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91.
FANG  Yu YIN  Yi-Qing 等 《中国化学》2002,20(4):317-321
The aggregation of dansyl chloride (DNS-Cl) in acetone has been studied in detail by steady-state fluorescence techniques.It has been demonstrated that DNS-Cl is stable in acetone during purification and aggregation study processes.The aggregates are not solvolyzed in acetone,and do not take part n any chemical reactions either.It has been found that DNS-Cl tends to aggregate even when its concentration is much lower than its solubility in acetone.The aggregation is reversible,and both the aggregation and the deaggregation are very slow processes.Introduction of SDS has a positive effect upon the formation and stabilization of the aggregates.  相似文献   
92.
朱世秋  E.I.RAU 《中国物理快报》2002,19(9):1329-1332
We present a novel contactless and nondestructive method called the surface electron beam induced voltage (SEBIV) method for characterizing semiconductor materials and devices.The SEBIV method is based on the detection of the surface potential induced by electron beams of scanning electron microscopy (SEM).The core part of the SEBIV detection set-up is a circular metal detector placed above the sample surface.The capacitance between the circular detector and whole surface of the sample is estimated to be about 0.64pf.It is large enough for the detection of the induced surface potential.The irradiation mode of electron beam (e-beam) influences the signal generation When the e-beam irradiates on the surface of semiconductors continuously,a differential signal is obtained.The real distribution of surface potentials can be obtained when a pulsed e-beam with a fixed frequency is used for irradiation and a lock-in amplifier is employed for detection.The polarity of induced potential depends on the structure of potential barriers and surface states of samples.The contrast of SEBIV images in SEM changes with irradiation time and e-beam intensity.  相似文献   
93.
In this paper a uniqueness theorem for a skewperiodic boundary value problem is obtained. By using the optimal control method, we derive the best estimate for the integration mean ensuring that the results hold.  相似文献   
94.
In the light of the recent works by Sen(hep-th/o203211,hep-th/0203265,hep-th/0204143)and Gibbons(hepth/0204008),we present a phase-plane analysis on the cosmology containing a rolling tachyon field in a potential resulting from string theory.we show that there is no stable point on the phase-plane,which indicates that there is a coincidence problem if we consider the tachyon as a candidate for quintessence.Furthermore,we also analyse the phase-plane of the cosmology cotaining a rolling tachyon field for an exactly solvable toy potential in which the critical point is stable.Therefore,it is possible for the rolling tachyon to be a candidate for quintessence if we give up the strict constraint on the potential or find a more appropriate effective potential for the tachyon from M/String theory.  相似文献   
95.
Intrinsic Josephson junctions on Bi2Sr2CaCu2O8 δ single crystals are successfully fabricated using photolithography and Ar jon milling .Here we discuss the properties of the surface CuO2/metal bilayers and surface junctions prepared with different crystal cleavage conditions and metal film deposition techniques.We show that,by cleaving the crystal at liquid nitrogen temperature in vacuum,the contents of the (interstitial) oxygen in the Bi-O layers become stable upon cleavage,leading to a CuO2/metal bilayer and to surface junctions with reproducible properites,These results can be useful for practical device fabrications as well as for the studies of the contact properties between high Tc superconductors and normal metals.  相似文献   
96.
The operator sets, which are the subject of this paper, have been studied in many papers where, under different restrictions on the generating operators, convexity, compactness in the weak operator topology, and nonemptiness were proved for sets of different classes under study. Then the results obtained were used in these papers to solve several applied problems. Namely, they played the key role in establishing the dichotomy of nonautonomous dynamical systems, with either continuous or discrete time. In the present paper, we generalize and sharpen the already known criteria and obtain several new criteria for convexity, compactness, and nonemptiness of several special operator sets. Then, using the assertions obtained, we construct examples of sets of the form under study which are nonconvex, noncompact in the weak operator topology, as well as empty, and are generated by "smooth" operators of a special class. The existence problem for such sets remained open until the authors of this paper announced some of its results.  相似文献   
97.
杨伟铮  谢达材等 《物理》1992,21(11):659-665
把Rietveld精化方法用于处理同步辐射X射线和中子粉末衍射数据,使得粉末试样的结构研究有很大发展。本文在简要介绍两种粉末衍射术和Rietveld方法之后,用实例描述它们在结构精化、解未知结构、沸石、有关微孔材料及磁结构材料测定中的应用。  相似文献   
98.
99.
STUDIES ON THE MOLECULAR STRUCTURE OF WT—12 DERIV ATIVE OF PYRAZOLO [3   总被引:1,自引:0,他引:1  
陈茹玉  王宏根 《结构化学》1991,10(2):132-135
  相似文献   
100.
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