that a combustion process occurred and
the nitrate ions acted as an oxidant in the combustion process. TEM photographs of synthesized powders from the sol-gel auto-combustion
showed that the crystallites were uniform in size. In addition, the XRD pattern of this sample showed that the particle size
was 8.9 nm. The BET curves, in turn, showed that the specific surface of the sample was 26.34 m2/g. The mechanism of the frothing process in restraining agglomeration is discussed.
__________
Translated from Journal of East China Normal University (Natural Science), 2007, (2): 52–57 [译自: 华东师范大学学报(自然科学版)] 相似文献
996.
在齐次Morrey-Herz空间上建立了高阶交换子~$T^{m}_{b,l}$ 和 ~$M^{m}_{b,l}$的有界性,其中~$T^{m}_{b,l}$ 和 ~$M^{m}_{b,l}$ 是由分数次积分算子和分数次极大算子分别与~BMO($R^{n}$)函数生成的高阶交换子. 相似文献
997.
Frictionless indentation responses of transversely isotropic piezoelectric film/rigid substrate systems under circular cylindrical indenter (i.e., punch), conical indenter (i.e., cone), and spherical indenter (i.e., sphere) are investigated. Both insulating and conducting indenters are considered. The technique of Hankel transformation is employed to derive the corresponding dual integral equations for the mixed boundary value indentation problems. For the two limiting cases of infinitely thick and infinitely thin piezoelectric films, closed-form solutions are obtained. For piezoelectric films of finite thickness, a numerical method is constructed to solve the dual integral equations and semi-empirical models having only two unknown parameters are proposed for the responses of indentation force, electric charge and electric potential, and contact radius. With the two parameters inferred from the numerical results, the semi-empirical formulae are found to provide good estimates of the indentation responses for the two limiting cases of infinitely thick and thin piezoelectric films, as well as those in between. The inferred parameters in the proposed semi-empirical formulae for normalized indentation force and electric charge are checked against four different piezoelectric materials and are found to be insensitive to the selection of piezoelectric materials. It is believed that the proposed semi-empirical indentation formulae are useful in developing experimental indentation techniques to extract the material properties of piezoelectric films. 相似文献
998.
Tie-Jun Liu Yue-Sheng Wang Chuanzeng Zhang 《Archive of Applied Mechanics (Ingenieur Archiv)》2008,78(4):267-282
The main interest of this study is a new method to solve the axisymmetric frictionless contact problem of functionally graded
materials (FGMs). Based on the fact that an arbitrary curve can be approached by a series of continuous but piecewise linear
curves, the FGM is divided into a series of sub-layers with shear modulus varying linearly in each sub-layer and continuous
at the sub-interfaces. With this model, the axisymmetric frictionless contact problem of a functionally graded coated half-space
is investigated. By using the transfer matrix method and Hankel integral transform technique, the problem is reduced to a
Cauchy singular integral equation. The contact pressure, contact region and indentation are calculated for various indenters
by solving the equations numerically.
An erratum to this article can be found at 相似文献
999.
利用熔融KOH和Co3O4在较低温度(480℃)下反应制备出K0.36CoO2,然后用高锰酸钾溶液和饱和的过硫酸钾溶液进行氧化处理.氧化的同时伴随有水分子嵌入.K0.36CoO2用高锰酸钾和过硫酸钾溶液处理后分别得到K0.12CoO2·0.8H2O和K0.16CO2·0.6H2O.这两种化合物都属于六角晶系,表现出金属行为,脱水后主相变为正交结构并且呈现出半导体特性.K0.16CoO2·0.6H2O在56K附近可能存在自旋玻璃转变行为或其他涨落.随着钾含量的减少和水含量的增多,样品的自旋玻璃行为受到抑制或发生磁性相分离.样品K0.12CoO2·0.8H2O在零场冷却和有场冷却曲线上的分叉现象基本上消失.还讨论了产生KxCoO2与NaxCoO2体系结构和物性差别的原因. 相似文献
1000.
A variety of aromatic amines are oxidized to their corresponding quinones in excellent yields by supported iodic acid under microwave irradiation and solvent free conditions. 相似文献