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61.
明确从地胆草中分离得到的两对牦牛儿内酯型的立体异构体即地胆草种内酯(scabertopin)、异地胆草种内酯(isoscabertopin)、异去氧地胆草内酯(isodeoxyelephantopin)和去氧地胆草内酯(deoxyelephantopin)的C-2相对构型;方法 NOESY技术,并结合这4个化合物的1H NMR,13C NMR,HMQC谱;结果 两对立体异构体的NOESY谱有明显差异;结论 通过分析NOESY谱,找寻H-1相关信息,若发现H-1与H-8,H-9β和14-CH3有NOE相关,可以判断化合物的C-2为α构型,若H-1与H-5,H-7,H-3α及H-9α之间有NOE相关,则化合物的C-2为β构型. 相似文献
62.
63.
Nongelatin dichromated holographic film(NGD) is a new holographic recordingmaterial.Holograms recorded on this material have better environmental stability, higherdiffraction efficiency and stronger real time effect, etc..An experimental study to ascertainthe influence of two electron donors, namely,N,N-dimethylformamide(DMF) and dimethyl-sulfoxide(DMSO),on the real time diffraction efficiency(RTDE) of NGD holograms is car-ried out.The pressence of electron donors not only improves the sensitivity,but also enhancesthe real time effect greatly.RTDE of above 60% at±1 orders of NGD plane transimissiongrating is achieved by introducing electron donors. 相似文献
64.
X.X. Guo 《Surface science》2004,549(3):211-216
We studied parallel conductivities of pure BaF2 films with thicknesses ranging from 35 to 300 nm, epitaxially grown on Al2O3(0 1 2) substrates by molecular beam epitaxy technique. The overall conductivities of the films are found to increase with decreasing thickness. The detailed investigation of the overall conductance as a function of the thickness permits the deconvolution of bulk and boundary effects, the latter being attributed to distinct space charge effects in the interface between BaF2 film and Al2O3 substrate. The (extrinsic) Debye length (λ) is estimated to be about 8 nm at T=593 K, which corresponds to an impurity content of 1018/cm3 (singly ionized dopant assumed). This is consistent with the fact that we observed a constant boundary contribution for all investigated films (film thickness >4λ). It is also consistent with the Debye length observed in a previous report on CaF2/BaF2 heterolayers fabricated by the same technique, in which the low temperature enhancement was also attributed to space charges in BaF2 [Nature 408 (2000) 946]. Only at low temperatures (below 370 °C), the conductance seems to be influenced by strain effect. 相似文献
65.
In this paper, we study the homogenous quotient modules of the Hardy module on the bidisk. The essential normality of the
homogenous quotient modules is completely characterized. We also describe the essential spectrum for a general quotient module.
The paper also considers K-homology invariant defined in the case of the homogenous quotient modules on the bidisk.
This work is partially supported by the National Natural Science Foundation of China (Grant No. 10525106), the Young Teacher
Fund, the National Key Basic Research Project of China (Grant No. 2006CB805905) and the Specialized Research for the Doctoral
Program 相似文献
66.
Yen-Shung TSAI 《中国科学A辑(英文版)》2007,50(7):1026-1034
By means of further investigation of solid codes,the problem“Is every fd-domain uni- formly dense”proposed by Yuqi Guo,C.M.Reis and G.Thierrin in 1988 is solved in this paper. 相似文献
67.
关于《一类奇异边值问题的正解》的注记 总被引:3,自引:0,他引:3
文[4]通过构造反例断言文[1]中定理的必要性证明有误,本文首先指出文[4] 的这个断言不正确,然后对文[4]中定理2.1作了本质性的改进. 相似文献
68.
给出目标信息系统学习的多准则决策方法,建立多准则决策的规则学习模型,讨论该模型的性质。该模型优于Z.Pawlak方法,将规则提取与信息融合为一体。也优于AHP等模型,具有简洁性.通过实例计算,取得了满意结果。 相似文献
69.
A subgroup H of a finite group G is said to have the semi cover-avoiding property in G if there is a normal series of G such that H covers or avoids every normal factor of the series. In this paper, some new results are obtained based on the assumption that some subgroups have the semi cover-avoiding property in the group. 相似文献
70.
By introducing an imaginary space transform curvature ρs, a complex space called Riemannian space is constructed, in which the light propagating in free space has the trajectory
of straight line while propagating. Moreover, this curvature couples with that of the wave front of the paraxial beam ρw, and therefore a complex curvature ρc is constructed, which can be employed to investigate the behavior of the light transmission and to generalize the ABCD law.
Project supported by the National Hi-Tech Inertial Confinement Fusion Committee, the Guangdong Natural Science Foundation
the Postdoctoral Foundation of Guangdong and National Postdoctoral Foundation of China. 相似文献