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121.
V. O. Kur'yanov T. F. Zhelobetskaya A. E. Zemlyakov V. Ya. Chirva 《Chemistry of Natural Compounds》1993,29(1):103-106
The synthesis has been effected of derivatives of MDP having a spacer with an amino or carboxy group. The final stage of the synthesis was the condensation of Boc-L-Ala-D-iGln with 6-aminohexanol (followed by the two-stage replacement of the hydroxy by an azido group) or with benzyl 6-aminohexanoate.Simferopol' State University. Translated from Khimiya Prirodnykh Soedinenii, No. 1, pp. 122–125, January–February, 1993. 相似文献
122.
R. Gerbaldo G. Ghigo G. Giunchi L. Gozzelino F. Laviano E. Mezzetti 《The European Physical Journal B - Condensed Matter and Complex Systems》2002,26(3):297-300
We present results from an extended magneto-optical (MO) analysis of two samples cut from high-density pellets of MgB2. The first sample was studied in order to show that no matter how large the sample is and despite the bulk granularity, the
material enters into a critical state in a crystal-like fashion. The second sample was chosen for the quantitative analysis.
A numerical approach based on an inverted 2D Biot-Savart model was used to calculate the current paths across the homogeneous
polycrystalline bulk, as well as in the vicinity and across some morphological defects. Local current densities in the homogeneous
part were estimated as a function of the applied magnetic field at different temperatures, in three regimes: below full penetration,
at full penetration and above full penetration, respectively. A hypothesis of interpretation of the apparent absence of magnetic
granularity inside the polycrystalline microstructure is presented. It is related to a critical state likely reached by a
network of strongly coupled Josephson junctions.
Received 31 May 2001 and Received in final form 5 December 2001 相似文献
123.
The energy characteristics of an XeCl exciplex lamp with planar construction pumped by a low-pressure gas discharge are investigated
experimentally. When a discharge gap of width 2 cm and a Xe-Cl2 mixture were used, average radiation powers up to 20 mW were obtained in the wavelength interval 200–380 nm at efficiencies
of ∼0.4%. In this case the total efficiency of radiation into an angle of 4π exceeded 4%. It is shown that increasing the working pressure and using low discharge currents can lead to “point” radiation
sources.
Zh. Tekh. Fiz. 67, 43–46 (December 1997) 相似文献
124.
S. Moss de Oliveira P. M. C. de Oliveira F. C. de Sá Barreto 《Journal of statistical physics》1995,78(5-6):1619-1627
Using the finite-size scaling renormalization group, we obtain the two-dimensional flow diagram of the Blume-Capel model forS=1 andS=3/2. In the first case our results are similar to those of mean-field theory, which predicts the existence of first- and second-order transitions with a tricritical point. In the second case, however, our results are different. While we obtain in theS=1 case a phase diagram presenting a multicritical point, the mean-field approach predicts only a second-order transition and a critical endpoint. 相似文献
125.
The 2D Rancieite type manganic acid was prepared by reduction of KMnO4 in acidic medium. Its ion exchange behavior allows to prepare alkali derivatives. All compounds were characterized with use of a combination of X-ray diffraction, chemical analyses, TGA, magnetic measurements and spectroscopic techniques. The evolution of their chemical composition versus temperature was studied between 180 and 400 °C. It shows that the dehydration process is partly reversible in these compounds whereas the weak reduction is irreversible. The 2D Rancieite-type manganic acid is readily different from a Birnessite-type phyllomanganate, as shown by several features: the interlayer distance, the ion exchange capacity, the thermal behavior, the interlayer cation content, the manganese average oxidation state, the magnetic behavior and the IR spectrum. 相似文献
126.
Fixed-frequency and threshold photoelectron spectra have been recorded for ionization from the S ls shells in SF6, CS2 and COS, the Si 1s shells in SiH4 and SiCl4 and the Cl 1s shell in SiCl4 using synchrotron radiation. Fixed-frequency spectra generally showed a single strong ionization feature with associated weak satellite structure due to excited ionized states. Threshold spectra closely resembled X-ray absorption spectra but with an additional feature due to direct ionization. In cases where resonant process enhanced the NEXAFS spectrum direct ionization was not observed. 相似文献
127.
John L. Wood Johannes Schwarzenberg Edward F. Zganjar Dubravka Rupnik 《Hyperfine Interactions》1992,75(1-4):51-58
State-of-the-art spectroscopy of nuclei far from stability has achieved an extraordinary level of sophistication and detail
in the last ten years. In principle, if a state can be populated, it can be characterized by its energy, spin, parity, and
major decay paths. Sometimes its lifetime can be measured. In practice, one is confronted with enormous complexity. To convert
raw spectroscopic data into nuclear structure data involves a complex process of disentangling gamma rays and conversion electrons
into decay schemes. Specifically, coincidence techniques, especially coincidence intensities, play a crucial role in this
process. Recent examples and methods from work done at UNISOR are presented. 相似文献
128.
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130.