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931.
双(十二烷基亚磺酰)乙烷溶剂萃取钯及其机理的研究   总被引:2,自引:0,他引:2  
李焕然  许洪民 《分析化学》1994,22(7):702-705
本文研究用双(十二烷基亚磺酰)乙烷萃取钯的性能,在KI存在下从7mol/L盐酸介质中用含有BDSE的氯仿能定量萃取钯,有机的钯可被硫脲或氨溶液反萃继之用TMK-TritonX-100光度法测定,研究了萃取的最佳条件及干扰情况,斜率法测得萃合物组成为Pd:I:BDSE=1:2:1,红外光谱证实萃合物中BDSE的二个亚砜以硫原子与钯配位,萃合物为异位体络合物,提出了选择性萃取分离钯的新方法。  相似文献   
932.
A Kind of direct methods is presented for the solution of optimal control problems with state constraints.These methods are sequential quadratic programming methods.At every iteration a quadratic programming which is obtained by quadratic approximation to Lagrangian function and Linear approximations to constraints is solved to get a search direction for a merit function.The merit function is formulated by augmenting the Lagrangian funetion with a penalty term.A line search is carried out along the search direction to determine a step length such that the merit function is decreased.The methods presented in this paper include continuous sequential quadratic programming methods and discreate sequential quadrade programming methods.  相似文献   
933.
In this paper,the super-inverse iterative method is proposed to compute the accurateand complete eigen-solutions for anti-plane cracks/notches with multi-materials,arbitrary opening an-gles and various surface conditions.Taking the advantage of the knowledge of the variation forms ofthe eigen-functions,a series of numerical techniques are proposed to simplify the computation andspeed up the convergence rate of the inverse iteration.A number of numerical examples are given todemonstrate the excellent accuracy,efficiency and reliability of the proposed approach.  相似文献   
934.
具有离散参数齐次随机场的线性预测(V)   总被引:1,自引:1,他引:0  
本文提出并研究下列四类线性预测问题:2(n0),6(n0),5(NO,n0)及3(N0,n0).不仅求出了它们的预测误差,而且也求出了它们的预测值.因而不仅推广了而且也改进了[2-5]中的结果.本文还给出了场{X(m,n)}的一个新形式的表示式.  相似文献   
935.
Zr—K—Fe/ZSM—48催化剂中锆的作用   总被引:1,自引:0,他引:1  
  相似文献   
936.
本文对四个主要麦芽品质性状—a一淀粉酶活力、麦芽汁粘度、麦芽汁色度和搪化力进行了杂种优势和相关分析.(1)相对优势结果表明,在84个组合次中,呈正向优势的46个,占54.76男,负向优势34个,占40.48男,无显性4个,占4.75男;(2)四个品质性状的中亲优势平均值分别为一6.117、一9.965 40.452和一。.545s a-淀粉酶活力和糖化力的超高亲优势分别为一14.578和一8.201,麦芽汁粘度和色度的超低亲优势分别为5.442和70.455.四个性状杂种优势的变异系数均很大.(3)麦芽汁色度的F,对MP的回归系数(B)和相关系数(r)均达显著水平,分别为。..43和0.50,麦芽汁粘度的相关系数达显著水平,为一。.45,其余均未达显著水平,(4)除麦芽汁色度性状外,另三个性状的中亲优势、超亲优势和特殊配合力的相关均达显著或极显著水平.(5)四个麦芽品质性状间的相关结果表明,仅有a-淀粉酶活力和麦芽汁粘度间呈极显著负相关(r=一0.56').最后,文章根据实验结果,就啤酒大麦麦芽品质改良的遗传育种及其杂种优势应用进行了初步讨论.  相似文献   
937.
This paper reports the results of a survey intended to discover the extent to which Checkland's Soft Systems Methodology (SSM) is used in practice. Some 300 questionnaires were sent to people who had had some exposure to SSM and, surprisingly, nearly half were returned. The majority described in detail their uses of SSM and most felt that it had been successful. This paper describes the overall quantitative results from the survey as well as presenting a qualitative analysis of the experiences of using SSM.  相似文献   
938.
We have demonstrated a temperature switch based on an optically bistable device integrated with an optical fibre. The principle demonstrated here might lead to the development of new types of all-optical temperature sensors.  相似文献   
939.
The main purpose of this paper is to give a procedure to “mollify” the low-pass filters of a large number ofMinimally Supported Frequency (MSF) wavelets so that the smoother functions obtained in this way are also low-pass filters for an MRA. Hence, we are able to approximate (in the L 2 -norm) MSF wavelets by wavelets with any desired degree of smoothness on the Fourier transform side. Although the MSF wavelets we consider are bandlimited, this may not be true for their smooth approximations. This phenomena is related to the invariant cycles under the transformation x ↦2x (mod2π). We also give a characterization of all low-pass filters for MSF wavelets. Throughout the paper new and interesting examples of wavelets are described.  相似文献   
940.
Traditional inventory models assume that a buyer places one order with a supplier in each order cycle. A large number of researchers have studied the benefits of dual sourcing such that an order quantity is split and placed simultaneously with two suppliers. We show that many of the benefits of dual sourcing are due to order splitting rather than using two suppliers. We investigate order splitting with one supplier such that the first part of the order is sent out immediately but the second part of the order is released later (scheduled-release). Through extensive computational results, we show that in many situations where dual sourcing or the use of a cheaper supplier would be cost effective, single sourcing with order splitting using scheduled-release orders is better. The paper provides a quantitative rationale to continue with one supplier. We also summarize the qualitative reasons to prefer single sourcing or multiple sourcing.  相似文献   
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