MAGNETIC PROPERTIES AND CRYSTALLIZATION OF THE RAPIDLY QUENCHED (Fe1-xNdx) 81.5B18.5 ALLOYS

Magnetic properties and crystallization behaviors of amorphous (Fe_1-xNd_x) _81.5B_18.5 alloys were studied. The crystallization temperature is found to rise at first and then drop monotonically with x, having a maximum value of 976K at x=0.11 (9at% Nd). The (Fe_1-xNd_x) _81.5B_18.5 alloys prepared at a quenching rate of v_s = 6.6m /s are amorphous, and exhibit good glass formability. Both the coercive field H_c and energy product (BH)_max depend strongly on Nd concentration. Amorphous (Fe_1-xNd_x) _81.5B_18.5 alloys with higher Nd concentration have a high coercive field at low temperature, due to the large random uniaxial anisotropy of Nd. The room-temperature H_c and (BH)_max obtained on optimal annealing con-ditions show two maxima as a function of Nd concentration x. The highest room-temperature coercive field H_c =22 kOe within the Nd concentrations around x=0.368 and the maximum energy product(RH)_max= 13.3 MG·Oe at x =0.055 are observed. The hard magnetic properties of these crystallized samples are related to the presence of the bard magnetic Nd₂Fe₁₄B phase.     

EFFECT OF MANGANESE SUBSTITUTION IN R2AlFe16-x Mnx(R=Y,Ho,Nd AND Pr)COMPOUNDS ON STRUCTURAL AND MAGNETIC PROPERTIES

The structural and magnetic properties of R₂AlFe_16-xMn_x(0≤x≤8 for Y,Ho,0≤x≤10 for Pr, 0≤x≤16 for Nd)compounds have been investigated by means of X-ray diffraction and magnetization measurements.The R₂AlFe_16-xMn_x compounds have a hexagonal Th₂Ni₁₇-type structure for R=Y and Ho, and a rhombohedral Th₂Zn₁₇-type structure for Nd and Pr.With increasing x,the unit-cell volumes have a small increase initially,followed by a greater linear increase.The Curie temperature and the saturation magnetizati on of these compounds show marvelous drop with increasing x.Compensation point was observed in the temperature dependence of the magnetization for Ho₂AlFe₁₂Mn₄ compound.     

2∶17型快淬Sm-Fe-Cu-Si-C的硬磁性

研究了Sm₂Fe₁₅Si₂C和Sm₂Fe₁₄CuSi₂C化合物的结构与磁性,测量了化合物的居里温度T_C和饱和磁化强度M_s.通过对取向样品在磁场平行和垂直取向方向测量的磁化曲线的拟合得到了不同温度下化合物的磁晶各向异性场H_A和各向异性常数K₁和K₂.实验结果表明,Cu的     

Sm2Fe14.5Cu0.5Ca2Cx快淬带的磁力显微镜研究

用磁力显微镜研究了Sm₂Fe_14.5Cu_0.5Ca₂C_x快淬带退火后的微结构与磁畴结构.从实验所得的形貌图和磁力图发现晶粒尺寸在25—55nm之间,磁畴尺寸为200—400nm,磁畴尺寸远大于晶粒尺寸.磁畴跨越许多晶粒,即出现交换作用畴结构.对磁力图的强度谱密度、最大相位移和粗糙度的分析表明,这些量与材料的内禀磁性（如H_A）有一定的关联. 关键词：     

2∶17型快淬Sm-Fe-Cu-Si-C的硬磁性

研究了Sm₂Fe₁₅Si₂C和Sm₂Fe₁₄CuSi₂C化合物的结构与磁性,测量了化合物的居里温度T_C和饱和磁化强度M_s.通过对取向样品在磁场平行和垂直取向方向测量的磁化曲线的拟合得到了不同温度下化合物的磁晶各向异性场H_A和各向异性常数K₁和K₂.实验结果表明,Cu的     

电流退火铁基薄带巨磁阻抗效应的影响

研究了电流退火工艺对铁基非晶合金Fe₈₄Zr₈Nb_3.5B_3.5Cu_{1〈/sub>薄带巨磁阻抗效应的影响.实验结果表明,该铁基合金的巨磁阻抗ΔZ/Z随退火电流的增加而增强,当电流为820mA时,ΔZ/Z达到最大值62％,阻抗变化灵敏度可达约0.23％（A/m)^-1.结合此合金在电流退火燧后电性能和软磁性能的演变,讨论了材料的巨磁阻抗效应借助趋肤效应与交流频率和外加纵向磁场的关系. 关键词：}     

基于深紫外激光-光发射电子显微技术的高分辨率磁畴成像

基于磁二色效应的光发射电子显微镜磁成像技术是研究薄膜磁畴结构的一种重要研究手段,具有空间分辨率高、可实时成像以及对表面信息敏感等优点.以全固态深紫外激光(波长为177.3 nm;能量为7.0 eV)为激发光源的光发射电子显微技术相比于传统的光发射电子显微镜磁成像技术(以同步辐射光源或汞灯为激发源),摆脱了大型同步辐射光源的限制;同时又解决了当前阈激发研究中由于激发光源能量低难以实现光电子直接激发的技术难题,在实验室条件下实现了高分辨磁成像.本文首先对最新搭建的深紫外激光-光发射电子显微镜系统做了简单介绍.然后结合超高真空分子束外延薄膜沉积技术,成功实现了L10-FePt垂直磁各向异性薄膜的磁畴观测,其空间分辨率高达43.2 nm,与利用X射线作为激发源的光发射电子显微镜磁成像技术处于同一量级,为后续开展高分辨磁成像提供了便利.最后,重点介绍了在该磁成像技术方面取得的一些最新研究成果:通过引入Cr的纳米"台阶",成功设计出FePt的(001)与(111)双取向外延薄膜;并在"台阶"区域使用线偏振态深紫外激光观测到了磁线二色衬度,其强度为圆二色衬度的4.6倍.上述研究结果表明:深紫外激光-光发射电子显微镜磁成像技术在磁性薄膜/多层膜体系磁畴观测方面具备了出色的分辨能力,通过超高真空系统与分子束外延薄膜制备系统相连接,可以实现高质量单晶外延薄膜制备、超高真空原位传输和高分辨磁畴成像三位一体的功能,为未来磁性薄膜材料的研究提供了重要手段.     

Structural and magnetic properties of Dy2Co17—xMnx compounds

Using x-ray diffraction and magnetic measurements, we have studied the structural and magnetic properties of Dy₂Co_17-xMn_x (x=0∽5) compounds with a rhombohedral Th₂Zn₁₇-type structure. With an increasing Mn concentration x, the unit-cell volume V was found to increase linearly. The Curie temperature T_c decreases linearly, and the saturation magnetization M_s at 5K first increases slightly for x<1, then decreases rapidly for x>1 with a further increase of Mn concentration x. In compounds for x=1～3, a spin reorientation was found. A magnetic diagram of the compounds is given.     

Change in the magnetic ground state of LaFe11.4Al1.6 compound by the substitution of Mn for Fe

The structure and magnetic properties of La(Fe_{1-x}Mn_x)_{11.4}Al_{1.6} (0≤x≤0.25)compounds have been studied. The NaZn_{13}-type structure is preserved and the lattice parameter increases linearly with increasing the Mn concentration. The magnetic ground state changes from the antiferromagnetic to the spin-glass or the cluster-glass state by the substitution of Mn for Fe. Furthermore, a field-induced transition from cluster glass to ferromagnet is found for the samples with x=0.05 and 0.10.     

Magnetism and magnetic entropy change in LaFe11Al2Cx compounds around room temperature

Magnetism and magnetic entropy changes in LaFe11A12Cx(x=0.0, 0.2 and 0.5) compounds have been investigated.The Curie temperature TC is conveniently controlled from 200K to room temperature by varying the carbon concentration.Large magnetic entropy change is obtained over a wide temperature range due to the high magnetization and the drastic decrease in the magnetization around TC.The large magnetic entropy change in wide temperature range,low cost and the convenience of controlling TC suggest that the LaFe11Al2Cx compounds are promising candidates for magnetic refrigerants in the corresponding temperature range.