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31.
32.
Roberto Martínez Corte C. Eduardo Salazar E. Olivia Linzaga E. Irma 《Journal of heterocyclic chemistry》1994,31(4):1061-1063
Catalytic hydrogenation of o-nitrophenylbenz[a], benz[c], dibenz[a,h] and dibenz[a,g]acridinones using Pd/C as catalyst, at 60 psi of pressure, gave the hiterto unknown benzoquinoacridine N-oxides and benzo-pyranonaphthyridine N-oxides. The structure of all products was corroborated by ir, 1H- and 13C-nmr and mass spectra data. 相似文献
33.
G. Michałek B.R. Bułka 《The European Physical Journal B - Condensed Matter and Complex Systems》2002,28(1):121-128
The currents and their fluctuations in two capacitively coupled single electron transistors are determined in the limit of
sequential tunnelling. Our considerations are restricted to the case when the islands (dots) of the transistors are atomic-sized,
which means each of them has only one single electronic level available for the tunnelling processes. The Coulomb interactions
of accumulated charges on the both single electron transistors lead to the effect of the negative differential resistance.
An enhancement of the current shot-noise was also found. Spectral decomposition analysis indicated the two main contributions
to the shot-noise: low- and high-frequency fluctuations. It was found that the low frequency fluctuations (polarization noise)
are responsible for a strong enhancement of the current noise.
Received 9 October 2001 / Received in final form 8 March 2002 Published online 9 July 2002 相似文献
34.
Principles and recent developments in ultrasound contrast agents 总被引:6,自引:1,他引:5
The behaviour of gas bubbles and gas encapsulated spheres as echographic contrast agents is reviewed. Compared with rigid spheres, gas bubbles are superior scattering agents and they offer a number of useful properties which can be exploited in a variety of ways. The analysis of their velocity of sound, back-scatter intensity, second harmonic emission and resonant frequency opens up new perspectives in the development of contrast agents for echocardiographic research with potential clinical applications. 相似文献
35.
Adsorption of the copper ions from aqueous solutions, benzene, and water on the active carbon obtained by chemical activation
from walnut shells was studied. The active carbon was additionally oxidized with hydrogen peroxide and then impregnated with
nitrogen-containing compounds. As a result of impregnation with melamine, a secondary porosity is formed within the oxidized
active carbon, leading to an increase in the specific surface of the sorbent. A modified carbon surface is heterogeneous,
and the carbons themselves exhibit catalytic activity in the oxidation of luminol and decomposition of hydrogen peroxide. 相似文献
36.
37.
The effective signal in x-ray diffraction analysis of material properties often contains high frequency (noise) and low frequency
(trend) components as additive parts. It is necessary to extract the effective signal from the noise to ensure high quality
of signal processing. Digital filters of Volterra type are proposed for filtering purposes and a comparison of Volterra filtration
implemented on x-ray diffraction data versus results from a set of other digital filters is given. 相似文献
38.
Marek Pękała Jan Mucha Benedicte Vertruyen Rudi Cloots Marcel Ausloos 《Journal of magnetism and magnetic materials》2006
Samples of La0.7Ca0.3Mn1−xGaxO3 with x=0, 0.025, 0.05 and 0.10 were prepared by standard solid-state reaction. They were first characterized chemically, including the microstructure. The magnetic properties and various transport properties, i.e. the electrical resistivity, magnetoresistivity (for a field below 8 T), thermoelectric power and thermal conductivity measured each time on the same sample, are reported. The markedly different behaviour of the x=0.1 sample from those with a smaller Ga content, is discussed. The dilution of the Mn3+/Mn4+ interactions with Ga doping considerably reduces the ferromagnetic double exchange interaction within the manganese lattice leading to a decrease of the Curie temperature. The polaron binding energy varies from 224 to 243 meV with increased Ga doping. 相似文献
39.
In this paper we study the pollution-error in the h-version of the finite element method and its effect on the local quality of a-posteriori error estimators. We show that the pollution-effect in an interior subdomain depends on the relationship between the mesh inside and outside the subdomain and the smoothness of the exact solution. We also demonstrate that it is possible to guarantee the quality of local error estimators in any mesh-patch in the interior of a finite-element mesh by employing meshes which are sufficiently refined outside the patch. 相似文献
40.