分光光度法测定鱼翅中锗

本文用分光光度法测定鱼翅中的总锗量。结果表明 ,鱼翅中的总锗含量为 18.2 5— 2 2 .75 μg·g-1;回收率为 85 .8%— 93.2 %。     

Persistence of Hyperbolic Tori in Generalized Hamiltonian Systems

In this paper we prove the persistence of hyperbolic invariant tori in generalized Hamiltonian systems, which may admit a distinct number of action and angle variables. The systems under consideration can be odd dimensional in tangent direction. Our results generalize the well-known results of Graff and Zehnder in standard Hamiltonians. In our case the unperturbed Hamiltonian systems may be degenerate. We also consider the persistence problem of hyperbolic tori on sub manifolds.     

Enhanced saturable absorption of MoS_2 black phosphorus composite in 2 μm passively Q-switched Tm: YAP laser

We report the fabrication of an MoS_2 black phosphorus(BP) composite saturable absorber by liquid phase exfoliation and the spin-coating method and further exploitation to build a 2 μm passively Q-switched Tm:YAP laser. Such a composite based Q-switched laser with a duration of 488 ns and corresponding peak power of 85.9 W is obtained, which shows an improved saturable absorption effect than that of single MoS_2(616 ns,68.7 W) and BP(932 ns, 22.4 W). The results indicate that simple and reasonable fabrication of the vertical composite from two-dimensional atomic layer materials opens up the possibility to create an unprecedented saturable absorber with exciting properties.     

受撞击黏弹性基支弹性直梁的动力响应

本文研究了半无限线性黏弹性Ｗｉｎｋｌｅｒ地基上的弹性直梁受低速运动物体撞击的动力响应分析问题．在不计撞击体中应力波传播的条件下，推导出了关于撞击力Ｆ（ｔ）的非线性Ｖｏｌｔｅｒｒａ积分方程，得出了梁的横向位移Ｗ（ｘ，ｔ）的一般表达式．作为实例，本文对两端简支弹性直梁受圆球对心横向撞击的问题进行了分析计算．     

winkler地基上弹性圆薄板受刚体撞击的动力响应

本文针对工程实际中所遇到的撞击问题,在事先仅知撞击体初始速度的条件下,研究分析了半无限粘弹性Winkler地基上的弹性圆薄板受刚体撞击的动力响应问题,推导出了关于撞击力F(t)的非线性Volterra积分方程,给出了薄板位移响应W(r,,t)的一般表达式,并给出了相应的数值求解方法。作为实例,本文对周边固定的弹性圆薄板在圆心处受刚球撞击问题进行了分析计算,并对某些参数的影响进行了讨论。     

岩石材料的一种蠕变损伤方程

通过大量的岩石蠕变试验研究，总结出了以能描述损伤历史的蠕变模量为参数的岩石蠕变损伤方程，由该方程能方便地定出任意蠕变时刻的损伤状态和进行蠕变损伤的测定。     

Broad-band phase retrieval method for transient radial shearing interference using chirp Z transform technique

The transient radial shearing interferometry technique based on fast Fourier transform (FFT) provides a means for the measurement of the wavefront phase of transient light field. However, which factors affect the spatial bandwidth of the wavefront phase measurement of this technology and how to achieve high-precision measurement of the broad-band transient wavefront phase are problems that need to be studied further. To this end, a theoretical model of phase-retrieved bandwidth of radial shearing interferometry is established in this paper. The influence of the spatial carrier frequency and the calculation window on phase-retrieved bandwidth is analyzed, and the optimal carrier frequency and calculation window are obtained. On this basis, a broad-band transient radial shearing interference phase-retrieval method based on chirp Z transform (CZT) is proposed, and the corresponding algorithm is given. Through theoretical simulation, a known phase is used to generate the interferogram and it is retrieved by the traditional method and the proposed method respectively. The residual wavefront RMS of the traditional method is 0.146λ, and it is 0.037λ for the proposed method, which manifests an improvement of accuracy by an order of magnitude. At the same time, different levels of signal-to-noise ratios (SNRs) from 50 dB to 10 dB of the interferogram are simulated, and the RMS of the residual wavefront is from 0.040λ to 0.066λ. In terms of experiments, an experimental verification device based on a phase-only spatial light modulator is built, and the known phase on the modulator is retrieved from the actual interferogram. The RMS of the residual wavefront retrieved through FFT is 0.112λ, and it decreases to 0.035λ through CZT. The experimental results verify the effectiveness of the method proposed in this paper. Furthermore, the method can be used in other types of spatial carrier frequency interference, such as lateral shearing interference, rotational shearing interference, flipping shearing interference, and four-wave shearing interference.     

二维单层MoSi2X4 (X=N,P, As)的电子结构及光学性质研究

采用平面波超软赝势方法研究了二维单层MoSi₂X₄ (X=N, P, As)的稳定性、电子结构和光学性质. 研究结果显示, 基于单层MoSi₂N₄的两种同分异构体M1和M2所构建的六种晶体结构具有较好的动力学稳定性. 通过能带和有效质量的计算, 单层MoSi₂N₄在MoSi₂X₄ (X=N, P, As)六种晶体结构中显示出最宽的间接带隙和最高的载流子迁移率. 随后带边电位的计算结果表明, 单层MoSi₂N₄带边势分别为M1: –0.368、1.416 V, M2: –0.227、1.837 V, 其结果相较于MoSi₂P₄和MoSi₂As₄导带边电位更负, 价带边电位更正, 是六种晶体结构中最适合用作光催化剂的材料. 同时, 光吸收谱的计算结果显示, 单层MoSi₂N₄的光学吸收表现出明显的各向异性, 在可见光和紫外光波段内具有较强的光吸收能力, 说明其在可见光催化领域有着潜在的应用前景. 这些结果为进一步深入研究二维单层MoSi₂N₄在光催化水解领域的应用提供了理论指导.     

短纤维取向对Al_2O_(3f) C_f/ZL109复合材料干滑动摩擦磨损性能的影响

利用挤压铸造法制备了 Al2 O3 f Cf/ZL10 9短纤维混杂金属基复合材料 ,并利用统计学方法对比研究了在滑动速度 0 .837m/s、载荷 196 N条件下纤维取向对该混杂复合材料干滑动摩擦磨损性能的影响 .结果表明 :在纤维平行取向和垂直取向时 ,该混杂复合材料的磨损率和摩擦系数均服从正态分布 ;平行取向情况下磨损率均值大于垂直取向下的磨损率 ,而摩擦系数均值小于垂直取向 ;纤维垂直取向有利于复合材料耐磨性能的提高 ,2种取向下复合材料的主要磨损机制均为犁沟磨损     

用记忆材料模拟流变大变形问题

本文采用具有记忆特性的有机玻璃材料结合网格法测量技术，以软岩巷道围岩流变形为例展开了有限变形模拟试验的研究工作，并以有限变形理论为基础结合现代计算机技术进行了实验数据处理。实例分析表明，所用方法和技术具有广泛的灵活性、可靠性的实用性。