The influence of nickel dopant on the microstructure and optical properties of SnO2 nano-powders

The microstructure and optical properties of Ni-doped SnO2 nano-powders are studied in detail. By Ni-doping, not only the grain size reduces, but also the grain shape changes from nano-rods to spherical particles. The crystallization becomes better with annealing temperature increasing. The band gap energy decreases as nickel doping level increases. The sp-d hybridization and alloying effect due to amorphous SnO2-x phase should be responsible for the band gap narrowing effect. Nickel dopant does not change the photoluminescence （PL） peak positions.     

CO2激光和等离子体清洗提高石英基片损伤阈值

 采用连续CO₂激光和真空等离子体相结合的方法对石英基片进行清洗。通过光学显微图、水接触角、透过率和损伤阈值测量分别表征了CO₂激光和等离子体对真空硅脂蒸发物污染过的石英基片的清洗效果。研究表明：对于真空硅脂蒸发物污染后的石英基片，可以先采用低能量的CO₂激光进行大面积清洗，再用真空等离子体进行精细清洗。光学显微图像表明：清洗后的基片表面的油珠被清除干净；水滴接触角由63°下降到4°；在400 nm附近，基片透过率由92.3%上升到93.3%；损伤阈值由3.77 J/cm²上升到5.09 J/cm²。     

含胺基功能性单体的聚合研究 XIV.含二甲氨基丙烯酰类衍生物与过硫酸钾引发体系引发的丙烯酰胺聚合

N-(N′,N′-二甲氨基亚甲基)甲基丙烯酰胺、甲基丙烯酸N,N二甲氨基乙酯、可聚合叔胺、氧化还原引发体系、超高分子量聚丙烯酰胺     

BENDING OF A CIRCULAR CYLINDER CONTAINING A CRACK

The sludy of bending of cracked circular cylinders is of more significance.The bendingof cylinders containing radical crack or cracks was discussed by refs.[1]-[4]and that ofconcentrically craked circular cylinders was studied by[5].Continuing[6]and usingcomplex variable methods in elasticity,this paper deals with the bending problems of acircular cylinder,containing an internal linear crack at any position under an acting forceperopendicular to the crack.The general forms of displacements stresses,and stress-intensity factors,expressed in terms of series,are obtained and to this bending problemswith small Ah are presented good approximate formulas for the stress-intebsity factorswhose variations with the center of the crack are analysed.Finally,the twist angle per unitlength and the center of bending for the radically cracked circular cylinder,one of whosecrack-tips is located at the origin,have been computed and the results are almost the sameas that calculated in[1].     

单层介质膜的反射起偏

本文讨论了单层介质膜反射起偏的特点,并导出起偏角所满足的关系式。     

电容器放电的演示

这个演示可以说明电容器的几个基本性能,使得这些性能有趣和可信。应该特别指出电容器本来就是一个把电介质放在金属板间做成的。以静电场形式储存能量的系统。     

四氯苯基卟啉锰配合物催化苯乙烯不对称环氧化反应

金属卟啉;催化剂;对映体过量;四氯苯基卟啉锰配合物催化苯乙烯不对称环氧化反应     

芳纶/环氧纤维复合材料超高速撞击特性研究

对芳纶/环氧复合材料的超高速撞击特性进行了实验研究,分析了芳纶/环氧复合材料撞击损伤区域的破坏形式和损伤特性,提出了以纱线断裂数目、穿孔体积等作为撞击吸能特性的表征参数,得到了芳纶/环氧纤维复合材料的超高速撞击防护性能和破坏规律,并讨论了撞击过程中的能量转换和传递过程。结果表明:随着厚度增加,芳纶/环氧复合材料超高速撞击防护性能也相应提高,但其防护效率却有所降低。当厚度较薄时,芳纶/环氧复合材料会被超高速弹丸直接贯穿;随着厚度增加,复合材料撞击损伤机理发生改变,复合材料发生层间开裂现象,并对弹丸产生分层破碎效应。     

稀有分散元素分析方法的研究进展

综述了1990年以来国内外关于镓、铟、铊、锗、硒和碲等稀有分散元素的样品分解方法、分离富集方法以及主要的检测方法,检测方法包括分光光度法、分子荧光光谱法、原子荧光光谱法、原子吸收光谱法、电化学分析法、电感耦合等离子体原子发射光谱法、电感耦合等离子体质谱法、中子活化分析法和化学发光法等,指出了各分析方法的特点和不足,并展望了这些方法在稀有分散元素分析中的应用前景(引用文献90篇)。