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Chaoying Wan Feng Zhao Xujin Bao Bala Kandasubramanian Matt Duggan 《Journal of Polymer Science.Polymer Physics》2009,47(2):121-129
Polyamide 12/Trisilanolphenyl‐POSS (PA 12/POSS) composites were prepared via melt‐compounding. The effect of polyhedral oligomeric silsesquioxane (POSS) on crystalline structure and crystalline transition of PA 12 was investigated by wide‐angle X‐ray diffraction (WAXD) and real time fourier transform infrared spectroscopy (FTIR). WAXD results indicated that PA 12 crystallized into γ‐form as slowly cooling from melt and the presence of POSS did not influence the crystalline structure of PA 12. Both PA 12 and PA 12/POSS composites underwent Brill transitions when they were heated from room temperature to melt point. Real time FTIR patterns showed that an absorption band at 697 cm?1 ascribed to Amide V (α) mode was emerged along with the disappearance of Amide VI (γ) band at 628 cm?1 with the increase of the temperature for PA 12 and PA 12/POSS composites, which suggested that the γ‐form crystalline has transformed into α form. The Brill bands were identified and the transformed mechanism was discussed based on the real FTIR results. The addition of POSS enhanced the tensile strength and thermal stability of PA 12. © 2008 Wiley Periodicals, Inc. J Polym Sci Part B: Polym Phys 47: 121–129, 2009 相似文献
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The comparison between three classical potentials and density functional theory (DFT) is performed mainly for divacancy and hexavacancy in Si crystal. According to their performances on the formation energies and structural properties (distortion magnitude, relaxation volume and symmetry), the limitations and validities of classical potentials are discussed. It is found that the outward relaxation directions of EDIP and Tersoff (T3) are contrary to the DFT and Stillinger-Weber (SW) directions (inward), which restrict their application in the structural property calculations. Except for the divacancy symmetries, the results of SW are in agreement with the DFT results. Thus, it can be concluded that SW should be the best potential to describe V2 and V6. 相似文献
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超声速钝体逆向喷流减阻的数值模拟研究 总被引:1,自引:0,他引:1
为研究逆向喷流技术对超声速钝体减阻的影响,采用标准k-ε湍流模型,通过求解二维Navier-Stokes方程对超声速球头体逆向冷喷流流场进行了数值模拟,并着重分析了喷口总压、喷口尺寸对流场模态和减阻效果的影响。计算结果显示:随着喷流总压的变化,流场可出现两种流动模态,即长射流穿透模态和短射流穿透模态;喷流能使球头体受到的阻力明显减小;存在最大减阻临界喷流总压值(在所研究参数范围内最大减阻可达51.1%);在其它喷流物理参数不变时,随着喷口尺寸的增大,同一流动模态下的减阻效果下降。本文的研究对超声速钝体减阻技术在工程上的应用具有一定的参考价值。 相似文献
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一种容错联邦滤波算法在INS/GPS/Doppler组合导航系统中的应用 总被引:2,自引:1,他引:2
本文提出了一种联邦滤波器的容错滤波算法,并在INS/GPS/Doppler 组合导航系统中进行了计算机仿真。仿真结果表明,该算法具有与集中卡尔曼滤波同等的导航精度,同时具有较强的容错性。 相似文献
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Sishen Xie Wenzhi Li Chaoying Wang Liwen Xu Hao Zhang Yun Zhang Luxi Qian 《中国科学A辑(英文版)》1997,40(9):971-977
Carbon nanotubes were prepared by chemical vapor deposition (CVD) of hydrocarbon gas on various substrates. The effect of substrates on the growth, morphology and structure of carbon nanotubes were investigated. Aligned carbon nanotubes with high density and purity were achieved by CVD on mesoporous silica substrate. The Raman scattering of aligned carbon nanotubes was carried out, and the dependence of the phonon properties on the microstructure of the nanotubes has been discussed. 相似文献
20.
Bo Liu Chaoying Wan Yinxi Zhang Yu Su Jiliang Ji 《Journal of Macromolecular Science: Physics》2013,52(6):1159-1169
Polycarbonate (PC) and acrylonitrile–EPDM (ethylene/propylene/diene elastomer)–styrene ter‐polymer (AES) blends and PC/AES/organically modified montmorillonite (OMMT) composites were prepared at 20%, 40%, 50% by weight of AES and 3% by weight of OMMT. The microstructure, interfacial interactions, and rheological properties of the PC/AES blends and PC/AES/OMMT composites were studied systematically. X‐ray diffractometer (XRD) results reveal that the AES is easier to intercalate into OMMT than PC, and the content of AES has a little effect on the interlayer distance of OMMT. Wetting coefficient calculation indicates that OMMT distributes primarily at the interface of the polymer blend. Field emission scanning electron microscope (FE‐SEM) observation indicates that the phase morphology of PC/AES blends and PC/AES/OMMT composites is not influenced by the OMMT. However, linear rheological properties suggest that the addition of OMMT has a great effect on the linear rheological property. 相似文献