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介绍了液态锂回路中的净化及在线检测装置。该装置采用了冷阱法和热阱法,使回路中产生的C、O、N和氢同位素等杂质降至10wppm以下。目前,已经利用四电极测电阻法测量了放锂前后的电阻随温度的变化曲线,再经过多项式拟合,计算得到了纯锂的电阻率随温度变化的函数。     

Theoretical Calculations for Structural, Elastic and Thermodynamic Properties of MgB2 under High Pressure

We have investigated the structural and elastic properties of MgB₂ under high pressures using the full-potential linearized muffin-tin orbital (FP-LMTO) scheme within the generalized gradient approximation correction (GGA) in the frame of density functional theory. The calculated pressure dependence of the normalized volume is in excellent agreement with the experimental results. At the same time the elastic constants and acoustic anisotropy as a function of applied pressure are presented. Through the quasi-harmonic Debye model, we also investigate the thermodynamic properties of MgB₂.     

First-Principle Calculations for Thermodynamic Properties of LiBC Under High Temperature and High Pressure

The thermodynamic properties of LiBC are investigated by using the full-potential linearized muffin-tin orbital method (FP-LMTO) within the frame of density functional theory (DFT) and using the quasi-harmonic Debye model. The dependencies of the normalized lattice parameters a/a0 and c/c0, the ratio (c/a)/2, the normalized primitive volume V/V0 on pressure and temperature are successfully obtained. It is found that the interlayer covalent interactions (Li-B bonds or Li-C bonds) are more sensitive to temperature and pressure than intralayer ones (B-C bonds), as gives rise to the extreme lattice anisotropy in the bulk hcp LiBC.     

高密度氢气的分子间相互作用与状态方程

本文从高密度氢气的分子间相互作用出发进行分析,在修改范德瓦耳方程的基础上,提出了一种新的适用于高密度氢气的状态方程,并用来系统地计算了氢气在临界区的等温压缩线.在缺乏实验数据的情况下,这些理论计算结果很有用.     

冷轧低碳钢高压相变组织的透射电镜分析

 对冷轧低碳钢在高压下进行再结晶,用透射电子显微镜（TEM）分析高压相变组织,发现压力可以使再结晶晶粒细化;压力升高,具有体心立方结构的普通低碳钢可形成ε-马氏体,并根据电子衍射花样的计算确定ε-马氏体的晶格参数。     

阴极不同进气对PEMFC性能影响的实验研究

针对阴极通纯氧气或空气两种情况,实验研究了温度及化学计量比的变化对反应面积为9 cm2、具有平行流场的PEMFC性能的影响.结果表明:升高电池温度可提高PEMFC的性能及极限电流密度;在本实验条件下,为提高电池性能,阴极通纯氧时,阳极化学计量比/阴极化学计量比应高于1.5/3.0,通空气时,两者之值应高于3.0/6.0;相对于阴极通空气的情况,阴极通氧气时电池性能显著提高,故在条件允许的前提下应尽量以纯氧作为氧化气体.     

高温高压气体的状态方程与热力学性质

本文根据高温高压下气体分子要压缩的观点出发,提出了一个简单实用的高温高压气体状态方程,并用以研究和计算气体在高温高压下的热力学函数与性质.     

The crystal change and "excess heat" produced by long time electrolysis of heavy water with titanium cathode

According to the theory given in the paper[1], the long time electrolysis experiment with titanium cathode in heavy water (D2O) were done for many times by using the open-loop multi-parameters electrolysis calorimetry system, which is established by us. The specialty is that the cathode is titanium rod and the anode is platinum wire. The early experiment result[3] is still repeated in our recent experiment. The obvious "excess heat" phenomenon can take place only when the electrolysis last more than ten days and amount of "excess heat" increased with the electrolysis time. The "excess heat" can also be obtained from the "boiling to dry" experiment. In the recent experiment, we obtain the results that the amount of "excess heat" is about 3.6 times the input energy, the "excess heat" power is 76.5 W, and the "excess heat" power density is 121.7 W/cm3. After the electrolysis, the crystal structure of the Ti cathode was measured with x-ray diffraction apparatus. We found that the crystal structure of Ti cathode was changed to face-centered cubic structure of TiD2 from its hexagonal structure. This result is in agreement with the Gou's theory mentioned in reference[1].     

35MeV/u 40Ar+197Au反应中复合核的激发能与温度

利用大面积位置灵敏气体探测器对35MeV/u ⁴⁰Ar+¹⁹⁷Au反应中形成的裂片进行了符合测量,由此得到了裂变复合核的速度分布.在大质量转移假设下扣除前平衡发射粒子的影响,得到复合核的激发能.另外利用望远镜探测器对反应中出射的轻带电粒子也进行了符合测量,并由后角α,p,d,t的能谱提取了复合核的温度.温度与激发能的关系没有表现出理论预言的相变特征.     

蔬菜中铁含量的测定及方法比较

用分光光度法直接测定蔬菜中铁的含量,方法简便、快速、准确.分别采用浓盐酸和浓硫酸两种消解方法对样品进行处理,并对其测定结果进行比较,实验结果表明,浓硫酸消解法消解能力更强,测定更为准确.5种蔬菜中木耳铁含量最高,对指导人们合理食用蔬菜进行补铁及进一步开发蔬菜产品提供了可靠的理论依据.