46．7MeV／A~（12）C轰击~（159）Tb、~（197）Au和~（209

用４６．７ＭｅＶ／Ａ１２Ｃ轰击１５９Ｔｂ、１９７Ａｕ和２０９Ｂｉ，测量关联裂片的速度和角度．研究了线动量转移、质量和出平面角分布，提取了核温度．应用级联两体统计衰变理论进行了拟合与解释，结果表明：在入射能约为５０ＭｅＶ／Ａ的中能重离子碰撞中，以非完全熔合方式形成了核温度高达４－５ＭｅＶ的类复合核，其后通过裂变、蒸发级联统计两体衰变而退激．     

Emission Time Measurements of Light Particles from 40Ar+197Au Collisions in Intermediate Energies

Particle-particle correlation functions have been measured for ⁴⁰Ar+¹⁹⁷Au collisions at E=25 MeV/u.Emission time of light particles has been extracted from correlation functions using the three-body trajectory model.The average emission time varies with the energy of particles. It decreases from about 300 fm/c for low energy particles to about 100fm/c for energetic particles.     

Theoretical analysis of double-differential neutron emission cross sections for n+~(56)Fe reactions at incident energies of 7-13 MeV

The double-differential neutron emission cross sections for n+⁵⁶Fe reactions at incident energies of 7-13 MeV at different angles are calculated by the UNF (abbreviation for unified, 2009 Version) code, which is based on the unified Hauser-Feshbach and exciton model. The results indicate that the higher the incident energies, the better the results, although there are some discrepancies between the calculated results and the measured data for natural iron. These discrepancies are analyzed in detail in this paper. In addition, the calculated results are also compared with the evaluated results of ENDFB Ⅶ.0 and JEFF-3.1.1 near the angle of 90° at incident energies of 8.17 and 11.5 MeV, respectively.     

Semiconvergence of parallel multisplitting methods for symmetric positive semidefinite linear systems

In this paper we construct some parallel relaxed multisplitting methods for solving consistent symmetric positive semidefinite linear systems, based on modified diagonally compensated reduction and incomplete factorizations. The semiconvergence of the parallel multisplitting method, relaxed multisplitting method and relaxed two‐stage multisplitting method are discussed. The results generalize some well‐known results for the nonsingular linear systems to the singular systems. Copyright © 2010 John Wiley & Sons, Ltd.     

酸溶ICP—AES法测定岩石,土壤样品中的硼

磷酸与许多金属有很强的络合能力，生成的磷酸盐在一定的ｐＨ值范围内易生成沉淀。本方法的特点是利用混合酸分解样品，以元素的磷酸盐沉淀分离样品中大量元素，然后用ＩＣＰ－ＡＥＳ法测定。本方法适用于岩石，土壤样中硼的测定，其检出限０．８ｎｇ／ｍＬ。     

聚马来松香乙二醇酯Cu(II)配合物固定化漆树漆酶的研究

制备了聚马来松香乙二醇酯(MEEP)Cu2 、Ni2 、Ca2 和Mg2 金属离子配合物,并分别以4种配合物为载体固定化漆树漆酶,初步探讨了反应时间对酶固定化的影响,考察了固定化酶的性质。实验结果表明,在反应温度为25℃条件下,漆树漆酶的最佳固定化时间为16h;MEEPCu2 配合物固定化酶的固定化结果较好,重复使用6次后,酶相对保留活力为55.0%;该固定化酶的最适作用温度为40℃,pH值范围为5.89~9.23,固定化漆树漆酶具有比游离酶更好的热稳定性和更广泛的pH值适用范围。     

Formulation optimization and in situ absorption in rat intestinal tract of quercetin-loaded microemulsion

A new microemulsion system has been developed to increase the solubility and oral absorption of quercetin, a poorly water-soluble drug. The formulation of quercetin-loaded microemulsion was optimized by a simplex lattice experiment design. The optimized microemulsion formulation consisted of oil (7%, w/w), surfactant (48%, w/w), and cosurfactant (45%, w/w). Under this condition, the mean droplet diameter of microemulsion was 38.9 nm and solubility of quercetin in the microemulsion was 4.138 mg/ml. The in situ absorption property of quercetin-loaded microemulsion in rat intestine was studied and the results showed there was significant difference in absorption parameters such as K_a, t_1/2 and uptake percentages between microemulsion and micelle solution containing quercetin. The study on absorption percentage in different regions of rat intestine attested that the colon had the best permeability, followed by ileum, duodenum in order. It can be concluded that microemulsion can improve the solubility and oral absorption of quercetin, a poorly water-soluble drug.     

稀土Eu掺杂PtRu/C催化剂及其对甲醇电氧化的性能

采用化学还原和热处理方法对商业PtRu/C催化剂进行稀土Eu掺杂,制备了不同Eu含量的PtRuEux/C催化剂.透射电子显微镜(TEM)、X射线能量色散光谱(EDX)、X射线衍射(XRD)和X射线光电子能谱(XPS)等方法表征催化剂的结果表明,Eu的掺杂未改变PtRu/C催化剂的平均粒径(约为3nm),并且Eu以金属和氧化物两种形态修饰PtRu表面.循环伏安和计时电流法测试显示,PtRuEux/C催化剂较商业PtRu/C对甲醇氧化具有更高的活性,其中PtRuEu0.3/C的活性最高.运用原位傅里叶变换红外(FTIR)光谱从分子水平研究了该催化剂对甲醇电催化氧化的反应过程,检测到甲醇在催化剂上解离吸附的吸附态产物是线型吸附态CO(COL),Eu的掺杂使COL的氧化电位降低,明显提高了催化剂的活性和抗CO毒化的能力.     

Asymmetric multifractal scaling behavior in the Chinese stock market: Based on asymmetric MF-DFA

We utilized asymmetric multifractal detrended fluctuation analysis in this study to examine the asymmetric multifractal scaling behavior of Chinese stock markets with uptrends or downtrends. Results show that the multifractality degree of Chinese stock markets with uptrends is stronger than that of Chinese stock markets with downtrends. Correlation asymmetries are more evident in large fluctuations than in small fluctuations. By discussing the source of asymmetric multifractality, we find that multifractality is related to long-range correlations when the market is going up, whereas it is related to fat-tailed distribution when the market is going down. The main source of asymmetric scaling behavior in the Shanghai stock market are long-range correlations, whereas that in the Shenzhen stock market is fat-tailed distribution. An analysis of the time-varying feature of scaling asymmetries shows that the evolution trends of these scaling asymmetries are similar in the two Chinese stock markets. Major financial and economical events may enhance scaling asymmetries.     

兔红细胞的共振散射光谱研究

研究了液相兔血红细胞的共振散射光谱 (RSS)及非线性分频散射和倍频散射。兔红细胞浓度在0 0 15～ 31 1× 10 6个·(mL) -1范围与共振散射光强度成线性关系。对非线性散射机理进行了探讨。