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31.
S. Lau Truong G. Levi F. Bozon-Verduraz A.V. Petrovskaya A.V. Simakin G.A. Shafeev 《Applied Physics A: Materials Science & Processing》2007,89(2):373-376
The formation of dense arrays of nanospikes occurs under laser ablation of bulk silver immersed in liquids such as water or
ethanol. The average height of spikes is 50 nm and their density on the target amounts to 1010 cm-2. This effect is observed with sufficiently short laser pulses. In particular, either a 350 ps or a 90 ps Nd:YAG lasers are
used operating in their fundamental harmonics. These nanospikes are characterized by UV–visible reflection spectrometry and
atomic force microscopy. The oscillations of electrons within Ag nanospikes results in a permanent coloration of the surface
and a modification of the optical reflection spectra of the metal. Nanospikes show a peak of plasmon resonance around 380 nm,
which shifts to the visible range upon oxidation in air. The initial spectrum may be restored by reduction of the oxidized
Ag surface through processing in an ammonia aqueous solution. Scanning the laser beam along the metal surface allows its nanostructuring
over extended areas (∼1 cm2). The nanostructured Ag surface shows enhanced Raman scattering of acridine molecules at a concentration of 10-5 M/l, whereas initial Ag target do not show any signal within the accuracy of measurements.
PACS 68.65.k; 64.70.Dv; 79.20.Ds; 42.62.Cf 相似文献
32.
2-Polyfluoroalkylchromene-4(4H)-thiones, synthesized from 2-polyfluoroalkylchromones and P2S5, react with aniline, phenylhydrazines, and hydroxylamine at the C(4) atom and afford corresponding anils, phenylhydrazones, and oximes of chromones. On heating in alcohol in the presence of concentrated HCl, chromone phenylhydrazones and oximes undergo ring closure to form 3-(2-hydroxyaryl)-1-phenyl-5-polyfluoroalkylpyrazoles and 5-hydroxy-3-(2-hydroxyaryl)-5-polyfluoroalkyl-Δ2-isoxazolines.__________Published in Russian in Izvestiya Akademii Nauk. Seriya Khimicheskaya, No. 10, pp. 2188–2195, October, 2004. 相似文献
33.
A.V. Karabutov V.D. Frolov E.N. Loubnin A.V. Simakin G.A. Shafeev 《Applied Physics A: Materials Science & Processing》2003,76(3):413-416
Low-threshold field electron emission (FEE) is reported for periodic arrays of micro-tips produced by laser ablation of Si
wafers. The best samples show emission at threshold fields as low as 4–5 V/μm for n-type Si substrates and of 1–2 V/μm for
p-doped Si substrates, as measured with a flat-screen technique. Auger electron spectroscopy and X-ray electron spectroscopy
reveal island-like deviation of the SiO2 stoichiometry on the tip surfaces, with lateral dimensions of less than 100 nm. Microscopic studies using a special field-emission
STM show that the emission originates from well-conducting regions of sub-micron size. The experimental data suggest FEE from
the tip arrays by a geometric field enhancement of both the individual micro-tip and the narrow conducting channels in the
tip body.
Received: 3 May 2002 / Accepted: 1 July 2002 / Published online: 28 October 2002
RID="*"
ID="*"Corresponding author. Fax: +7-095/135-82-34, E-mail: shafeev@kapella.gpi.ru 相似文献
34.
A.A. Lyalin A.V. Simakin G.A. Shafeev E.N. Loubnin 《Applied Physics A: Materials Science & Processing》1999,68(3):373-376
6 H5CH3, C6H6, and C6H5CH(CH3)2) to pulsed visible laser radiation of a copper vapor laser (λ=510.6 nm). The X-ray Auger electron spectroscopy (XAES), reflection
high energy electron diffraction (RHEED), and Raman analysis are employed to characterize the deposited films. The sp3 fraction in deposited films amounts to 60–70% and depends on the precursor. The average film thickness on a glass substrate
is about 100 nm. The films show excellent adherence, are transparent in the visible and have microhardness of 50–70 GPa, as
measured by nanoindentor.
Received: 28 September 1998 / Accepted: 13 January 1999 相似文献
35.
A. G. Denisova N. N. Gryzunova A. A. Vikarchuk M. R. Shafeev V. V. Bekin A. M. Gryzunov 《Bulletin of the Russian Academy of Sciences: Physics》2017,81(11):1348-1352
The influence of adding zinc nitrate(II) to a copper electrolyte on the morphologies, phase compositions, and specific surface areas of cupriferous coatings is studied. It is shown that copper–zinc coatings have high specific surface areas and exhibit good catalytic activities in the decomposition of formic acid. 相似文献
36.
E. Stratakis V. Zorba M. Barberoglou C. Fotakis G.A. Shafeev 《Applied Surface Science》2009,255(10):5346-5350
We report on the formation of self-organized nanostructures (NS) on bulk Al under its ablation in air and liquids with femtoseconds (fs) laser pulses. In case of exposure into liquids, NS are regularly formed on the Al surface with an average period of about 200 nm, independent of the laser polarization. A dispersion of Al nanoparticles (NPs) into the liquid additionally occurs. Irregular nano-bumps are produced when the irradiation is performed in air. NP dispersions as well as NS formed on Al surface show a characteristic absorption peak in the near UV which has been attributed to plasmon oscillation of electrons. The wings of this peak extending to the visible, lead to a distinct yellow coloration of the processed Al surface and the liquid dispersions. Ultrafast laser processing of bulk Al in liquids may be potentially a promising technique for efficient production of nanosized aluminum. 相似文献
37.
S. N. Andreev E. V. Barmina V. G. Kalinnikov A. V. Simakin A. A. Smirnov V. I. Stegailov S. I. Tyutyunnikov G. A. Shafeev I. A. Scherbakov 《Physics of Particles and Nuclei Letters》2017,14(6):900-903
Laser-light effects on γ-activities of the 137Cs and 134Cs water solutions containing gold nanoparticles are investigated at laser-light intensity on the order of 1012 W/cm2. The irradiation is found to reduce the radioactivities of both nuclides. Over the period of irradiation, no enhancement of the γ lines of spontaneous decays is detected. Possible mechanisms of the observed effect are discussed. 相似文献
38.
L. Nánai I. Hevesi N. F. Bunkin B. A. Zon S. V. Lavrishev B. S. Luk'yanchuk G. A. Shafeev 《Applied Physics A: Materials Science & Processing》1990,50(1):27-34
We present experimental data for vanadium and copper oxidation by cw CO2 laser light in an external electric field. Direct influence of the external field on the crystallisation process has been demonstrated in both vanadium and copper cases; the oxidation rate and surface morphology depend sensitively on the sign and strength of the external field. 相似文献
39.
The fabrication of solar cells based on laser-modified silicon (LMS) has been experimentally investigated. Laser ablation of single-crystal Si in air results in the formation of a quasi-periodic array of microcones. After removing the oxide layer, this array is coated by a transparent conducting tin oxide layer. A comparison of the spectral dependence of the mirror reflection of laser-modified Si with that of the initial flat Si surface shows a 10 to 15% drop in reflectivity. The light-to-electricity conversion efficiency is shown to exceed that of the initial flat Si surface by more than 20%. 相似文献
40.