Crystal and molecular structures of 1-[3-(3,4-dimethoxyphenyl)-2-propenoyl]pyrrolidine.

The crystal structure of 1-[3-(3,4-dimethoxyphenyl)-2-propenoyl]pyrrolidine (C15H19NO3) (I) has been determined by X-ray analysis. It crystallizes orthorhombic space group Pbca with a = 24.295(3), b = 15.086(3), c = 7.552(3)A, V = 2768(1)A3, Z = 8, Dcalc = 1.254 g/cm3, mu = (Mo K(alpha)) = 0.87 cm(-1). The title compound has analgesic activity of cycloaliphatic amine part. The molecule is deviated from planar configuration.     

Optimizing the optical field distribution of solid immersion lens system by a continuous phase filter

In solid immersion lens (SIL) microscopy systems with high numerical aperture (NA), there always exists the aberration produced by Fresnel effects at the interface between SIL and the sample. This aberration may cause the degradation of the image of sample. We design a continuous phase filter and optimize the optical field distribution of SIL system. The numerical results show that when the continuous phase filter is used, the field distribution of SIL system can be optimized, and the focal depth and intensity of transmitted light can be increased. At the same time, the intensity of side-lobe and the resolution are kept almost unchanged.     

Analysis and implementation of cross sync period underwater acoustical positioning techniques for underwater targets

I.IlltroductionWhenanactiveunderwateracousticalpositioningsystemissearchingforanunderwatertarget,itisnecessaryforittocompleteatransmittingandreceivingcycIewithineachworkingperiodinordertofindoutthelocationofthetargetcorrectly.Forexample,whenanunder-wateracoustica1synchronouspositioningsystemistrackinganunderwatertargetwithagivensynchr0nizingperiod,thepropagati0ntimeofthepositioningsignaltravellingfr0mthetaJrgettothearrayofthesystemshouldbelessthanthesynchronizingperiod0therwisetargetdis-tance…     

The Existence of Periodic Orbits for Higher Dimensional Autonomous Systemswith Small Perturbations

ＴｈｅＥｘｉｓｔｅｎｃｅｏｆＰｅｒｉｏｄｉｃＯｒｂｉｔｓｆｏｒＨｉｇｈｅｒＤｉｍｅｎｓｉｏｎａｌＡｕｔｏｎｏｍｏｕｓＳｙｓｔｅｍｓｗｉｔｈＳｍａｌｌＰｅｒｔｕｒｂａｔｉｏｎｓＪｉａｎｇＬｉｑｉｎｇ（蒋里强）；ＺｈｏｕＹｉ（周毅）；ＦａｎＹｅ（范晔）（...     

混合流体浸润相变的研究(Ⅲ)——二元系统的四相共存态

本文讨论二元Sullivan系统的一个特殊状态——二元四相系的浸润相变性质,该系统的许多性质可以通过对两个二元二相系的讨论而得到。结果表明:这一系统同时存在一级相变和二级相变。 关键词：     

A PICARD TYPE THEOREM AND BLOCH LAW

Ａ ＰＩＣＡＲＤ ＴＹＰＥ ＴＨＥＯＲＥＭ ＡＮＤ ＢＬＯＣＨ ＬＡＷ ￥ＹＥＹＡＳＨＥＮＧＡｂｓｔｒａｃｔ：Ａｐｉｃａｒｄｔｙｐｅｔｈｅｏｒｅｍｉｓｐｒｏｖｅｄ，ａｎｄａｃｏｕｎｔｅｒｅｘａｍｐｌｅｉｓｇｉｖｅｎｔｏｓｈｏｗｔｈａｔｔｈｅＢｏｌｃｈ...     

高频单线圈双调谐NMR单晶探头的研制

本文报道了一种测角单晶NMR探头。该探头采用单线圃双调谐电路,工作频率在90MHz-110 MHz连续可调,可进行交叉极化大功率去耦实验。文中提出了一种简单而有效的测角装置,可使单晶绕三个互相垂直轴转动实现单晶的NMR测量。作为典型的应用例子,本文利用该探头实现了单晶DGO(2NH₂CH₂COOH·H₂C₂O₄)屏蔽张量的测量。     

THE VALIDITY OF HIGH TEMPERATURE APPROXIMATION IN NMR SPECTROSCOPY AND ITS RELATED PROBLEMS

A large body of conspicuous publications [1] in recent years asserts that the high temperature approximation (HTA), a mostly tested and most widely used assumption in NMR spectroscopy and MRI technology, is invalid for concentrated samples in high magnetic fields such as for a proton COSY spectrum of water [1].     

单晶光纤损耗谱测量装置

本文描述了一套用以测量单晶光纤损耗谱的装置。本装置由卤钨灯,单色仪,积分球,AgORbCs光电倍增管以及数据采集,处理和控制系统组成。可测量300～1150nm的光谱范围。利用本装置可获得单晶光纤的吸收光谱,透过率谱,散射光谱以及散射位置谱。     

脱镁叶绿素a和脱镁叶绿素b的联合同步荧光分析法

建立了脱镁叶绿素a和脱镁叶绿素b的联合同步荧光分析法。方法简便快速。脱镁叶绿素a和脱镁叶绿素b的线性范围分别为0～400ng/ml和0～200ng/ml,检出限分别为1ng/ml和0.5ng/ml。