龙爪芦荟和库拉索芦荟中微量锗的测定与红外光谱区别

采用吸光光度法对龙爪芦荟和库拉索芦荟中的微量锗进行了测定,并探讨了两种芦荟的红外光谱的区别。结果表明,龙爪芦荟中含锗量在26.1～28.6μg·g-1,回收率为91.6%～97 5%。库拉索芦荟中含锗量在16.8～20.0μg·g-1,回收率为87.1%～94.5%。两种芦荟的FT IR光谱图在2100cm-1处有明显差异,由此可区别两种芦荟。     

Contributions to Group IV organometallic chemistry : II. Preparation and properties of dithiacyclopentane and dithiacyclohexane derivatives of silicon,germanium and tin

The preparation and properties of dithiacyclopentane and dithiacyclohexane derivatives of silicon, germanium and tin are described and general mass spectral features of these heterocycles are discussed.     

微波促进的N-取代2,3,3a,4,7,7a-六氢异吲哚-1,3-二酮的Beller法合成

A rapid and facile synthesis of N-substituted 2,3,3a,4,7,7a-hexahydroisoindole-l,3-dione derivatives via microwave-promoted Beller three-component domino reaction of α,β,-unsaturated aldehydes, amides and N-substituted maleimides was described.     

On Mixed Pressure-Velocity Regularity Criteria to the Navier-stokes Equations in Lorentz Spaces,Part Ⅱ:The Non-slip Boundary Value Problem

This paper is a continuation of the authors recent work [Beir?o da Veiga, H.and Yang, J., On mixed pressure-velocity regularity criteria to the Navier-Stokes equations in Lorentz spaces, Chin. Ann. Math., 42(1), 2021, 1–16], in which mixed pressure-velocity criteria in Lorentz spaces for Leray-Hopf weak solutions of the three-dimensional NavierStokes equations, in the whole space R~3 and in the periodic torus T~3, are established. The purpose of the present work is to extend the result of mentio...     

A new proposal for the discretization of the Griffin—Wheeler—Hartree—Fock equations

A polynomial expansion is proposed as a new way to discretize the Griffin-Wheeler-Hartree-Fock equations of the Generator Coordinate Hartree-Fock method. The implementation of the polynomial expansion in the Generator Coordinate Hartree-Fock method discretizes the Griffin-Wheeler-Hartree-Fock equations through a numerical mesh which is not equally spaced. This procedure makes the optimization of Gaussian exponents in the Generator Coordinate Hartree-Fock method more flexible and more efficient. The results obtained with the polynomial expansion for atomic Hartree-Fock energies show this technique is very powerful when employed in the design of compact and high accurate Gaussian basis sets used in ab initio non-relativistic (Hartree-Fock) and relativistic (Dirac-Fock) calculations.     

COMPONENT ALLEE EFFECTS AND STAGE‐SPECIFIC PREDATION: A BRIEF INSIGHT INTO CONSERVATION AND BIOLOGICAL CONTROL ISSUES

In this paper, we propose a two‐stage structured population model subject to component Allee effects in fecundity and maturation, and with two disturbances (predation only and harvest and predation) acting on both stages. It is shown that this combination leads to a demographic Allee effect—a characteristic that could be exploited in pest biological control, but on the other hand, it represents a bane in conservation biology. The analysis is performed for disturbances with functional responses type 2 and 3, and the models show that they yield qualitatively similar results. This characteristic is discussed from the species conservation and biological control point of view, together with possible extensions of this work.     

基于多分辨分析的沪深股市相关性分析

为了有效地揭示沪深股市不同交易周期股票交易的相关性,本文采用极大重叠离散小波变换,将上证指数和深圳成指高频收益率分解在不同的交易周期上,对各个周期的收益率采用semi-GPD模型作为其边缘分布分别进行拟合,在此基础上采用Copula函数方法建立同周期收益率的联合分布,度量了沪深两市同周期交易的相关性.实证表明,不同交易周期所表现出的相关性存在明显差异,并且随着交易期的增长,沪深两市非对称结构逐步明显。     

Organoboron compounds XIII. Preparation and properties of some 2-substituted 1,3,2-dithiaborinans

The preparation and properties of some boron heterocycles of the general formula

(where X = Ph, SR, NR₂, NHR and NHNPh) are described and the general features of their mass spectra discussed.     

高分辨率多光谱数字相机电子学系统的设计

设计了一种基于多光谱技术的机载数字相机电子学系统。它包括时序产生单元、信号处理单元、信号控制单元、数据输出接口单元和数据采集存储单元等几部分。系统具有调光和行频调节功能,用以满足在不同能量状态和不同飞行高度下的成像质量。考虑到机载设备的特殊要求,对其进行了轻量化设计和机载稳定平台设计。它具有实时高速存储和实时采集数据的功能。结果表明,机载数字相机电子学系统的各种功能完全满足设计要求,为实现高分辨率探测提供了保证。