大气条件等离子体针处理Enterococcus faecalis菌

自行研制的等离子体针在大气压下通过介质阻挡放电产生的等离子体,再由喷嘴处安装的漏斗形装置聚焦形成针状等离子体. 然后对针状等离子体的基本特性和杀Enterococcus faecalis（E. faecalis）菌进行了研究,E. faecalis菌是一种引起完善充填根管再感染的主要微生物. 当等离子体针功率为5—28?W时,对等离子体的温度进行了测量,表明它不同于其他热杀菌方式. 通过改变等离子体针内电极末端注入的氧气量,发现适当的氧气量,不仅增加等离子体内含氧粒子的浓度而且对等离子体的长度影响也不明显. 实验表明最佳参数为功率15?W,0.1?m³·h^-1氦和2.5%氧气,间距12?mm,处理时间30 s. 为了找出杀菌的关键粒子,进一步比较了大气压下的等离子体针的发射光谱与agar（琼脂）2?mm下的光谱并找出关键粒子. 关键词： 大气压等离子体 介质阻挡放电 E. faecalis菌')" href="#">E. faecalis菌 光谱     

Improved λ/4 phase-shifted DFB semiconductor laser with spatial hole burning compensation using grating chirp

A λ/4 phase-shifted distributed feedback (DFB) semiconductor laser with a preformed chirped grating used to compensate the spatial hole burning (SHB) induced index change is proposed and analyzed. It shows that compared with the three phase shifted DFB laser which is known for its good performance to eliminate SHB, the proposed SHB compensated laser has better single longitudinal mode property, narrower spectral linewidth and better dynamic characteristics.     

Temperature dependence of the Raman spectra of Bi2Te3 and Bi0.5Sb1.5Te3 thermoelectric films

The temperature dependence of the Raman spectra of Bi₂Te₃ and Bi_0.5Sb_1.5Te₃ thermoelectric films was investigated. The temperature coefficients of the E_g(2) peak positions were determined as –0.0137 cm^–1/°C and –0.0156 cm^–1/°C, respectively. The thermal expansion of the crystal caused a linear shift of the Raman peak induced by the temperature change. Based on the linear relation, a reliable and noninvasive micro‐Raman scattering method was shown to measure the thermal conductivity of the thermoelectric films. (© 2012 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim)     

Stereochemical analysis of ferrocene and the uncertainty of fluorescence XAFS data

Methods for the quantification of statistically valid measures of the uncertainties associated with X‐ray absorption fine structure (XAFS) data obtained from dilute solutions using fluorescence measurements are developed. Experimental data obtained from 10 mM solutions of the organometallic compound ferrocene, Fe(C₅H₅)₂, are analysed within this framework and, following correction for various electronic and geometrical factors, give robust estimates of the standard errors of the individual measurements. The reliability of the refinement statistics of standard current XAFS structure approaches that do not include propagation of experimental uncertainties to assess subtle structural distortions is assessed in terms of refinements obtained for the staggered and eclipsed conformations of the C₅H₅ rings of ferrocene. Standard approaches (XFIT, IFEFFIT) give refinement statistics that appear to show strong, but opposite, preferences for the different conformations. Incorporation of experimental uncertainties into an IFEFFIT‐like analysis yield refinement statistics for the staggered and eclipsed forms of ferrocene which show a far more realistic preference for the eclipsed form which accurately reflects the reliability of the analysis. Moreover, the more strongly founded estimates of the refined parameter uncertainties allow more direct comparison with those obtained by other techniques. These XAFS‐based estimates of the bond distances have accuracies comparable with those obtained using single‐crystal diffraction techniques and are superior in terms of their use in comparisons of experimental and computed structures.     

Effect of oxygen partial pressure on the structure and properties of Cu–Al–O thin films

We have studied the electrical and optical properties of Cu–Al–O films deposited on silicon and quartz substrates by using radio frequency (RF) magnetron sputtering method under varied oxygen partial pressure P_O. The results indicate that P_O plays a critical role in the final phase constitution and microstructure of the films, and thus affects the electrical resistivity and optical transmittance significantly. The electrical resistivity increases with the increase of P_O from 2.4 × 10^?4 mbar to 7.5 × 10^?4 mbar and afterwards it decreases with further increasing P_O up to 1.7 × 10^?3 mbar. The optical transmittance in visible region increases with the increase of P_O and obtains the maximum of 65% when P_O is 1.7 × 10^?3 mbar. The corresponding direct band gap is 3.45 eV.     

对23P2介子九重态中同位旋标量成员的质量分析

基于实验上已经确认的基态张量介子九重态的安排和现有的实验数据,利用从雷吉轨迹理论和质量混合矩阵推导出的介子质量关系,对张量介子第一径向激发态的安排做了分析预测.根据得到的结果,可以推测f₂（1810）和f₂（2010）可能作为张量介子第一径向激发态的候选者.同时给出了f₂（1810）和f₂（2010）作为张量介子第一径向激发态时的衰变信息.这些结论对激发态张量介子,特别是其中的同位旋标量态的安排将提供帮助.     

Recombination during expansion of ultracold plasma

Signals of ultracold plasma are observed by two-photon ionization of laser-cooled caesium atoms in a magneto-optical trap. Recombination of ions and electrons into Rydberg atoms during the expansion of ultracold plasma is investigated by using state-selective field ionization spectroscopy. The dependences of recombination on initial electron temperature (1--70 K) and initial ion density ($ \sim $10$^{10}$ cm$^{ - 3})$ are investigated. The measured dependence on initial ion density is $N^{1.547\pm 0.004}$ at a delay time of 5 $\mu $s. The recombination rate rapidly declines as initial electron temperature increases when delay time is increased. The distributions of Rydberg atoms on different values of principal quantum number $n$, i.e. $n=30$--60, at an initial electron temperature of 3.3 K are also investigated. The main experimental results are approximately explained by the three-body recombination theory.     

Photonic true-time delay unit for broadband adaptive nulling in antenna arrays

An Opto-VLSI-based (VLSI: very-large-scale-integration) tunable true-time delay (TTD) generation unit used for adaptive null steering in phased array antennas is presented. The system is based on continuous tunable optical TTD technique. Arbitrary multiple true-time delays to generate multiple broadband nulls can simultaneously be synthesised for each antenna element. The proposed structured are characterised both theoretically and experimentally. Experimental results demonstrating the principle of the true-time delay for null generations are presented. The maximum time delay measured for a wavelength tuning from 1530 to 1560 nm is 9.5 ns.     

Microstructure and dielectric properties of PMN–PT ceramics prepared by the molten salts method

The sintering characteristic and dielectric properties of 0.67PMN–0.33PT ceramics prepared by the molten salt synthesis (MSS) method were investigated. PMN–PT particles synthesized by MSS with smaller grain size and good dispersion could lower the sintering temperature of ceramics; PMN–PT ceramics with relative density above 96% could be obtained in the range 1150–1180 °C. The molten salts species could significantly affect the microstructure and properties of MPN-PT ceramics. In the range 1100–1200 °C, PMN–PT ceramics from the sulfate flux MSS powders showed intergranular fracture, but that from the chloride flux MSS powder showed transgranular fracture. At the same sintering condition, the properties of PMN–PT ceramics from the powders prepared in the chloride flux are better than that from the powders prepared in the sulfate flux, their maximum dielectric constant ε_max≈29,385 and piezoelectric constant d₃₃≈660 pC/N. The above results demonstrated that PMN–PT ceramics prepared by the molten salts method possessed excellent piezoelectric and dielectric properties.