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111.
建立了ICP-AES测定超导粉中痕量镍的新方法。优化了仪器工作参数,对超导前驱粉中痕量镍测定时的基体干扰及干扰消除方法进行了系统研究,结果表明:大量存在的基体元素产生严重基体效应,导致测定重现性及准确度变差,实验采用分离富集方法以提高测定结果的准确度和精密度。实验中首先用阴离子交换树脂,除去Bi3+及部分Pb2+,Sr2+,Ca2+,Cu2+等基体元素;在碱性条件下再通过甲苯萃取镍与丁二酮肟的络合物、稀盐酸反萃取富集镍;对分离富集条件进行了优化。对模拟标准样品进行测定,分析结果与理论值一致,相对标准偏差为1.9%,方法检出限为0.19μg.g-1。该方法已用于超导前驱粉样品中痕量镍的分析,结果令人满意。 相似文献
112.
利用可调谐激光二极管吸收光谱技术进行气体检测时,波长调制伴随的光强幅度调制,会使解调出的谐波谱线发生畸变.在傅里叶分析的基础上对可调谐激光二极管吸收光谱任意调制幅度的波长调制光谱信号进行了分析,给出了光强幅度调制引起吸收谱线畸变的理论解释.提出了在波长调制过程中进行旧步平抑幅度调制的方法来消除谱线畸变,设计了实验方案并... 相似文献
113.
利用中子飞行时间技术和BC501A液体闪烁探测器的粒子分辨特性,测量了0°方向、20 MeV氘束轰击厚金属铍靶反应产生的中子源能谱,测量的中子能谱范围为0.7~25.0 MeV。在60°方向放置芪晶体闪烁探测器,由刻度好的BC501A液体闪烁探测器归一校正后,用于中子源强度监测。利用Be(d, n) 反应中子源,采用单粒子灵敏度标定方法,实验标定了0.75~15.75 MeV能量范围内的薄膜闪烁探测器中子能量响应曲线,实验结果与蒙特卡罗模拟计算结果在8%的不确定度范围内一致。 相似文献
114.
115.
The Fengyun-2 (FY-2) meteorological satellite uses a one-dimensional dynamic angular measuring system to evaluate the stepping accuracy of the scanning mirror. The basic principle of this angular measurement is detecting the light-spot position displacement using a linear charge-coupled device (CCD). This paper presents the design of this non-contact and non-destructive measuring system. To achieve high repeatability and accuracy the centroid method is employed to estimate the light-spot energy gravity, with 20-segment polygonal approximations as a nonlinear compensation. Experimental results show that the measurement system can achieve dynamic angular measurement with up to ±5″ accuracy and 3.5″ repeatability, which makes a credible evaluation for the scanning mirror of FY-2 meteorological satellite. 相似文献
116.
A very compact Mach-Zehnder interferometer (MZI) composed of two parallel straight waveguides with left-handed material (LHM) layers is proposed. The operating principle and characteristics of the MZI with electro-optic material (EOM) core are analyzed by using the supermode theory and coupled mode theory. The result shows that regardless of material loss, a very compact MZI of only 0.87 mm × 0.022 mm can be achieved by utilizing EOM with ultrahigh electro-optic coefficient, which means a new way to fulfill a very compact electro-optic modulator or optical switch. The absorption effect of the proposed MZI is also analyzed by perturbation method which is generated by lossy LHM layers. 相似文献
117.
Consistency-dependent optical properties of lubricating grease studied by terahertz spectroscopy 下载免费PDF全文
The optical properties of four kinds of lubricating greases (urea, lithium, extreme pressure lithium, molybdenum disulfide lithium greases) with different NLGL (National Lubricant Grease Institute of America) numbers were investigated using terahertz time-domain spectroscopy. Greases with different NLGL grades have unique spectral features in the terahertz range. Comparison of the experimental data with predictions based on Lorentz--Lorenz theory exhibited that the refractive indices of each kind of lubricating grease were dependent on the their consistency. In addition, molybdenum disulfide (MoS2) as a libricant additive shows strong absorption from 0.2 to 1.4 THz, leading to higher absorption of MoS2-lithium grease than that of lithium grease. 相似文献
118.
LIU Yimin HUANG Gangming & BAO Chengguang . Department of Physics Zhongshan University Guangzhou China . Department of Physics Shaoguan University Shaoguan China 《中国科学G辑(英文版)》2004,47(5):521-530
1 Introduction Quantum dots (QDs), often referred to as artificial atoms, are currently under in-tense study because they provide ideal structures used in optical-electronic microdevices, so they are essential in developing microtechniques. They are also essential in the aca-demic aspect, because rich information on microstructures can be extracted both theo-retically and experimentally. Since the early fabrication of the QDs, external magnetic field has been used to control their propertie… 相似文献
119.
Nonlinear cascade-configuration multi-wave mixing scheme based on electromagnetically induced transparency 下载免费PDF全文
A nonlinear optical cascade-configuration multi-wave mixing (CCMWM) scheme is presented and analysed for the generation of coherent light in a six-level atomic system in the context of electromagnetically induced transparency (EIT). A detailed semi-classical study of the propagation of the generated mixing and probe fields is demonstrated. We show by numerical simulations that EIT is capable of suppressing linear and nonlinear photon absorption. The analytical dependence of the generated mixing field on the probe field and the respective detuning is also predicted. Such a nonlinear optical process can be used for generating coherent short-wavelength radiation. 相似文献
120.
Photoemission spectra are measured for Yb covered surface of wet-chemically-etched H-Si (111). The results reveal that the lattice structure of the H-Si (111) surface is stable against the deposition of Yb atoms. X-ray photoemission spectra indicate the formation of a polarized (dipole) surface layer, with the silicon negatively charged. Ultraviolet photoemission spectra exhibit the semiconducting property of the interface below one monolayer coverage. Work function variation during the formation of the Yb/H-Si (111) interface is measured by the secondary-electron cutoff in the ultraviolet photoemission spectral line. The largest decrease of work function is ~1.65eV. The contributions of the dipole surface layer and the band bending to the work function change are determined to be ~1.15eV and ~0.5eV, respectively. The work function of metal Yb is determined to be ~2.80±0.05eV. 相似文献