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最近发现的水合钴氧化物超导体引起了超导领域的强烈兴趣.由于该超导体非常不稳定,因此有关该超导体的合成和表征是个重要的基本课题.本文报道几种典型的合成方法,并对所得到的超导体进行表征.我们将着重介绍利用歧化反应来制备含有很低的钠离子浓度和很高的水合氢离子浓度的钴氧化物超导体的新方法. 相似文献
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Neutron Powder Diffraction Study on the Non-Superconducting Phases of ThFeAsN_(1-x)O_x(x=0.15,0.6)Iron Pnictide 下载免费PDF全文
We use neutron powder diffraction to study the non-superconducting phases of ThFeAsN_(1-x)O_x with x = 0.15,0.6.In our previous results of the superconducting phase ThFeAsN with T_c = 30 K,no magnetic transition is observed by cooling down to 6 K,and possible oxygen occupancy at the nitrogen site is shown in the refinement[Europhys.Lett.117(2017)57005].Here in the oxygen doped system ThFeAsN_(1-x)O_x,two superconducting regions(0≤x≤0.1 and 0.25≤x≤0.55)are identified by transport experiments[J.Phys.:Condens.Matter30(2018)255602].However,within the resolution of our neutron powder diffraction experiment,neither the intermediate doping x= 0.15 nor the heavily overdoped compound x = 0.6 shows any magnetic order from 300 K to 4 K.Therefore,while it shares the common phenomenon of two superconducting domes as most 1111-type iron-based superconductors,the magneticall.y ordered parent compound may not exist in this nitride family. 相似文献
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The recent discovery of high-temperature superconductivity in iron-based pnictides (chalcogenides) not only trig- gers tremendous enthusiasm in searching for new superconducting materials, but also opens a new avenue to the study of the Kondo physics. CeFeAsO is a parent compound of the 1111-type iron-based superconductors. It shows 3d- antiferromagnetic (AFM) ordering below 139 K and 4f-AFM ordering below 4 K. On the other hand, the phosphide CeFePO is a ferromagnetically corelated heavy-fermion (HF) metal with Kondo scale TK 10 K. These properties set up a new platform for research of the interplay among magnetism, Kondo effect, and superconductivity (SC). In this review, we present the recent progress in the study of chemical pressure effect in CeFeAsOl_yFy (y = 0 and 0.05). This P/As-doping in CeFeAsO serves as an effective controlling parameter which leads to two magnetic critical points, Xcl -- 0.4 and Xc2 - 0.92, associated with suppression of 3d and 4f magnetism, respectively. We also observe a turning point of AFM-FM ordering of Ce3+ moment at Xc3 - 0.37. The SC is absent in the phase diagram, which is attributed to the destruction to Cooper pair by Ce-FM fluctuations in the vicinity of Xcl. We continue to investigate CeFeAsl-xPxO0.95Fo.os. With the separation of xcl and xc3, this chemical pressure results in a broad SC region 0〈 x 〈 0.53, while the original HF behavior is driven away by 5% F- doping. Different roles of P and F dopings are addressed, and the interplay between SC and Ce-4f magnetism is also discussed. 相似文献
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用固相反应法和脉冲激光沉积 (PLD)制备了CaCu3Ti4O1 2 块材和薄膜 ,获得了相对介电常数ε′( 1kHz ,3 0 0K)高于140 0 0的介电特性 ,是目前该体系最好的结果 .报道了 ( 0 0l)取向高质量CaCu3Ti4O1 2 外延薄膜及其介电性质 .CaCu3Ti4O1 2 相对介电常数ε′在 10 0— 3 0 0K温度范围内基本保持恒定 ,稳定性好 .基于跳跃电导模型 ,对CaCu3Ti4O1 2薄膜介电电导的频率依赖关系作了合理解释 相似文献
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SYNTHESIS AT AMBIENT PRESSURE AND SUPERCONDUCTIVITY OF Hg-DOPED TI-BASED DOUBLE [(T1, Hg)-O]-LAYERED CDPHATES 下载免费PDF全文
The Hg-doped T1-based 2201 and 2212 phase layered cuprates have been successfully syn-thesized at ambient pressure and identified by X-ray powder diffraction and electron diffraction analysis. Compared with pure T1-based 2212 phase compound, there are indications that the corresponding Hg-doped T1-based compound (T11.8Hg0.2)Ba2CaCu2Oz exhibits much higher Tc (> 132K). 相似文献