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排序方式: 共有331条查询结果,搜索用时 15 毫秒
31.
32.
Hui H. Chin Leonid V. Azroff Agya R. Saini Robert W. Lenz 《Journal of Polymer Science.Polymer Physics》1989,27(10):2001-2009
Semiflexible thermotropic aromatic polyesters with lateral groups were aligned magnetically and mechanically in monodomains after separation into high-molecular-weight (polymer) and low-molecular-weight (oligomer) fractions. Based on the x-ray intensity distributions recorded for a series of seven different substituents in the arylsulfonyl substituted group, a novel smectic structure was determined for H, F, Cl, OCH3, and CH3 in the para position while a normal nematic alignment prevailed when it contained Br or NO2. 相似文献
33.
C. Baiocchi G. Saini P. L. Bertolo C. Carpenito E. Marengo D. Giacosa 《Chromatographia》1990,29(7-8):355-362
Summary The RP-HPLC technique has been applied to the analysis of the flavonoid content of leaf extracts from various genotypes ofPopulus nigra andPopulus deltoides and from several of their hybrids. Two elution procedures different either as regards gradient program or the type of organic modifier used were checked to optimize the reliability of the results obtained. Before making any identification, the chromatographic profiles proved so typical of each species as to allow of their use as fingerprints in this type of taxonomic problem. Individual identifications were carried out by spiking real samples with known amounts of standard substances. The presence of flavonoid compounds previously identified was confirmed and a few new identifications were proposed. 相似文献
34.
The preparation of some novel 3-(arylideneamino)-3a,8a-dihydroxy-1,3,3a,8a-tetrahydroindeno[1,2-d]imidazole-2,8-diones 8(i–xiv) and 3-(arylideneamino)-3a,8a-dihydroxy-2-thioxo-1,3,3a,8a-tetrahydroindeno[1,2-d]imidazol-8(2H)-ones 9(i–xiv) have been reported through one-pot catalyst-free reaction of aldehydes, semicarbazide hydrochloride/thiosemicarbazide with ninhydrin. All the synthesized compounds have been screened for antimicrobial activity and some of them were observed to possess broad spectrum antibacterial potential as well as significant antagonistic potential against fungal pathogens. 相似文献
35.
S. Songara M.K. Patra M. Manoth L. Saini V. Gupta G.S. Gowd S.R. Vadera N. Kumar 《Journal of photochemistry and photobiology. A, Chemistry》2010,209(1):68-73
Pure and (0.5–3 at%) vanadium doped TiO2 nanoparticles have been synthesized by wet chemical method. The as synthesized materials have been characterized by using XRD, atomic force microscope (AFM), Raman, EPR and UV–vis spectroscopy techniques. From XRD studies, both pure as well as vanadium doped TiO2 have been found to show pure anatase phase. The value of lattice constant c is smaller in doped TiO2 as compared to undoped and has been found to decrease with increase in vanadium concentration. AFM studies show formation of spherical particles with particle size ~23 nm in all the samples. Photochromic behavior of these materials has been studied by making their films in alkyd resin. Vanadium doped TiO2 films show reversible change in color from beige-yellow to brownish violet on exposure to UV light. The mechanism of coloration and bleaching process has been discussed. 相似文献
36.
Nirmala Saini 《Optics Communications》2011,284(3):756-763
Biometric systems are gaining importance because of increased reliability for authentication and identification. A biometric recognition technique has been proposed earlier, in which biohashing code has been generated by using a joint transform correlator. The main drawback of the base biohashing method is the low performance of the technique when an “impostor” steals the pseudo-random numbers of the genuine and tries to authenticate as genuine. In the proposed technique, soft biometrics of the same person has been used to improve the discrimination between the genuine and the impostor populations. The soft biometrics are those characteristics that provide some information about the individual, but lack the distinctiveness and permanence to sufficiently differentiate between any two individuals. In the enrolment process, biohash code of the target face images has been integrated with the different soft biometrics of the same person. The obtained code has been stored for verification. In the verification process, biohash code of the face image to be verified is again diffused with the soft biometric of the person. The obtained code is matched with the stored code of the target. The receiving operating characteristic (ROC) curve and the equal error rate (EER) have been used to evaluate the performance of the technique. A detailed study has been carried out to find out the optimum values of the weighting factor for the diffusion process. 相似文献
37.
Mukesh G. Nayak L.K. Saini 《Physica E: Low-dimensional Systems and Nanostructures》2011,44(1):196-201
We study the effect of finite width on the ground-state of a spin-polarized electron–electron quantum bilayers (EEBL) system at temperature T=0. Correlations among carriers are treated beyond the static mean-field theories by using the quantum or dynamical version of Singwi, Tosi, Land and Sjölander (qSTLS) theory. Numerical results are presented for the pair-correlation function, the ground-state energy, the static density susceptibility, and the static local-field correction factor as a function of density parameter rsl and interlayer spacing d. Interestingly, we find that the inclusion of finite width lowered the critical density, for the onset of Wigner crystal (WC) ground-state, as compared to the similar recent study of spin-polarized EEBL system without finite width effect. Further, spin-polarization effect is seen to introduce a marked change in the ground-state energy of the EEBL system as compared to the results of unpolarized EEBL system with finite width. Results of ground-state energies are also compared with the recent diffusion Monte Carlo (DMC) and variational Monte Carlo (VMC) simulation studies of spin-polarized EEBL system with zero width. 相似文献
38.
R.K. Bhan Raghvendra Sahai Saxena N.K. Saini L. Sareen R. Pal R.K. Sharma 《Infrared Physics & Technology》2011,54(5):379-381
Hg1−xCdxTe Metal–Insulator–Semiconductor (MIS) capacitors were studied both experimentally and theoretically to investigate the capacitance contributions due to band-to-band (btb) tunnelling and generation–recombination (gr) of carriers to inversion layer capacitance. A good fit to the data has been obtained by including the btb contributions rather than gr contributions. 相似文献
39.
R. Albrecht T. C. Awes P. Beckmann F. Berger M. A. Bloomer D. Bock R. Bock G. Claesson G. Clewing L. Dragon A. Eklund R. L. Ferguson A. Franz S. Garpman R. Glasow H. Å. Gustafsson H. H. Gutbrod M. Hartig G. Hölker J. Idh P. Jacobs K. H. Kampert B. W. Kolb P. Kristiansson H. Löhner I. Lund F. E. Obenshain A. Oskarsson I. Otterlund T. Peitzmann S. Persson F. Plasil A. M. Poskanzer M. Purschke H. G. Ritter B. Roters S. Saini R. Santo H. R. Schmidt R. Schmidt S. P. Sørensen K. Steffens P. Steinhauser E. Stenlund D. Stüken M. L. Tincknell A. Twyhues G. R. Young 《Zeitschrift fur Physik C Particles and Fields》1992,53(2):225-237
Correlations between positive pions are investigated in the target fragmentation region of 200A GeV16O+nucleus collisions. The pions are measured with the Plastic Ball detector in the WA80 experiment at the CERN SPS. The target mass dependence of the radii and the correlation strength extracted by interferometry is studied. A new approach to the fit of the correlation function is introduced. The correlation strength and both invariant and transverse radii increase with decreasing target mass. The transverse radius for16O+C reactions appears to be much larger than the geometrical radius of the nuclei involved. For the Au target only a small fraction of the measured pions contributes to the apparent correlation. Hints for a much larger second component in16O+Au reactions are observed. Rescattering phenomena may provide a clue to understand these phenomena. 相似文献
40.
A Convenient and Facile Synthesis of Isoxazolyl‐chromeno[4,3,2‐de]pyrimido[4,5‐h][1,6]napthyridinones
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Eligeti Rajanarendar Saini Ramakrishna Baireddy Kishore 《Journal of heterocyclic chemistry》2014,51(5):1415-1420
The ceric ammonium nitrate‐catalyzed synthesis of (E)‐5‐amino‐N‐(3‐methyl‐5‐styrylisoxazol‐4‐yl)‐2‐arylchromeno[4,3,2‐de][1,6]napthyridin‐4‐carboxamides 5 was simply achieved upon the one‐pot four‐component reaction of isoxazolyl cyanoacetamide 1 with malononitrile 2 , 2‐hydroxy acetophenone 3 , and aromatic aldehydes 4 in ethanol. Compounds 5 on heating with acetic anhydride underwent tandem N‐acetylation and cyclocondensation involving intramolecular cyclization to afford the title compounds (E)‐11‐methyl‐12‐(3‐methyl‐5‐styrylisoxazol‐4‐yl)‐2‐arylchromeno[4,3,2‐de][1,6]napthyridin‐13(12H)‐ones 6 in good yields. The chemical structures have been confirmed by analytical and spectral analyses. 相似文献