同步辐射讲座 第二讲 同步辐射X射线荧光及其在植物微量元素分析中的应用

比较了同步辐射（SR）X射线荧光（XRF），电子和质子激发的X射线谱，介绍了XRF谱的采集方法及数据处理方法（主要是能谱方法），智能方法的无标样（基本参数法）定量分析原理，以及近期在植物微量元素分析中得到的结果。     

超临界流体触媒作用下石墨-金刚石转变

 研究了超临界流体CO₂在石墨-金刚石转变中的触媒作用。实验中，采用Ag₂O作为流体触媒的先驱材料，在7.7 GPa压力下，Ag₂O在1 200 ℃分解成Ag和O₂，O₂与石墨套管在高温高压下反应形成CO₂超临界流体。研究结果表明，在7.7 GPa和1 500 ℃以上温度条件下，石墨在CO₂流体触媒的作用下可转变为金刚石晶体，在1 500～1 700 ℃温度范围内合成出的金刚石具有完好的八面体形貌，与天然金刚石的生长特征非常相似。     

空心阴极灯激发的微波等离子体炬原子/离子荧光光谱研究--钙的原子/离子荧光光谱

用强短脉冲供电技术的空心阴极灯作激发源、微波等离子体炬作原子／离子化器，建立了原子／离子荧光光谱实验装置。详细研究了微波等离子体功率、观察高度、空心阴极灯电流等因素对原子／离子荧光信号强度的影响，测量了系统对Ca的原子／离子荧光光谱的检出限。     

变系数非线性方程的Jacobi椭圆函数展开解

把Jacobi椭圆函数展开法扩展并应用到求解变系数的非线性演化方程,比较方便地得到新的解析解 关键词： Jacobi椭圆函数 变系数非线性方程 类椭圆余弦波解 类孤子解     

溴酸钾-亚甲蓝催化光度法测定硝酸盐和亚硝酸盐

用镉柱将NO-3 还原为NO-2 ,利用在磷酸介质中NO-2 对溴酸钾氧化亚甲蓝这一褪色反应具有强烈的催化作用而建立了同时测定痕量硝酸盐和亚硝酸盐的新方法。本方法简便、快速、灵敏 ,对亚硝酸盐和硝酸盐测定的线性范围分别为 0～ 2 0 0 μg·L-1和 0 0 0 3～ 310 μg·L-1,用于测定各种水样中痕量NO-2 和NO-3 的含量均获得满意结果     

静态球对称黑洞Dirac场的统计熵

利用改进的brickwall模型,给出了一类静态球对称黑洞Dirac场的熵,结果表明,在取相同的截断因子时,Dirac场的熵均为标量场的熵的72倍 关键词： 黑洞 统计熵 brickwall模型 Dirac场     

Circular dichroism of some bisbenzyltetrahydroisoquinoline alkaloids

The circular dichroism (CD) method has been used to study the stereochemistry of the bisbenzyltetrahydroisoquinoline alkaloids. A relationship has been established between the absolute configurations of the asymmetric centers and the parameters of the Cotton effects in the CD spectra. The changes in the CD spectra on protonation have been correlated with conformational rearrangements of the molecules due to the different attachment of the oxygen bridges.Institute of the Chemistry of Plant Substances, Academy of Sciences of the Uzbek SSR, Tashkent. Translated from Khimiya Prirodnykh Soedinenii, No. 6, pp. 818–823, November–December, 1979.     

关于广义分数次积分的合成

Compositions of generalized fractional integral operators involving Gauss hy-pergeometric function with power weights are studied. Composition formulas for such integrals which are the operators of the same type are obtained. In parti-cular, compositions of two identical operators are given.     

具有随机生存域的随机场

本文研究具有随机开参数集的随机场构造,获得了具有已知有穷维分布的随机场存在和唯一性条件。     

The diffraction of plane gravitational waves by the edge of an ice cover

The diffraction of plane surface gravitational waves by the edge of an ice cover lying on the surface of an incompressible fluid of infinitely great depth is considered. The ice cover is simulated by a thin elastic plate. The wave reflection and transmission coefficients are determined when it interacts with the ice cover. A wave field is constructed in the fluid under the conditions that a periodic lumped force and a lumped moment act on the edge of the ice cover. It is shown that as the incident wavelength increases the reflection coefficient tends to zero and the transmission coefficient tends to unity.