表面活性剂增敏光度法测定海产品中的微量镉(Ⅱ)

在六次甲基四胺缓冲溶液(pH=6.3)存在下,以二甲酚橙(XO)作显色剂,表面活性剂十六烷基三甲基溴化铵(CTMAB)对镉(Ⅱ)与XO的显色反应具有增敏作用,形成的镉(Ⅱ)-XO-CTMAB三元配合物呈紫色,配合物的最大吸收波长为605nm,表观摩尔吸光系数为2.04×10~5 L/(mol.cm)。镉(Ⅱ)的浓度在0～8μg(25mL)内符合比耳定律,线性回归方程为A=0.025c+0.2,检出限为5×10~(-4)μg/mL。该法用于海产品中微量镉的测定,测定结果的相对标准偏差为0.104％,回收率为91.0％。     

Investigation of transfer ionization in collisions of partially stripped carbon ions with helium at low to intermediate velocities

The ratios of transfer ionization (TI) to single-electron capture (SC) cross sections have been measured for the collisions of partially stripped C^q+ ions (q=1--4) with He. The collision velocity ranges from 0.7 to 4.4v₀ (v₀ is the Bohr velocity). The projectile-ion and recoil-ion coincidence technique is used to separate the processes of TI and SC. The ratios reach the maximum when the velocity is about 3.7v₀ This can be explained qualitatively based on the two-step mechanism. The experimental results are also compared with the results calculated using the classical trajectory Monte Carlo (CTMC) method. The CTMC results are in agreement with the experimental data basically. The discrepancies in higher velocity region are interpreted by the effective charge effect.     

Q235钢在假单胞菌和铁细菌混合作用下的腐蚀行为

采用腐蚀失重法、电化学阻抗谱(EIS)和表面分析技术研究了Q235钢在假单胞菌和铁细菌共同作用下的腐蚀行为.结果表明:与单种菌相比,两种菌混合作用下Q235钢腐蚀受到了抑制.混菌体系中金属电极自腐蚀电位升高,腐蚀电流密度减小,交流阻抗值随时间增大.扫描电子显微镜(SEM)分析结果表明混合菌体系中Q235钢表面形成了均匀致密的腐蚀产物膜.     

通过熵产率构建的两类损失模型计算精度比较

本文采用雷诺平均及雷诺平均-大涡模拟方法对一直叶栅进行数值模拟,分别对比分析了两类基于熵产率构建的损失模型结果。一类为假设模拟结果的湍流耗散等于湍流生成构建的模型,称为Moore模型;另一类为通过湍流模型参数直接求解湍流耗散率构建的模型,称为K-B模型。经过对比4°攻角下当地损失系数及2°、4°、7°攻角下积分损失可发现,无论是雷诺平均还是雷诺平均-大涡模拟方法模拟,Moore模型均与K-B模型在定性及定量上有一定差距。     

延迟退休和经济增长

§ 1　IntroductionPopulation aging is a common feature in developed economies.How to deal with it?Most governments turn to postponing retirement.What impact does it have on macroeco-nomic performance?For instance,if a longer working time decreases the ratio of retiredpeople to working people,does itincrease the aggregate saving rate?Doesittherefore accel-erate economic growth?We study these issues in a general equilibrium model of life cyclesavings combined with endogenous growth.An intuitiv…     

A DOMAIN DECOMPOSITION ALGORITHM WITH FINITE ELEMENT-BOUNDARY ELEMENT COUPLING

A domain decomposition algorithm coupling the finite element and the boundary element was presented. It essentially involves subdivision of the analyzed domain into sub-regions being independently modeled by two methods, i.e., the finite element method (FEM) and the boundary element method (BEM). The original problem was restored with continuity and equilibrium conditions being satisfied on the interface of the two sub-regions using an iterative algorithm. To speed up the convergence rate of the iterative algorithm, a dynamically changing relaxation parameter during iteration was introduced. An advantage of the proposed algorithm is that the locations of the nodes on the interface of the two sub-domains can be inconsistent. The validity of the algorithm is demonstrated by the consistence of the results of a numerical example obtained by the proposed method and those by the FEM, the BEM and a present finite element-boundary element (FE-BE) coupling method.     

需求和汇率风险下的全球供应链汇率风险对冲策略

在下游零售商同时面临市场需求风险和汇率风险的背景下,研究了汇率风险对冲(外汇期货对冲)策略在全球供应链运作及风险管理中的作用。在无/有对冲策略两种情形下分别构建了上游制造商和下游零售商的动态博弈模型,并求解了均衡结果。两种情形下的均衡结果显示,汇率风险对冲策略可以提高供应链系统订货量、增加零售商收益的期望值和确定性等价量、增加供应链系统的总收益。进一步讨论了有对冲策略的情形下,两类外生风险对供应链均衡决策变量和盈利性的影响方式。结果表明,汇率风险对冲策略对汇率风险起到了有效的隔离作用,避免了供应链下游的汇率风险向上游企业传递,并能实现供应链收益与风险的权衡。     

反应pH值对微波法合成的Mo修饰的Pt/C催化剂结构和乙醇电氧化催化性能的影响

通过调节微波反应溶液的pH值合成了一系列Mo修饰的Pt/C催化剂并用于乙醇的电氧化催化反应.利用X射线衍射(XRD)、透射电子显微镜(TEM)及X射线光电子能谱(XPS)对催化剂的晶型结构、微观形貌、粒径尺寸和表面电子结构进行了表征,并采用循环伏安法(CV)、计时电流法(CA)和电化学阻抗谱(EIS)对催化剂的乙醇电氧化催化性能进行了测试.结果表明,碱性环境有利于催化剂组分在碳载体上的均匀分布,pH值为14时制得的催化剂组分颗粒尺寸最小,且分布最均匀.该催化剂不仅表现出了最大的有效电化学比表面积和最高的乙醇电氧化催化活性,而且具有最稳定的乙醇氧化催化性能.     

84.5 MeV12C4+离子诱发金属靶原子发射的Kβ与Kα-X射线强度比值的研究

本实验是在中国科学院兰州近代物理研究所,国家实验室的重离子加速器上完成的.实验用OR-TEC公司生产的HPGe X射线探测器测量了84.5 MeV的12C4+离子轰击Cu,Mo,Ag,Cd,In,Sn,W和Au金属靶产生的K壳层特征X射线谱,计算了Kβ与Kα-X射线强度的比值,并将结果与Scofield用HartreeFock-Slater模型计算出的理论值与用其它方法(如:衰变幅射,用光子,电子,质子等粒子与靶相互作用)得到的实验值进行了比较.比较结果表明用84.5 MeV的12C4+离子轰击Cu,Mo,Ag,Cd,In,Sn,W和Au金属靶产生的Kβ与Kα-X射线强度比值比理论值和其它实验值要大许多.     

妙解一则

题目已知f(x)一了1 扩，且xl并为，求证:}f(x，)一f(两)J<}x，一x:1.证明设百一(1，x，)，万~(l，xZ). x、护x:，}f(x，)一f(x:){一}1百，一}万日杜娟$新疆呼图壁县111团中学!831206~~