聚酰胺酸合成工艺研究

 采用超声波在线测量溶液粘度的方法，研究了合成聚酰胺酸过程中实验条件的影响，并对实验结果进行分析，由此确定了合成高分子量聚酰胺酸的最佳实验条件。研究表明：在加料次序为先加二胺后加二酐（二酐与二胺的摩尔比为1.01～1.02：1）、试剂中含水量尽可能少，反应温度0～5℃、反应时间以溶液粘度到达最大值为止的条件下，所合成的聚酰胺酸溶液粘度最大，可满足惯性约束聚变（ICF）充气腔靶端口膜的需要。     

软门限去噪法在X射线能谱分析中的应用

从函数空间的剖分和理想滤波器组的角度分析了多分辨率信号的分解与重构，提出了一种X射线能谱去噪的方法，即应用Mallat算法对谱信号进行小波分解，然后应用一个非线性软门限函数在小波域内将噪声抑制和消除，最后重构得到去噪后的能谱。该方法明显改善了能谱定量分析的结果。     

EAST装置等离子体放电位形快速识别研究

为了适应超导托卡马克装置EAST位形控制运行模式的需要，研究了等离子体放电位形快速识别算法，给出了等离子体放电位形重建的模拟计算结果，并与美国GA平衡反演程序EFIT计算的平衡结果进行了详细的误差对比分析.结果表明，通过外部磁测量和合适的电流剖面模型，并结合实时平衡重建算法可以快速地对EAST等离子体放电位形进行识别. 关键词： 托卡马克 等离子体 平衡重建 数值模拟     

High temperature superconducting thin films for microwave filters

YBa₂Cu₃O_7-δ and Tl₂Ba₂CaCu₂O₈ thin films for microwave filters were synthesized by pulsed laser deposition and the two-step thalliation process. Substrate quality requirements and the relation of thin film morphology, microstructure with microwave surface resistance were discussed.     

基于免疫算法的组合预测方法

利用免疫算法搜索全局最优解能力,提出了一种其于免疫算法的组合预测权系数确定的新方法,并给出了具体算法.仿真实验结果表明了免疫算法在组合预测方面具有很好的可行性和有效性.     

The best uniform convergence rate of linear empirical bayes estimators

In this paper the thought on the uniform convergence of an empirical Bayes estimator or linear empirical Bayes (l.e.B.) estimator is advanced. Under two different models the l.e.B. estimators of the parameter are constructed respectively. It is proved that the convergence rates and uniform convergence rates of these l.e.B. estimators are all one with respect to the corresponding prior families. It is shown that the uniform convergence rate one is the best, under mild assumptions imposed on the conditional density of the sample.     

动态模糊随机信息处理的数学方法

本文系统地概述了我们近年来提出的动态模糊随机信息处理的数学方法,内容包括模糊随机变量、模糊随机过程和模糊随机微分方程的基本解法等方面的基本概念、基本定义和某些重要的定理,以及动态系统的模糊随机响应与可靠性分析的方法等。这些方法是为我们研究工程实际问题的需要逐步发展起来的,对于处理某些类型的问题简便实用。     

Melt rheology of polylactide/montmorillonite nanocomposites

In this article, the linear and nonlinear shear rheological behaviors of polylactide (PLA)/clay (organophilic‐montmorillonite) nanocomposites (PLACNs) were investigated by an Advanced Rheology Expanded System rheometer. The nanocomposites were prepared by master batch method using a twin‐screw extruder with poly(ε‐caprolactone) (PCL) as a compatibilizer. The presence of org‐MMT leads to obvious pseudo‐solid‐like behaviors of nanocomposite melts. The behaviors caused by the formation of a “percolating network” derived from the reciprocity among the strong related sheet particles. Therefore, the storage moduli, loss moduli, and dynamic viscosities of PLACNs show a monotonic increase with MMT content. Nonterminal behaviors exists in PLACNs nanocomposites. Besides the PLACNs melts show a greater shear thinning tendency than pure PLA melt because of the preferential orientation of the MMT layers. Therefore, PLACNs have higher moduli but better processibility compared with pure PLA. © 2007 Wiley Periodicals, Inc. J Polym Sci Part B: Polym Phys 45: 3189–3196, 2007     

Mössbauer Studies and Magnetic Properties of Y3−x Ce x Fe5O12

It is shown that in-situ ^166mHo (I = 7) in a spherical single crystal of HoF₃ can be used as sensitive internal thermometer to thermally detect NMR (NMR-TDNO) from the 100% abundant stable ¹⁶⁵Ho (I = 7/2) nuclei. In addition, new ^166mHo NMRON results are reported. Both the ^166mHo NMRON and ¹⁶⁵Ho NMR-TDNO spectra show three distinct quadrupolar split sub-resonances, in zero applied field. The data is used to make estimates of the Ho magnetic moments and quadrupole parameters for the ^166mHo and ^166mHo sites.