百万大气压下的压强校准及5.5 Mbar静压强的获得

进行了百万大气压下,静水压和非静水压条件下的压力校准,同时观察到金刚石砧容器中红宝石R线红移至830nm处,由校准公式算得对应的压强为5.5Mbar。 关键词：     

拖曳线列阵用光纤水听器的研究

报道了光纤水听器用于拖曳线列阵的研究结果。在保证光纤水听器声相位灵敏度的前提下, 优化设计了光纤水听器的结构,降低了光纤水听器的加速度灵敏度36dB。实验测得在20-1600Hz 频段,该光纤水听器的相位灵敏度为-162．7dB,频段内灵敏度的起伏为±0．7dB,加速度灵敏度小于-30dB。     

Determination of residual solvents in a transdermal system by means of headspace gas chromatography

Summary Pharmaceutical products have to be tested for impurities including residual solvents. This is also required in production control. The simplest solution to this problem is headspace gas chromatography. This paper describes the determination of residual volatile hydrocarbons in the transdermal system DEPONIT by only one headspace measurement. Accuracy is ensured by the multiple headspace extraction technique.

---

Bestimmung von Restlösungsmittelgehalten in einem transdermalen System durch Headspace-Gas-Chromatographie

Zusammenfassung Pharmazeutische Produkte müssen auf Verunreinigungen geprüft werden, auch auf Restlösungsmittelgehalte. Ein zusätzlicher Grund ist die fortlaufende Kontrolle der Herstellung. Die einfachste Möglichkeit für dieses Problem ist die Bestimmung durch Headspace-Gas-Chromatographie. Dieser Artikel beschreibt die Bestimmung von noch vorhandenen flüchtigen Kohlenwasserstoffen in dem transdermalen System DEPONIT durch nur eine Headspace-Messung. Die Richtigkeit ist durch die Anwendung der Mehrfach-Gasextraktionstechnik sichergestellt.

     

Skew Models II

If g and G are the pdf and the cdf of a distribution symmetric around 0 then the pdf 2g(u)G(λ u) is said to define a skew distribution. In this paper, we provide a mathematical treatment of the skew distributions when g and G are taken to come from one of Pearson type II, Pearson type VII or the generalized t distribution.      

A MINI MULTI-GAS DETECTION SYSTEM BASED ON INFRARED PRINCIPLE

To counter the problems of gas accidents in coal mines, family safety resulted from using gas, a new infrared detection system with integration and miniaturization has been developed. The infrared detection optics principle used in developing this system is mainly analyzed. The idea that multi gas detection is introduced and guided through analyzing single gas detection is got across. Through researching the design of cell structure, the cell with integration and miniaturization has been devised. The way of data transmission on Controller Area Network (CAN) bus is explained. By taking Single-Chip Microcomputer (SCM) as intelligence handling, the functional block diagram of gas detection system is designed with its hardware and software system analyzed and devised. This system designed has reached the technology requirement of lower power consumption, mini-volume, big measure range, and able to realize multi-gas detection.     

First-Principles Study on the Electronic Structures for Y^3＋：PbWO4 Crystals

The possible defect models of Y^3＋：PbWO4 crystals are discussed by defect chemistry and the most possible substituting positions of the impurity Y^3＋ ions are studied by using the general utility lattice program （GULP）. The calculated results indicate that in the lightly doped Y^3＋ ：PWO crystal, the main compensating mechanism is [2Ypb^＋ ＋ VPb^2-], and in the heavily doped Y^3＋ ：PWO crystal, it will bring interstitial oxygen ions to compensate the positive electricity caused by YPb^＋, forming defect clusters of [2Ypb^＋ ＋Oi^2-] in the crystal. The electronic structures of Y3＋ ：PWO with different defect models are calculated using the DV-Xα method. It can be concluded from the electronic structures that, for lightly doped cases, the energy gap of the crystal would be broadened and the 420nm absorption band will be restricted; for heavily doped cases, because of the existence of interstitial oxygen ions, it can bring a new absorption band and reduce the radiation hardness of the crystal.     

同时估计回归函数零点及噪声参数

对未知的回归函数以 ARMA 型的误差得到量测时,本文以随机逼近型算法搜索回归函数的零点,同时以参数辨识算法估计噪声模型中的未知系数阵.本文证明了两种算法以概率1的收敛性.     

Li2O-B2O3-P2O5系统非晶态混合骨架效应的NMR研究

用核磁共振对非晶态中B³⁺离子的微观结构进行了测定,结合Raman光谱的研究,对Li₂O-B₂O₃-P₂O₅系统非晶态的性能(电导率、密度等)在P₂O₅/B₂O₃比约等于1时产生极值的原因从理论上作了阐明。     

纳米累托石-TiO2光催化剂的制备及表征

以TiCl4和累托石为主要原料，制备出纳米累托石-TiO2粉末，并用X-衍射、透射电镜等对其进行表征．结果表明：纳米累托石-TiO2粉末平均直径为17．5nm当焙烧温度从500℃升至800℃时，累托石-TiO2粉末的比表面积从65．7m^2／g下降至3．3m^2／g，单位质量吸附剂的孔体积从0．1430cm。／u降到0．0213cm^3／g；当焙烧温度从300℃上升至500℃时，孔径变化不大，属中孔范围；当焙烧温度升至800℃时，一些孔道出现坍塌，不利于纳米累托石-TiO2粉末的光催化活性．     

Pascal矩阵与Vandermonde矩阵的关系

EI-Mikkawy M证明了对称Pascal矩阵Q_n和Vlandermonde矩阵V_n之间满足矩阵方程Q_n=T_nV_n,这里T_n是一个随机矩阵。本文证明了随机矩阵T_n能够分解成第一类Stirling矩阵和对角矩阵的乘积,得到了矩阵T_n的元素之间的递推关系,从而回答了EI-Mikkawy M的一个公开问题。同时得到了一些与Stirling数相关的组合恒等式。