新型低beta超导腔调谐算法分析与测试

为了使腔体在复杂电磁环境下处于谐振状态,保持超导腔加速电压的幅度相位稳定,研发了一种应用于自激锁相模式的腔体新型调谐算法。利用正交电压Q值控制调谐器调谐,从而消除了输入和输出间的相位误差,给出了理论推导过程与该算法的可靠性分析。该算法已应用于中国科学院近代物理研究所ADS项目超导加速器中,简化了传统控制模式中的信号采样数量,提高了系统控制精度与抗干扰能力,使腔体克服了在调谐过程中由于功率上冲引起的氦压波动。保证了超导腔在工作状态下,频率稳定在162.5 MHz,频率误差小于17 Hz。For the purposes of keeping the resonant cavity steady in a complex electromagnetic environment and maintaining stable amplitude and phase, a new tuning algorithm for superconducting RF cavity operated in self-excited phase-locked mode has been developed. The quadrature voltage was employed to control the tuner under the phase-locked condition, so as to eliminate phase measurement between the input and the output. This paper demonstrates the principle of this "Minimum Q" tuning algorithm and presents an analysis of the stability of the system. The algorithm is applied to the superconducting accelerator of the Institute of Modern Physics' ADS project. The "Minimum Q" tuning algorithmnot only simplifies the number of signal sampling but also improves the control accuracy and anti-interference ability of the system, while enables the cavity to overcome the helium pressure fluctuation which caused by power overshoot. It ensures that the frequency of the superconducting cavity is stable at 162.5 MHz, and the frequency error is less than 17 Hz.     

高效液相色谱测法测定家蚕酪氨酸羟化酶活性

建立了HPLC-紫外检测法快速测定家蚕酪氨酸羟化酶活性的方法。采用的色谱柱为Venusil XBP C18(4.6 mm×100 mm,5μm),流动相pH为3.5,流速0.5 mL/min,紫外检测波长280nm,柱温30℃。L-多巴在0.1～100μg/mL范围内线性良好,r=0.9991(n=6),L-多巴最低检测限是0.02μg/mL(S/N≥3),日内、日间相对标准偏差(RSD)在3.1%～12%之间,样品回收率在89%～104.6%之间。该方法可用于昆虫酪氨酸羟化酶(TH)活性测定。     

钴原子团簇电子结构的理论研究

应用多重散射自治场理论对钴原子团簇(N=3—13)的电子结构进行了理论研究.通过电离阈值在不同构型、不同组态的理论值与实验值的对比,初步探讨了合适的电子组态及团簇构型.根据电子组态的局域3d价电子布局,发现钴团簇的平均原子磁矩,总体来说随原子数增加而下降.根据团簇构型,推测了钴原子团簇的稳定性及多种生长方式. 关键词：     

Controlled Evolution of Silicon Nanocone Arrays Induced by Ar+ Sputtering at Room Temperature

Controlled evolution of silicon nanocone arrays induced by Ar^＋ sputtering at room temperature, using the coating carbon as a mask, is demonstrated. The investigation of scanning electron microscopy indicates that the morphology of silicon nanostructures can be controlled by adjusting the thickness of the coating carbon film. Increasing the thickness of the coating carbon film from 50-60 nm, 250-300 nm and 750-800 nm to 1500 nm, the morphologies of silicon nanostructures are transformed from smooth surface ripple, coarse surface ripple and surface ripple with densely distributed nanocones to nanocone arrays with a high density of about 1 × 10^9- 2 × 10^9 cm^-2.     

The Carrier-Envelope Phase of Focused Few-Cycle Laser Pulses

The Gouy phase shift modulates the carrier-envelope phase of a focused few-cycle laser pulse. We investigate the variations of the carrier-envelope （CE） phase of a pulsed Gaussian beam on and off the axis by the first-order approximation and numerical calculation. The CE phase undergoes a π shift from minus infinity to infinity, and it changes fastest with distance at the focus. The variation of CE phase on propagation distance is nearly independent of pulse duration At when At is greater than lO fs and the first order approximation fits this result very well. The maximum difference of CE phase between a pulse with duration of one cycle and the result of first-order approximation is 0.09.     

导纳谱研究两类Si基量子阱基态子能级的性质

用导纳谱技术研究了两类Si基量子阱样品基态子能级的性质.基于量子阱中载流子的热激发模型，从导纳谱中得到的激发能值被认为是阱中重空穴基态位置到阱顶的距离.对于SiGe合金和Si形成的组分量子阱，主要研究了退火对重空穴基态子能级的影响.发现样品的退火温度为800℃时，随退火时间延长，激发能增加.对此现象的解释是，由于Si,Ge互扩散，导致界面展宽，量子限制效应降低，重空穴基态位置下降，从而激发能增加.900℃下退火，由于扩散系数增大和应变弛豫加强，激发能值单调下降，量子限制效应引起的变化被掩盖.对于B高浓度超 关键词：     

薄膜尺寸效应对表面临界行为的影响

本文利用平均场理论讨论了薄膜尺寸效应对表面物理量临界指数及表面标度律的影响,说明表面临界行为亦存在渡越现象.     

考虑碳减排成本的内生经济增长路径研究

为了分析碳减排对内生经济增长的影响,将碳减排比例引入生产函数,将对气候变化的警惕意识引入效用函数,建立了考虑碳减排成本的内生经济增长模型,比较分析了各参数对经济增长路径的影响.长期来看,碳强度、碳减排比例与经济增长之间呈负向关系.低碳技术应用越广泛,研发成果对技术积累贡献率越大,消费者对当前消费的偏好程度越小,人们对气候变化的警惕意识越强,越有利于经济可持续发展.     

离子束辐照的碳纳米管及其物性研究

离子束辐照通常被认为导致材料产生缺陷, 形成无序结构, 从而破坏材料的性能。 但是, 最近利用离子束辐照碳纳米管的实验显示离子束辐照碳纳米管形成无定形的过程不能用传统的离子束辐照材料的机制来解释, 离子束辐照可导致碳纳米管形成一些自组装结构, 如无定形碳纳米结和碳纳米管连接结等。 研究还发现离子束辐照的碳纳米管薄膜在导电性和场发射性能方面都能得到明显的增强。 Ion beam irradiation is usually thought to induce defects and disordered structures in materials and then to destroy the properties of the materials. However, our recent experiments about the ion beam irradiation on carbon nanotubes(CNTs) indicate that the ion beam modification mechanism of CNTs is completely different from traditional one of bulk materials, and ion beam irradiation can lead to self organized structures in CNTs, such as amorphous junctions and CNT junctions. Moreover, the irradiated CNTs exhibit a improved conductivity and an enhanced field emission.     

同位素稀释高分辨气相色谱-高分辨质谱法测定土壤中痕量有机氯农药残留

建立了同位素稀释高分辨气相色谱-高分辨质谱测定土壤中痕量有机氯农药残留的分析方法。采用加速溶剂法萃取土壤样品,以正己烷/丙酮(体积比为1:1)为提取溶剂,提取液经过Florisil硅土固相萃取小柱净化后,采用高分辨DB-5MS毛细管色谱柱(30 m×0.25 mm×0.25 μm)分离,以保留时间和同位素特征离子丰度比定性,同位素峰面积比定量。实验结果表明,方法的回收率为77.3%～114.5%,相对标准偏差(RSD)≤10.81%（n=5）,检出限均小于0.04 pg/g。应用该方法检测某地区表层土壤中的有机氯农药,结果表明该方法适合测定环境土壤背景中痕量有机氯残留。